Article(id=1239973083646324902, tenantId=1146029695717560320, journalId=1205117023404326918, issueId=1239973077845603299, articleNumber=null, orderNo=null, doi=10.16155/j.0254-1793.2024-0030, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1705248000000, receivedDateStr=2024-01-15, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1773562220726, onlineDateStr=2026-03-15, pubDate=1730304000000, pubDateStr=2024-10-31, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1773562220726, onlineIssueDateStr=2026-03-15, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1773562220726, creator=13701087609, updateTime=1773562220726, updator=13701087609, issue=Issue{id=1239973077845603299, tenantId=1146029695717560320, journalId=1205117023404326918, year='2024', volume='44', issue='10', pageStart='1647', pageEnd='1826', issueExtLink='null', onlineDate='null', pubDate='null', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1773562219344, creator=13701087609, updateTime=1773563041495, updator=13701087609, preIssue=null, nextIssue=null, ext={EN=IssueExt(id=1239976526251356920, tenantId=1146029695717560320, journalId=1205117023404326918, issueId=1239973077845603299, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1239976526251356921, tenantId=1146029695717560320, journalId=1205117023404326918, issueId=1239973077845603299, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null}, startPage=1665, endPage=1678, ext={EN=ArticleExt(id=1239973083885400245, articleId=1239973083646324902, tenantId=1146029695717560320, journalId=1205117023404326918, language=EN, title=Study on the quality evaluation method of the characteristic traditional Chinese medicine
Ligusticum sinense Oliv. cv.
Chaxiong Mss. from Jiangxi Province
*, columnId=1206272756333736276, journalTitle=Chinese Journal of Pharmaceutical Analysis, columnName=Ingredient Analysis, runingTitle=null, highlight=null, articleAbstract=
Objective: To establish a method of thin-layer chromatographic identification,HPLC fingerprints and a method of the content determination of 13 chemical constituents (chlorogenic acid,caffeic acid,ferulic acid,senkyunolide I,senkyunolide H,coniferyl ferulate,senkyunolide A,butylphthalide,sedanolide,Z-ligustralactone,butenylylphthalide,levistilide A,and linoleic acid) in Ligusticum sinense Oliv. cv. Chaxiong Mss. and to provide a basis for the quality control of Ligusticum sinense Oliv. cv. Chaxiong Mss.
Methods: Thin-layer chromatography was used for the qualitative identification of senkyunolide I,scopoletin,ferulic acid,levistilide A and Z-ligustilide in Ligusticum sinense Oliv. cv. Chaxiong Mss. using n-hexane,ethyl acetate and acetic acid (10:5:0.5) as the mobile phase. The separation was carried out on an Acutfex PA-C18 column (250 mm×4.6 mm,5 μm),with gradient elution of 0.1% aqueous phosphoric acid solution and acetonitrile at a flow rate of 1 mL·min-1. The column temperature was 30 ℃,the injection volume was 10 μL,and the detection wavelengths were 210 nm and 285 nm. The fingerprints of 54 batches of Ligusticum sinense Oliv. cv. Chaxiong Mss. were constructed. SPSS and SIMCA software were used for the chemical pattern recognition analysis,and 13 chemical components were determined at the same time.
Results: A thin-layer chromatographic method was established for the identification of senkyunolide I,scopoletin,ferulic acid,levistilide A and Z-ligustilide in Ligusticum sinense Oliv. cv. Chaxiong Mss. The HPLC fingerprints of Ligusticum sinense Oliv. cv. Chaxiong Mss. were established,21 common peaks were found,13 common peaks were identified,and the similarities of all batches of the herbs were above 0.9,except sample S47. The herbs could be roughly divided into four groups according to the collection time and altitude by clustering analysis. OPLS-DA screened out seven differential constituents:peak 17(Z-ligustilide),peak 13 (senkyunolide A),peak 12 (coniferyl ferulate),peak 5 (ferulic acid),peak 6,peak 16 (sedanolide),and peak 2 (chlorogenic acid). A method was established for the determination of chlorogenic acid,caffeic acid,ferulic acid,senkyunolide I,senkyunolide H,coniferyl ferulate,senkyunolide A,butylphthalide,sedanolide,Z-ligustralactone,butenylylphthalide,levistilide A and linoleic acid in Ligusticum sinense Oliv. cv. Chaxiong Mss. with good linearity,precision,stability,reproducibility,and spiked recoveries. And the content ranges of the above-mentioned compounds in the herbs were 0.03-3.80 mg·g-1,0.004-0.055 mg·g-1,0.17-0.82 mg·g-1,0.08-0.57 mg·g-1,0.01-0.19 mg·g-1,0.04-2.51 mg·g-1,1.37-11.64 mg·g-1,0.15-0.58 mg·g-1,0.18-4.22 mg·g-1,2.69-9.53 mg·g-1,0.15-0.59 mg·g-1,0.07-0.62 mg·g-1 and 0.31-6.04 mg·g-1,respectively.
Conclusion: The method of thin-layer chromatography,HPLC fingerprints,and the determination method of the 13 constituents in Ligusticum sinense Oliv. cv. Chaxiong Mss. are simple,accurate and reliable,and can provide a basis for the evaluation of the quality of Ligusticum sinense Oliv. cv. Chaxiong Mss..
, correspAuthors=Can-jian WANG, Guo-song ZHANG, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, authorCompany=null, fund=null, authors=null, authorsList=Tang-xun WANG, Guan-sheng ZHANG, Jian-bo YANG, Yang CHEN, Yu-fang HUANG, Guang-di YANG, Ming-yan XIA, Can-jian WANG, Guo-song ZHANG), CN=ArticleExt(id=1239973087014351139, articleId=1239973083646324902, tenantId=1146029695717560320, journalId=1205117023404326918, language=CN, title=江西特色中药茶芎的质量评价方法研究
*, columnId=1206272756476342615, journalTitle=药物分析杂志, columnName=成分分析, runingTitle=null, highlight=null, articleAbstract=
目的: 建立茶芎的薄层色谱鉴别方法、HPLC指纹图谱以及绿原酸、咖啡酸、阿魏酸、洋川芎内酯I、洋川芎内酯H、阿魏酸松柏酯、洋川芎内酯A、正丁基苯酞、新蛇床内酯、Z-藁本内酯、丁烯基苯酞、欧当归内酯A、亚油酸13个化学成分含量测定方法,为茶芎药材的质量控制提供依据。
方法: 采用薄层色谱法,以正己烷-乙酸乙酯-冰醋酸(10:5:0.5)为展开剂,对茶芎中洋川芎内酯I、东莨菪内酯、阿魏酸、欧当归内酯A、Z-藁本内酯进行鉴别;采用Acutfex PA-C18 (250 mm×4.6 mm,5 μm)色谱柱,以0.1%磷酸水溶液-乙腈为流动相,进行梯度洗脱,体积流量1 mL·min-1,柱温30 ℃,进样量10 μL,检测波长210、285 nm,对54批茶芎药材进行指纹图谱构建;采用SPSS和SIMCA软件进行化学模式识别分析,同时测定13个化学成分的含量。
结果: 建立了茶芎药材中洋川芎内酯I、东莨菪内酯、阿魏酸、欧当归内酯A、Z-藁本内酯的薄层色谱鉴别方法;建立了茶芎的HPLC指纹图谱,标定了21个共有峰,指认出13个共有峰,除S47号药材外,其他批次药材相似度均>0.9;聚类分析后可以按照采集时间和海拔分为4类;OPLS-DA筛选出峰17(Z-藁本内酯)、峰13(洋川芎内酯A)、峰12(阿魏酸松柏酯)、峰5(阿魏酸)、峰6、峰16(新蛇床内酯)、峰2(绿原酸)7个差异性成分;建立了茶芎中绿原酸、咖啡酸、阿魏酸、洋川芎内酯I、洋川芎内酯H、阿魏酸松柏酯、洋川芎内酯A、正丁基苯酞、新蛇床内酯、Z-藁本内酯、丁烯基苯酞、欧当归内酯A、亚油酸的含量测定方法,其线性、精密度、稳定性、重复性、加样回收率均良好,上述各成分在药材中含量范围分别为0.03~3.80、0.004~0.055、0.17~0.82、0.08~0.57、0.01~0.19、0.04~2.51、1.37~11.64、0.15~0.58、0.18~4.22、2.69~9.53、0.15~0.59、0.07~0.62、0.31~6.04 mg·g-1。
结论: 建立的茶芎薄层色谱鉴别、HPLC指纹图谱及13个成分的含量测定方法操作简便,准确可靠,可为茶芎药材质量评价提供依据。
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2.National Engineering Research Center of Chinese Medicine Solid Preparation Manufacturing Technology, Nanchang 330006, China), AuthorCompanyExt(id=1239977431059190215, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, companyId=1239977431046607300, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=
2.中药固体制剂制造技术国家工程研究中心,南昌 330006)]), AuthorCompany(id=1239977431155659214, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, xref=3., ext=[AuthorCompanyExt(id=1239977431164047822, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, companyId=1239977431155659214, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=
3.National Institutes for Food and Drug Control, Beijing 100050, China), AuthorCompanyExt(id=1239977431176630736, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, companyId=1239977431155659214, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=
3.中国食品药品检定研究院,北京 100050)]), AuthorCompany(id=1239977431260516820, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, xref=4., ext=[AuthorCompanyExt(id=1239977431268905429, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, companyId=1239977431260516820, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=
4.Guangxi University of Chinese Medicine, Nanning 530200, China), AuthorCompanyExt(id=1239977431277294039, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, companyId=1239977431260516820, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=
4.广西中医药大学,南宁 530200)])], figs=[ArticleFig(id=1239977440311825089, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, language=EN, label=Fig.1, caption=
Thin-layer chromatograms, figureFileSmall=tzsxE7tAABjQg8ihVMlq4g==, figureFileBig=lnDFgpUO55j72bl6ZlaRIQ==, tableContent=null), ArticleFig(id=1239977440408294085, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, language=CN, label=图1, caption=
薄层色谱图1.洋川芎内酯I对照品(senkyunolide I reference substance) 2.东莨菪内酯对照品(scopoletin reference substance) 3.阿魏酸对照品(ferulic acid reference substance) 4.混合对照品(mixed reference substances) 5.样品(S54)(sample) 6.欧当归内酯A对照品(levistilide A reference substance) 7.Z-藁本内酯对照品(Z-ligustilide reference substance)
, figureFileSmall=tzsxE7tAABjQg8ihVMlq4g==, figureFileBig=lnDFgpUO55j72bl6ZlaRIQ==, tableContent=null), ArticleFig(id=1239977440525734603, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, language=EN, label=Fig.2, caption=
Thin layer chromatograms of different batches of herbs, figureFileSmall=zvQljFypCgOc0hdLmZ8aVg==, figureFileBig=nubnqFiS0OsVAMgzwGEYMA==, tableContent=null), ArticleFig(id=1239977440613814990, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, language=CN, label=图2, caption=
不同批次药材薄层色谱图1.洋川芎内酯I(senkyunolide I) 2.东莨菪内酯(scopoletin) 3.阿魏酸(ferulic acid) 4.欧当归内酯A(levistilide A) 5.Z-藁本内酯(Z-ligustilide)
, figureFileSmall=zvQljFypCgOc0hdLmZ8aVg==, figureFileBig=nubnqFiS0OsVAMgzwGEYMA==, tableContent=null), ArticleFig(id=1239977440710283986, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, language=EN, label=Fig.3, caption=
Overlay HPLC fingerprints and reference fingerprint (R) of 54 batches of Ligusticum sinense Oliv. cv. Chaxiong Mss., figureFileSmall=GdT+Te31wMyYIRAKs0QR+g==, figureFileBig=W8vGnW+GQRRucIqLOYFn6w==, tableContent=null), ArticleFig(id=1239977440794170067, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, language=CN, label=图3, caption=
54批茶芎药材的HPLC叠加指纹图谱及对照指纹图谱(R), figureFileSmall=GdT+Te31wMyYIRAKs0QR+g==, figureFileBig=W8vGnW+GQRRucIqLOYFn6w==, tableContent=null), ArticleFig(id=1239977440911610586, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, language=EN, label=Fig.4, caption=
Dendrogram of hierarchical cluster analysis for 54 batches of Ligusticum sinense Oliv. cv. Chaxiong Mss., figureFileSmall=Nu8KUL6Fsu01JLidqimMug==, figureFileBig=xefjThHPPbvrjwTBIlrJWA==, tableContent=null), ArticleFig(id=1239977441024856798, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, language=CN, label=图4, caption=
54批次茶芎样品的聚类分析树状图, figureFileSmall=Nu8KUL6Fsu01JLidqimMug==, figureFileBig=xefjThHPPbvrjwTBIlrJWA==, tableContent=null), ArticleFig(id=1239977442526417631, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, language=EN, label=Fig.5, caption=
OPLS-DA scores plot of Ligusticum sinense Oliv. cv. Chaxiong Mss., figureFileSmall=TfpBrfReg/ozrqLJNhV6eg==, figureFileBig=mqBYvdUjlGxByDPthu46xA==, tableContent=null), ArticleFig(id=1239977442652246757, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, language=CN, label=图5, caption=
茶芎OPLS-DA得分图1.低海拔(low altitude) 2.中海拔(middle altitude) 3.高海拔(high altitude) 4.非当季茶芎(out-of-season Chaxiong)
, figureFileSmall=TfpBrfReg/ozrqLJNhV6eg==, figureFileBig=mqBYvdUjlGxByDPthu46xA==, tableContent=null), ArticleFig(id=1239977442736132840, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, language=EN, label=Fig.6, caption=
Cross validation plot of Ligusticum sinense Oliv. cv. Chaxiong Mss., figureFileSmall=C31dPQsCOZqNiiOW2r/ZNg==, figureFileBig=hdlsRlnISzy8NCIQzUGuxA==, tableContent=null), ArticleFig(id=1239977442878739183, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, language=CN, label=图6, caption=
茶芎药材交叉验证图, figureFileSmall=C31dPQsCOZqNiiOW2r/ZNg==, figureFileBig=hdlsRlnISzy8NCIQzUGuxA==, tableContent=null), ArticleFig(id=1239977442966819570, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, language=EN, label=Fig.7, caption=
VIP plot of Ligusticum sinense Oliv. cv. Chaxiong Mss., figureFileSmall=+3HtR9k3xut3ceTk3ndxHg==, figureFileBig=6RPN/CtLq6dwv4p8vFuKQA==, tableContent=null), ArticleFig(id=1239977443054899956, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, language=CN, label=图7, caption=
茶芎药材VIP图, figureFileSmall=+3HtR9k3xut3ceTk3ndxHg==, figureFileBig=6RPN/CtLq6dwv4p8vFuKQA==, tableContent=null), ArticleFig(id=1239977443122008825, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, language=EN, label=Fig.8, caption=
HPLC chromatograms of mixed reference substances (A) and sample S54 (B), figureFileSmall=5ncYdknR2jLqsDrTOeShyw==, figureFileBig=wfo4AF1SMNDUhH7/jwWXAg==, tableContent=null), ArticleFig(id=1239977443239449340, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, language=CN, label=图8, caption=
混合对照品(A)和样品S54(B)的HPLC图1.绿原酸(chlorogenic acid) 2.咖啡酸(caffeic acid) 3.阿魏酸(ferulic acid) 4.洋川芎内酯I(senkyunolide I) 5.洋川芎内酯H(senkyunolide H) 6.阿魏酸松柏酯(coniferyl ferulate) 7.洋川芎内酯A(senkyunolide A) 8.正丁基苯酞(butylphthalide) 9.新蛇床内酯(sedanolide) 10. Z-藁本内酯(Z-ligustilide) 11.丁烯基苯酞(butylidenephthalide) 12.欧当归内酯A(levistilide A) 13.亚油酸(linoleic acid)
, figureFileSmall=5ncYdknR2jLqsDrTOeShyw==, figureFileBig=wfo4AF1SMNDUhH7/jwWXAg==, tableContent=null), ArticleFig(id=1239977443327529727, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, language=EN, label=Tab.1, caption=
Information of sample source
, figureFileSmall=null, figureFileBig=null, tableContent=
样品编号 (sample No.) | 地点 (habitat) | 时间 (time) | 经度 (longitude) | 纬度 (latitude) | 海拔 (altitude)/m |
|---|
| S1 | 德安县邹桥乡付山村(Fushan Village,Zouqiao Township,De′an County) | 2023.7 | 115°31′11″ | 29°27′38″ | 306.1 |
| S2 | 德安县邹桥乡付山村(Fushan Village,Zouqiao Township,De′an County) | 2023.7 | 115°31′10″ | 29°27′36″ | 301.0 |
| S3 | 德安县邹桥乡付山村(Fushan Village,Zouqiao Township,De′an County) | 2023.7 | 115°31′10″ | 29°27′36″ | 300.8 |
| S4 | 德安县邹桥乡付山村(Fushan Village,Zouqiao Township,De′an County) | 2023.7 | 115°31′8″ | 29°27′36″ | 302.3 |
| S5 | 武宁县鲁溪镇夏宕村(Xiadang Village,Luxi Township,Wuning County) | 2023.7 | 115°12′24″ | 29°28′18″ | 370.1 |
| S6 | 武宁县鲁溪镇夏宕村(Xiadang Village,Luxi Township,Wuning County) | 2023.7 | 115°12′23″ | 29°28′18″ | 369.7 |
| S7 | 武宁县鲁溪镇夏宕村(Xiadang Village,Luxi Township,Wuning County) | 2023.7 | 115°12′23″ | 29°28′18″ | 369.8 |
| S8 | 武宁县鲁溪镇夏宕村(Xiadang Village,Luxi Township,Wuning County) | 2023.7 | 115°12′24″ | 29°28′18″ | 369.5 |
| S9 | 武宁县鲁溪镇夏宕村(Xiadang Village,Luxi Township,Wuning County) | 2023.7 | 115°12′5″ | 29°28′28″ | 404.4 |
| S10 | 武宁县鲁溪镇夏宕村(Xiadang Village,Luxi Township,Wuning County) | 2023.7 | 115°12′3″ | 29°28′29″ | 406.7 |
| S11 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°11′19″ | 29°28′47″ | 473.65 |
| S12 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°11′16″ | 29°28′46″ | 484.7 |
| S13 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°11′10″ | 29°28′53″ | 488.7 |
| S14 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°11′19″ | 29°28′51″ | 487.4 |
| S15 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°11′17″ | 29°28′48″ | 480.8 |
| S16 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°11′21″ | 29°28′46″ | 473.2 |
| S17 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°11′19″ | 29°28′47″ | 468.4 |
| S18 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°11′18″ | 29°28′47″ | 481.6 |
| S19 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°11′15″ | 29°28′46″ | 490.4 |
| S20 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°10′45″ | 29°29′0″ | 481.4 |
| S21 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°10′45″ | 29°29′0″ | 473.4 |
| S22 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°10′45″ | 29°29′0″ | 462.3 |
| S23 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°10′45″ | 29°29′0″ | 479.5 |
| S24 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°10′45″ | 29°29′1″ | 473.2 |
| S25 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°10′40″ | 29°29′1″ | 478.6 |
| S26 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°10′41″ | 29°29′0″ | 473.5 |
| S27 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°10′41″ | 29°29′0″ | 474.7 |
| S28 | 瑞昌市乐园乡张坊村(Zhangfang Village,Leyuan Township,Ruichang City) | 2023.7 | 115°7′35″ | 29°35′10″ | 478.0 |
| S29 | 瑞昌市乐园乡张坊村(Zhangfang Village,Leyuan Township,Ruichang City) | 2023.7 | 115°10′41″ | 29°30′48″ | 470.8 |
| S30 | 瑞昌市乐园乡张坊村(Zhangfang Village,Leyuan Township,Ruichang City) | 2023.7 | 115°10′40″ | 29°30′49″ | 470.6 |
| S31 | 瑞昌市南义镇和平村(Heping Village,Nanyi Township,Ruichang City) | 2023.7 | 115°18′26″ | 29°30′19″ | 456.3 |
| S32 | 瑞昌市南义镇和平村(Heping Village,Nanyi Township,Ruichang City) | 2023.7 | 115°18′26″ | 29°30′17″ | 471.6 |
| S33 | 瑞昌市南义镇和平村(Heping Village,Nanyi Township,Ruichang City) | 2023.7 | 115°18′34″ | 29°30′17″ | 479.6 |
| S34 | 瑞昌市南义镇和平村(Heping Village,Nanyi Township,Ruichang City) | 2023.7 | 115°18′35″ | 29°30′21″ | 485.4 |
| S35 | 瑞昌市南义镇杨塅村(Yangduan Village,Nanyi Township,Ruichang City) | 2023.7 | 115°22′9″ | 29°31′53″ | 498.1 |
| S36 | 瑞昌市南义镇杨塅村(Yangduan Village,Nanyi Township,Ruichang City) | 2023.7 | 115°22′7″ | 29°31′53″ | 501.1 |
| S37 | 瑞昌市南义镇杨塅村(Yangduan Village,Nanyi Township,Ruichang City) | 2023.7 | 115°22′10″ | 29°31′52″ | 498.4 |
| S38 | 瑞昌市南义镇杨塅村(Yangduan Village,Nanyi Township,Ruichang City) | 2023.7 | 115°22′14″ | 29°31′58″ | 493.0 |
| S39 | 武宁县鲁溪镇夏宕村(Xiadang Village,Luxi Township,Wuning County) | 2023.6 | 115°12′3″ | 29°28′29″ | 406.7 |
| S40 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.6 | 115°11′19″ | 29°28′47″ | 473.65 |
| S41 | 瑞昌市南义镇和平村(Heping Village,Nanyi Township,Ruichang City) | 2023.6 | 115°18′26″ | 29°30′19″ | 456.3 |
| S42 | 瑞昌市乐园乡张坊村(Zhangfang Village,Leyuan Township,Ruichang City) | 2023.6 | 115°10′41″ | 29°30′48″ | 470.8 |
| S43 | 德安县邹桥乡付山村(Fushan Village,Zouqiao Township,De′an County) | 2023.6 | 115°31′11″ | 29°27′38″ | 306.1 |
| S44 | 德安县邹桥乡付山村(Fushan Village,Zouqiao Township,De′an County) | 2023.6 | 115°31′8″ | 29°27′36″ | 302.3 |
| S45 | 武宁县鲁溪镇夏宕村(Xiadang Village,Luxi Township,Wuning County) | 2023.5 | 115°12′3″ | 29°28′29″ | 406.7 |
| S46 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.5 | 115°11′19″ | 29°28′47″ | 473.65 |
| S47 | 瑞昌市乐园乡张坊村(Zhangfang Village,Leyuan Township,Ruichang City) | 2023.5 | 115°10′41″ | 29°30′48″ | 470.8 |
| S48 | 德安县邹桥乡付山村(Fushan Village,Zouqiao Township,De′an County) | 2023.5 | 115°31′8″ | 29°27′36″ | 302.3 |
| S49 | 武宁县鲁溪镇夏宕村(Xiadang Village,Luxi Township,Wuning County) | 2022.7 | - | - | - |
| S50 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2022.7 | - | - | - |
| S51 | 德安县邹桥乡付山村(Fushan Village,Zouqiao Township,De′an County) | 2022.7 | - | - | - |
| S52 | 瑞昌市(Ruichang City) | 2022.7 | - | - | - |
| S53 | 瑞昌市和平乡(Heping Township,Ruichang City) | 2021.7 | - | - | - |
| S54 | 江西江中中药饮片有限公司(Jiangxi Jiangzhong Prepared Slices of Chinese Crude Drugs Co.) | 2022.5 | - | - | - |
), ArticleFig(id=1239977443453358850, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, language=CN, label=表1, caption=
样品来源信息
, figureFileSmall=null, figureFileBig=null, tableContent=
样品编号 (sample No.) | 地点 (habitat) | 时间 (time) | 经度 (longitude) | 纬度 (latitude) | 海拔 (altitude)/m |
|---|
| S1 | 德安县邹桥乡付山村(Fushan Village,Zouqiao Township,De′an County) | 2023.7 | 115°31′11″ | 29°27′38″ | 306.1 |
| S2 | 德安县邹桥乡付山村(Fushan Village,Zouqiao Township,De′an County) | 2023.7 | 115°31′10″ | 29°27′36″ | 301.0 |
| S3 | 德安县邹桥乡付山村(Fushan Village,Zouqiao Township,De′an County) | 2023.7 | 115°31′10″ | 29°27′36″ | 300.8 |
| S4 | 德安县邹桥乡付山村(Fushan Village,Zouqiao Township,De′an County) | 2023.7 | 115°31′8″ | 29°27′36″ | 302.3 |
| S5 | 武宁县鲁溪镇夏宕村(Xiadang Village,Luxi Township,Wuning County) | 2023.7 | 115°12′24″ | 29°28′18″ | 370.1 |
| S6 | 武宁县鲁溪镇夏宕村(Xiadang Village,Luxi Township,Wuning County) | 2023.7 | 115°12′23″ | 29°28′18″ | 369.7 |
| S7 | 武宁县鲁溪镇夏宕村(Xiadang Village,Luxi Township,Wuning County) | 2023.7 | 115°12′23″ | 29°28′18″ | 369.8 |
| S8 | 武宁县鲁溪镇夏宕村(Xiadang Village,Luxi Township,Wuning County) | 2023.7 | 115°12′24″ | 29°28′18″ | 369.5 |
| S9 | 武宁县鲁溪镇夏宕村(Xiadang Village,Luxi Township,Wuning County) | 2023.7 | 115°12′5″ | 29°28′28″ | 404.4 |
| S10 | 武宁县鲁溪镇夏宕村(Xiadang Village,Luxi Township,Wuning County) | 2023.7 | 115°12′3″ | 29°28′29″ | 406.7 |
| S11 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°11′19″ | 29°28′47″ | 473.65 |
| S12 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°11′16″ | 29°28′46″ | 484.7 |
| S13 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°11′10″ | 29°28′53″ | 488.7 |
| S14 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°11′19″ | 29°28′51″ | 487.4 |
| S15 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°11′17″ | 29°28′48″ | 480.8 |
| S16 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°11′21″ | 29°28′46″ | 473.2 |
| S17 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°11′19″ | 29°28′47″ | 468.4 |
| S18 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°11′18″ | 29°28′47″ | 481.6 |
| S19 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°11′15″ | 29°28′46″ | 490.4 |
| S20 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°10′45″ | 29°29′0″ | 481.4 |
| S21 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°10′45″ | 29°29′0″ | 473.4 |
| S22 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°10′45″ | 29°29′0″ | 462.3 |
| S23 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°10′45″ | 29°29′0″ | 479.5 |
| S24 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°10′45″ | 29°29′1″ | 473.2 |
| S25 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°10′40″ | 29°29′1″ | 478.6 |
| S26 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°10′41″ | 29°29′0″ | 473.5 |
| S27 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.7 | 115°10′41″ | 29°29′0″ | 474.7 |
| S28 | 瑞昌市乐园乡张坊村(Zhangfang Village,Leyuan Township,Ruichang City) | 2023.7 | 115°7′35″ | 29°35′10″ | 478.0 |
| S29 | 瑞昌市乐园乡张坊村(Zhangfang Village,Leyuan Township,Ruichang City) | 2023.7 | 115°10′41″ | 29°30′48″ | 470.8 |
| S30 | 瑞昌市乐园乡张坊村(Zhangfang Village,Leyuan Township,Ruichang City) | 2023.7 | 115°10′40″ | 29°30′49″ | 470.6 |
| S31 | 瑞昌市南义镇和平村(Heping Village,Nanyi Township,Ruichang City) | 2023.7 | 115°18′26″ | 29°30′19″ | 456.3 |
| S32 | 瑞昌市南义镇和平村(Heping Village,Nanyi Township,Ruichang City) | 2023.7 | 115°18′26″ | 29°30′17″ | 471.6 |
| S33 | 瑞昌市南义镇和平村(Heping Village,Nanyi Township,Ruichang City) | 2023.7 | 115°18′34″ | 29°30′17″ | 479.6 |
| S34 | 瑞昌市南义镇和平村(Heping Village,Nanyi Township,Ruichang City) | 2023.7 | 115°18′35″ | 29°30′21″ | 485.4 |
| S35 | 瑞昌市南义镇杨塅村(Yangduan Village,Nanyi Township,Ruichang City) | 2023.7 | 115°22′9″ | 29°31′53″ | 498.1 |
| S36 | 瑞昌市南义镇杨塅村(Yangduan Village,Nanyi Township,Ruichang City) | 2023.7 | 115°22′7″ | 29°31′53″ | 501.1 |
| S37 | 瑞昌市南义镇杨塅村(Yangduan Village,Nanyi Township,Ruichang City) | 2023.7 | 115°22′10″ | 29°31′52″ | 498.4 |
| S38 | 瑞昌市南义镇杨塅村(Yangduan Village,Nanyi Township,Ruichang City) | 2023.7 | 115°22′14″ | 29°31′58″ | 493.0 |
| S39 | 武宁县鲁溪镇夏宕村(Xiadang Village,Luxi Township,Wuning County) | 2023.6 | 115°12′3″ | 29°28′29″ | 406.7 |
| S40 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.6 | 115°11′19″ | 29°28′47″ | 473.65 |
| S41 | 瑞昌市南义镇和平村(Heping Village,Nanyi Township,Ruichang City) | 2023.6 | 115°18′26″ | 29°30′19″ | 456.3 |
| S42 | 瑞昌市乐园乡张坊村(Zhangfang Village,Leyuan Township,Ruichang City) | 2023.6 | 115°10′41″ | 29°30′48″ | 470.8 |
| S43 | 德安县邹桥乡付山村(Fushan Village,Zouqiao Township,De′an County) | 2023.6 | 115°31′11″ | 29°27′38″ | 306.1 |
| S44 | 德安县邹桥乡付山村(Fushan Village,Zouqiao Township,De′an County) | 2023.6 | 115°31′8″ | 29°27′36″ | 302.3 |
| S45 | 武宁县鲁溪镇夏宕村(Xiadang Village,Luxi Township,Wuning County) | 2023.5 | 115°12′3″ | 29°28′29″ | 406.7 |
| S46 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2023.5 | 115°11′19″ | 29°28′47″ | 473.65 |
| S47 | 瑞昌市乐园乡张坊村(Zhangfang Village,Leyuan Township,Ruichang City) | 2023.5 | 115°10′41″ | 29°30′48″ | 470.8 |
| S48 | 德安县邹桥乡付山村(Fushan Village,Zouqiao Township,De′an County) | 2023.5 | 115°31′8″ | 29°27′36″ | 302.3 |
| S49 | 武宁县鲁溪镇夏宕村(Xiadang Village,Luxi Township,Wuning County) | 2022.7 | - | - | - |
| S50 | 武宁县鲁溪镇北屏村(Beiping Village,Luxi Township,Wuning County) | 2022.7 | - | - | - |
| S51 | 德安县邹桥乡付山村(Fushan Village,Zouqiao Township,De′an County) | 2022.7 | - | - | - |
| S52 | 瑞昌市(Ruichang City) | 2022.7 | - | - | - |
| S53 | 瑞昌市和平乡(Heping Township,Ruichang City) | 2021.7 | - | - | - |
| S54 | 江西江中中药饮片有限公司(Jiangxi Jiangzhong Prepared Slices of Chinese Crude Drugs Co.) | 2022.5 | - | - | - |
), ArticleFig(id=1239977443579187974, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, language=EN, label=Tab.2, caption=
Characteristic values and variance contribution rates of principal components
, figureFileSmall=null, figureFileBig=null, tableContent=
主成分 (principal component) | 特征值 (eigen value) | 方差贡献率 (variance contribution rate)/% | 累积方差贡献率 (cumulative variance contribution rate)/% |
|---|
| 1 | 7.404 | 35.257 | 35.257 |
| 2 | 5.707 | 27.176 | 62.433 |
| 3 | 2.523 | 12.015 | 74.449 |
| 4 | 1.68 | 8.001 | 82.449 |
), ArticleFig(id=1239977443692434185, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, language=CN, label=表2, caption=
主成分特征值及方差贡献率
, figureFileSmall=null, figureFileBig=null, tableContent=
主成分 (principal component) | 特征值 (eigen value) | 方差贡献率 (variance contribution rate)/% | 累积方差贡献率 (cumulative variance contribution rate)/% |
|---|
| 1 | 7.404 | 35.257 | 35.257 |
| 2 | 5.707 | 27.176 | 62.433 |
| 3 | 2.523 | 12.015 | 74.449 |
| 4 | 1.68 | 8.001 | 82.449 |
), ArticleFig(id=1239977443784708878, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, language=EN, label=Tab.3, caption=
Matrix of principal components
, figureFileSmall=null, figureFileBig=null, tableContent=
峰号 (peak No.) | 主成分(principal component) |
|---|
| 1 | 2 | 3 | 4 |
|---|
| 15 | 0.892 | -0.142 | -0.106 | 0.168 |
| 7 | 0.819 | 0.476 | -0.054 | -0.188 |
| 19 | 0.806 | 0.245 | 0.209 | 0.069 |
| 6 | 0.798 | 0.502 | -0.042 | -0.19 |
| 13 | 0.793 | -0.02 | -0.189 | 0.427 |
| 11 | 0.779 | 0.378 | 0.378 | 0.009 |
| 16 | 0.767 | 0.144 | -0.285 | 0.158 |
| 17 | 0.767 | -0.196 | -0.009 | 0.416 |
| 2 | 0.749 | 0.534 | -0.038 | -0.268 |
| 9 | -0.246 | 0.907 | 0.177 | 0.143 |
| 4 | -0.449 | 0.833 | 0.179 | 0.155 |
| 8 | -0.514 | 0.78 | 0.203 | 0.241 |
| 20 | -0.025 | 0.774 | 0.335 | 0.07 |
| 3 | 0.271 | 0.76 | 0.054 | -0.172 |
| 21 | -0.034 | 0.651 | 0.066 | -0.436 |
| 18 | -0.611 | 0.649 | 0.094 | 0.359 |
| 5 | 0.408 | -0.379 | 0.759 | 0.122 |
| 12 | 0.342 | 0.278 | -0.701 | 0.349 |
| 10 | 0.503 | -0.341 | 0.695 | 0.221 |
| 1 | -0.249 | -0.271 | 0.548 | 0.339 |
| 14 | -0.328 | 0.323 | -0.343 | 0.605 |
), ArticleFig(id=1239977443906343699, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, language=CN, label=表3, caption=
主成分矩阵
, figureFileSmall=null, figureFileBig=null, tableContent=
峰号 (peak No.) | 主成分(principal component) |
|---|
| 1 | 2 | 3 | 4 |
|---|
| 15 | 0.892 | -0.142 | -0.106 | 0.168 |
| 7 | 0.819 | 0.476 | -0.054 | -0.188 |
| 19 | 0.806 | 0.245 | 0.209 | 0.069 |
| 6 | 0.798 | 0.502 | -0.042 | -0.19 |
| 13 | 0.793 | -0.02 | -0.189 | 0.427 |
| 11 | 0.779 | 0.378 | 0.378 | 0.009 |
| 16 | 0.767 | 0.144 | -0.285 | 0.158 |
| 17 | 0.767 | -0.196 | -0.009 | 0.416 |
| 2 | 0.749 | 0.534 | -0.038 | -0.268 |
| 9 | -0.246 | 0.907 | 0.177 | 0.143 |
| 4 | -0.449 | 0.833 | 0.179 | 0.155 |
| 8 | -0.514 | 0.78 | 0.203 | 0.241 |
| 20 | -0.025 | 0.774 | 0.335 | 0.07 |
| 3 | 0.271 | 0.76 | 0.054 | -0.172 |
| 21 | -0.034 | 0.651 | 0.066 | -0.436 |
| 18 | -0.611 | 0.649 | 0.094 | 0.359 |
| 5 | 0.408 | -0.379 | 0.759 | 0.122 |
| 12 | 0.342 | 0.278 | -0.701 | 0.349 |
| 10 | 0.503 | -0.341 | 0.695 | 0.221 |
| 1 | -0.249 | -0.271 | 0.548 | 0.339 |
| 14 | -0.328 | 0.323 | -0.343 | 0.605 |
), ArticleFig(id=1239977444132836120, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, language=EN, label=Tab.4, caption=
Linear relationship of 13 components
, figureFileSmall=null, figureFileBig=null, tableContent=
| 成分(component) | 回归方程(regression equation) | r | 线性范围(linear range)/(μg·mL-1) |
|---|
| 绿原酸(chlorogenic acid) | Y=12 683X+620.84 | 0.999 5 | 0.13~3.15 |
| 咖啡酸(caffeic acid) | Y=35 086X+245.27 | 0.999 5 | 0.085~2.13 |
| 阿魏酸(ferulic aci) | Y=40 560X-13 291 | 0.999 9 | 1.03~25.80 |
| 洋川芎内酯I(senkyunolide I) | Y=39 237X-7 954.9 | 0.999 9 | 0.76~19.03 |
| 洋川芎内酯H(senkyunolide H) | Y=21 411X-1 290.2 | 1.000 | 0.28~7.04 |
| 阿魏酸松柏酯(coniferyl ferulate) | Y=21 879X-13 224 | 1.000 | 3.14~78.38 |
| 洋川芎内酯A(senkyunolide A) | Y=8 655.9X-31 619 | 1.000 | 16.23~405.83 |
| 正丁基苯酞(butylphthalide) | Y=31 761X-13 289 | 0.999 9 | 1.31~32.69 |
| 新蛇床内酯(sedanolide) | Y=20 053X-53 564 | 0.999 9 | 10.11~252.75 |
| Z-藁本内酯(Z-ligustilide) | Y=20 151X-71 949 | 1.000 | 16.84~421.12 |
| 丁烯基苯酞(butylidenephthalide) | Y=24 892X-6 958.6 | 0.999 9 | 1.03~25.69 |
| 欧当归内酯A(levistilide A) | Y=18 815X-4 732.9 | 0.999 9 | 0.69~17.27 |
| 亚油酸(linoleic acid) | Y=4 951X+17 350 | 0.999 9 | 7.54~188.42 |
), ArticleFig(id=1239977444262859547, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, language=CN, label=表4, caption=
13个成分的线性关系
, figureFileSmall=null, figureFileBig=null, tableContent=
| 成分(component) | 回归方程(regression equation) | r | 线性范围(linear range)/(μg·mL-1) |
|---|
| 绿原酸(chlorogenic acid) | Y=12 683X+620.84 | 0.999 5 | 0.13~3.15 |
| 咖啡酸(caffeic acid) | Y=35 086X+245.27 | 0.999 5 | 0.085~2.13 |
| 阿魏酸(ferulic aci) | Y=40 560X-13 291 | 0.999 9 | 1.03~25.80 |
| 洋川芎内酯I(senkyunolide I) | Y=39 237X-7 954.9 | 0.999 9 | 0.76~19.03 |
| 洋川芎内酯H(senkyunolide H) | Y=21 411X-1 290.2 | 1.000 | 0.28~7.04 |
| 阿魏酸松柏酯(coniferyl ferulate) | Y=21 879X-13 224 | 1.000 | 3.14~78.38 |
| 洋川芎内酯A(senkyunolide A) | Y=8 655.9X-31 619 | 1.000 | 16.23~405.83 |
| 正丁基苯酞(butylphthalide) | Y=31 761X-13 289 | 0.999 9 | 1.31~32.69 |
| 新蛇床内酯(sedanolide) | Y=20 053X-53 564 | 0.999 9 | 10.11~252.75 |
| Z-藁本内酯(Z-ligustilide) | Y=20 151X-71 949 | 1.000 | 16.84~421.12 |
| 丁烯基苯酞(butylidenephthalide) | Y=24 892X-6 958.6 | 0.999 9 | 1.03~25.69 |
| 欧当归内酯A(levistilide A) | Y=18 815X-4 732.9 | 0.999 9 | 0.69~17.27 |
| 亚油酸(linoleic acid) | Y=4 951X+17 350 | 0.999 9 | 7.54~188.42 |
), ArticleFig(id=1239977444346745630, tenantId=1146029695717560320, journalId=1205117023404326918, articleId=1239973083646324902, language=EN, label=Tab.5, caption=
Contents of 13 components in 54 batches of Ligusticum sinense Oliv. cv. Chaxiong Mss.
, figureFileSmall=null, figureFileBig=null, tableContent=
| 编号(No.) | 含量(content)/(mg·g-1) |
|---|
绿原酸 (chlorogenic acid) | 咖啡酸 (caffeic acid) | 阿魏酸 (ferulic acid) | 洋川芎内酯I (senkyunolide I) | 洋川芎内酯H (senkyunolide H) | 阿魏酸松柏酯 (coniferyl ferulate) | 洋川芎内酯A (senkyunolide A) | 正丁基苯酞 (butylph-thalide) | 新蛇床内酯 (sedanolide) | Z-藁本内酯 (Z-ligus-tilide) | 丁烯基苯酞 (butylidene-phthalide) | 欧当归内酯A (levistilide A) | 亚油酸 (linoleic acid) |
|---|
| S1 | 0.29 | 0.004 | 1.62 | 0.09 | 0.03 | 0.92 | 7.65 | 0.19 | 2.20 | 9.44 | 0.20 | 0.15 | 0.99 |
| S2 | 0.29 | 0.009 | 1.29 | 0.11 | 0.04 | 0.47 | 7.26 | 0.20 | 1.64 | 8.81 | 0.23 | 0.14 | 0.85 |
| S3 | 0.12 | 0.005 | 1.41 | 0.13 | 0.05 | 0.63 | 7.39 | 0.24 | 1.69 | 8.52 | 0.24 | 0.14 | 0.94 |
| S4 | 0.10 | 0.008 | 0.85 | 0.13 | 0.04 | 0.18 | 5.33 | 0.18 | 1.67 | 7.20 | 0.23 | 0.13 | 0.87 |
| S5 | 0.21 | 0.009 | 0.88 | 0.10 | 0.03 | 0.17 | 6.79 | 0.18 | 3.21 | 7.17 | 0.19 | 0.10 | 0.71 |
| S6 | 0.23 | 0.014 | 0.80 | 0.10 | 0.03 | 0.08 | 7.03 | 0.20 | 3.18 | 6.97 | 0.19 | 0.09 | 0.86 |
| S7 | 0.09 | 0.014 | 0.85 | 0.13 | 0.04 | 0.16 | 6.20 | 0.20 | 2.46 | 7.49 | 0.25 | 0.12 | 0.59 |
| S8 | 0.11 | 0.009 | 0.52 | 0.08 | 0.03 | 0.08 | 5.25 | 0.15 | 3.02 | 4.96 | 0.15 | 0.07 | 0.31 |
| S9 | 0.07 | 0.011 | 1.01 | 0.14 | 0.05 | 0.67 | 5.42 | 0.24 | 2.28 | 5.18 | 0.24 | 0.09 | 2.62 |
| S10 | 0.14 | 0.009 | 1.82 | 0.14 | 0.05 | 1.50 | 7.70 | 0.24 | 3.12 | 7.21 | 0.23 | 0.11 | 2.31 |
| S11 | 0.08 | 0.015 | 1.71 | 0.18 | 0.06 | 1.41 | 6.88 | 0.35 | 1.59 | 6.44 | 0.31 | 0.11 | 1.21 |
| S12 | 0.28 | 0.017 | 1.40 | 0.11 | 0.04 | 1.05 | 6.04 | 0.23 | 2.55 | 6.13 | 0.26 | 0.10 | 0.88 |
| S13 | 0.04 | 0.020 | 1.52 | 0.17 | 0.05 | 1.27 | 7.67 | 0.37 | 2.92 | 5.77 | 0.31 | 0.08 | 0.86 |
| S14 | 0.04 | 0.005 | 0.52 | 0.20 | 0.07 | 0.14 | 4.23 | 0.35 | 1.26 | 4.62 | 0.28 | 0.07 | 5.10 |
| S15 | 0.07 | 0.013 | 1.22 | 0.17 | 0.06 | 0.70 | 5.92 | 0.34 | 1.57 | 5.86 | 0.29 | 0.10 | 1.49 |
| S16 | 0.11 | 0.013 | 1.65 | 0.14 | 0.05 | 1.35 | 6.51 | 0.32 | 1.74 | 6.37 | 0.27 | 0.10 | 1.22 |
| S17 | 0.10 | 0.010 | 1.34 | 0.19 | 0.06 | 1.00 | 5.10 | 0.31 | 1.52 | 6.03 | 0.31 | 0.11 | 1.39 |
| S18 | 0.35 | 0.019 | 1.31 | 0.10 | 0.04 | 0.95 | 4.17 | 0.25 | 1.75 | 6.59 | 0.26 | 0.13 | 1.33 |
| S19 | 0.09 | 0.021 | 1.58 | 0.18 | 0.06 | 1.33 | 5.30 | 0.31 | 2.08 | 6.85 | 0.31 | 0.13 | 0.93 |
| S20 | 0.10 | 0.011 | 1.76 | 0.16 | 0.05 | 1.31 | 8.27 | 0.33 | 2.55 | 7.48 | 0.27 | 0.12 | 1.03 |
| S21 | 0.23 | 0.012 | 2.06 | 0.13 | 0.04 | 1.59 | 9.07 | 0.25 | 2.76 | 8.27 | 0.24 | 0.14 | 1.10 |
| S22 | 0.15 | 0.025 | 2.01 | 0.17 | 0.05 | 1.55 | 8.67 | 0.27 | 1.89 | 7.89 | 0.27 | 0.15 | 1.16 |
| S23 | 0.26 | 0.027 | 2.26 | 0.15 | 0.05 | 1.92 | 8.53 | 0.27 | 3.46 | 8.31 | 0.27 | 0.16 | 1.22 |
| S24 | 0.19 | 0.008 | 1.02 | 0.12 | 0.04 | 0.53 | 5.76 | 0.23 | 1.61 | 6.01 | 0.23 | 0.09 | 4.71 |
| S25 | 0.11 | 0.020 | 1.89 | 0.18 | 0.06 | 1.63 | 5.51 | 0.21 | 1.79 | 7.26 | 0.28 | 0.15 | 1.17 |
| S26 | 0.08 | 0.020 | 1.91 | 0.16 | 0.05 | 1.60 | 6.94 | 0.25 | 2.23 | 6.65 | 0.25 | 0.12 | 0.85 |
| S27 | 0.31 | 0.009 | 1.35 | 0.08 | 0.03 | 1.01 | 5.65 | 0.17 | 2.48 | 6.03 | 0.18 | 0.10 | 1.02 |
| S28 | 0.13 | 0.011 | 1.77 | 0.16 | 0.05 | 1.51 | 6.57 | 0.24 | 2.55 | 7.14 | 0.27 | 0.14 | 1.06 |
| S29 | 0.10 | 0.012 | 1.65 | 0.18 | 0.06 | 1.40 | 6.75 | 0.48 | 2.57 | 7.08 | 0.28 | 0.13 | 1.32 |
| S30 | 0.13 | 0.013 | 2.03 | 0.20 | 0.07 | 1.76 | 7.63 | 0.48 | 3.58 | 8.38 | 0.33 | 0.15 | 1.53 |
| S31 | 0.06 | 0.009 | 1.60 | 0.16 | 0.05 | 1.33 | 7.05 | 0.50 | 2.27 | 5.53 | 0.25 | 0.08 | 1.44 |
| S32 | 0.06 | 0.006 | 1.67 | 0.17 | 0.06 | 1.37 | 6.69 | 0.51 | 2.63 | 6.01 | 0.29 | 0.09 | 1.40 |
| S33 | 0.04 | 0.015 | 1.56 | 0.21 | 0.07 | 1.22 | 6.33 | 0.47 | 3.38 | 7.18 | 0.33 | 0.12 | 1.60 |
| S34 | 0.05 | 0.011 | 1.34 | 0.17 | 0.05 | 0.86 | 7.33 | 0.49 | 2.78 | 6.54 | 0.30 | 0.09 | 1.22 |
| S35 | 0.08 | 0.008 | 1.68 | 0.17 | 0.06 | 1.40 | 4.23 | 0.40 | 1.87 | 7.39 | 0.35 | 0.12 | 1.54 |
| S36 | 0.05 | 0.020 | 1.52 | 0.25 | 0.08 | 1.21 | 4.05 | 0.25 | 1.64 | 7.23 | 0.42 | 0.17 | 3.02 |
| S37 | 0.09 | 0.011 | 2.26 | 0.18 | 0.04 | 1.89 | 6.91 | 0.27 | 2.67 | 8.82 | 0.35 | 0.15 | 2.31 |
| S38 | 0.07 | 0.010 | 0.74 | 0.16 | 0.06 | 0.35 | 3.61 | 0.23 | 1.58 | 4.52 | 0.29 | 0.08 | 5.55 |
| S39 | 0.65 | 0.010 | 1.67 | 0.23 | 0.08 | 0.04 | 5.77 | 0.34 | 1.71 | 5.87 | 0.35 | 0.14 | 1.52 |
| S40 | 0.04 | 0.017 | 1.41 | 0.29 | 0.09 | 0.87 | 8.24 | 0.45 | 2.23 | 6.19 | 0.41 | 0.11 | 0.94 |
| S41 | 0.04 | 0.014 | 0.96 | 0.37 | 0.12 | 1.58 | 5.79 | 0.50 | 2.00 | 5.17 | 0.49 | 0.10 | 1.21 |
| S42 | 0.03 | 0.013 | 0.98 | 0.29 | 0.10 | 1.61 | 5.57 | 0.35 | 2.59 | 6.02 | 0.44 | 0.11 | 0.85 |
| S43 | 0.29 | 0.007 | 1.30 | 0.25 | 0.09 | 1.05 | 4.64 | 0.31 | 1.49 | 4.87 | 0.36 | 0.11 | 1.16 |
| S44 | 0.04 | 0.015 | 1.18 | 0.43 | 0.13 | 2.51 | 5.88 | 0.58 | 1.44 | 4.62 | 0.49 | 0.12 | 2.85 |
| S45 | 2.49 | 0.033 | 0.41 | 0.14 | 0.06 | 0.60 | 11.64 | 0.30 | 0.18 | 8.58 | 0.21 | 0.17 | 3.49 |
| S46 | 0.41 | 0.023 | 1.05 | 0.22 | 0.08 | 0.95 | 6.43 | 0.47 | 3.23 | 5.03 | 0.36 | 0.10 | 1.29 |
| S47 | 2.00 | 0.028 | 1.77 | 0.10 | 0.05 | 0.30 | 6.68 | 0.20 | 3.20 | 7.78 | 0.17 | 0.18 | 1.87 |
| S48 | 3.80 | 0.038 | 2.18 | 0.12 | 0.05 | 1.09 | 10.79 | 0.23 | 4.22 | 9.53 | 0.20 | 0.22 | 3.17 |
| S49 | 0.47 | 0.016 | 1.44 | 0.29 | 0.10 | 0.66 | 5.08 | 0.27 | 2.97 | 6.60 | 0.34 | 0.35 | 2.89 |
| S50 | 0.40 | 0.015 | 3.01 | 0.31 | 0.10 | 0.76 | 9.29 | 0.45 | 3.11 | 9.28 | 0.43 | 0.44 | 2.51 |
| S51 | 0.29 | 0.007 | 1.30 | 0.25 | 0.09 | 1.08 | 4.64 | 0.31 | 1.49 | 4.87 | 0.36 | 0.11 | 1.16 |
| S52 | 0.04 | 0.015 | 1.18 | 0.43 | 0.13 | 1.01 | 5.88 | 0.58 | 1.44 | 4.62 | 0.49 | 0.12 | 2.85 |
| S53 | 0.65 | 0.046 | 0.86 | 0.11 | 0.15 | 1.46 | 1.46 | 0.22 | 1.85 | 3.78 | 0.49 | 0.59 | 3.65 |
| S54 | 0.05 | 0.038 | 1.36 | 0.27 | 0.08 | 1.07 | 5.13 | 0.32 | 1.76 | 5.25 | 0.34 | 0.26 | 1.59 |
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54批茶芎药材中13个成分的含量
, figureFileSmall=null, figureFileBig=null, tableContent=
| 编号(No.) | 含量(content)/(mg·g-1) |
|---|
绿原酸 (chlorogenic acid) | 咖啡酸 (caffeic acid) | 阿魏酸 (ferulic acid) | 洋川芎内酯I (senkyunolide I) | 洋川芎内酯H (senkyunolide H) | 阿魏酸松柏酯 (coniferyl ferulate) | 洋川芎内酯A (senkyunolide A) | 正丁基苯酞 (butylph-thalide) | 新蛇床内酯 (sedanolide) | Z-藁本内酯 (Z-ligus-tilide) | 丁烯基苯酞 (butylidene-phthalide) | 欧当归内酯A (levistilide A) | 亚油酸 (linoleic acid) |
|---|
| S1 | 0.29 | 0.004 | 1.62 | 0.09 | 0.03 | 0.92 | 7.65 | 0.19 | 2.20 | 9.44 | 0.20 | 0.15 | 0.99 |
| S2 | 0.29 | 0.009 | 1.29 | 0.11 | 0.04 | 0.47 | 7.26 | 0.20 | 1.64 | 8.81 | 0.23 | 0.14 | 0.85 |
| S3 | 0.12 | 0.005 | 1.41 | 0.13 | 0.05 | 0.63 | 7.39 | 0.24 | 1.69 | 8.52 | 0.24 | 0.14 | 0.94 |
| S4 | 0.10 | 0.008 | 0.85 | 0.13 | 0.04 | 0.18 | 5.33 | 0.18 | 1.67 | 7.20 | 0.23 | 0.13 | 0.87 |
| S5 | 0.21 | 0.009 | 0.88 | 0.10 | 0.03 | 0.17 | 6.79 | 0.18 | 3.21 | 7.17 | 0.19 | 0.10 | 0.71 |
| S6 | 0.23 | 0.014 | 0.80 | 0.10 | 0.03 | 0.08 | 7.03 | 0.20 | 3.18 | 6.97 | 0.19 | 0.09 | 0.86 |
| S7 | 0.09 | 0.014 | 0.85 | 0.13 | 0.04 | 0.16 | 6.20 | 0.20 | 2.46 | 7.49 | 0.25 | 0.12 | 0.59 |
| S8 | 0.11 | 0.009 | 0.52 | 0.08 | 0.03 | 0.08 | 5.25 | 0.15 | 3.02 | 4.96 | 0.15 | 0.07 | 0.31 |
| S9 | 0.07 | 0.011 | 1.01 | 0.14 | 0.05 | 0.67 | 5.42 | 0.24 | 2.28 | 5.18 | 0.24 | 0.09 | 2.62 |
| S10 | 0.14 | 0.009 | 1.82 | 0.14 | 0.05 | 1.50 | 7.70 | 0.24 | 3.12 | 7.21 | 0.23 | 0.11 | 2.31 |
| S11 | 0.08 | 0.015 | 1.71 | 0.18 | 0.06 | 1.41 | 6.88 | 0.35 | 1.59 | 6.44 | 0.31 | 0.11 | 1.21 |
| S12 | 0.28 | 0.017 | 1.40 | 0.11 | 0.04 | 1.05 | 6.04 | 0.23 | 2.55 | 6.13 | 0.26 | 0.10 | 0.88 |
| S13 | 0.04 | 0.020 | 1.52 | 0.17 | 0.05 | 1.27 | 7.67 | 0.37 | 2.92 | 5.77 | 0.31 | 0.08 | 0.86 |
| S14 | 0.04 | 0.005 | 0.52 | 0.20 | 0.07 | 0.14 | 4.23 | 0.35 | 1.26 | 4.62 | 0.28 | 0.07 | 5.10 |
| S15 | 0.07 | 0.013 | 1.22 | 0.17 | 0.06 | 0.70 | 5.92 | 0.34 | 1.57 | 5.86 | 0.29 | 0.10 | 1.49 |
| S16 | 0.11 | 0.013 | 1.65 | 0.14 | 0.05 | 1.35 | 6.51 | 0.32 | 1.74 | 6.37 | 0.27 | 0.10 | 1.22 |
| S17 | 0.10 | 0.010 | 1.34 | 0.19 | 0.06 | 1.00 | 5.10 | 0.31 | 1.52 | 6.03 | 0.31 | 0.11 | 1.39 |
| S18 | 0.35 | 0.019 | 1.31 | 0.10 | 0.04 | 0.95 | 4.17 | 0.25 | 1.75 | 6.59 | 0.26 | 0.13 | 1.33 |
| S19 | 0.09 | 0.021 | 1.58 | 0.18 | 0.06 | 1.33 | 5.30 | 0.31 | 2.08 | 6.85 | 0.31 | 0.13 | 0.93 |
| S20 | 0.10 | 0.011 | 1.76 | 0.16 | 0.05 | 1.31 | 8.27 | 0.33 | 2.55 | 7.48 | 0.27 | 0.12 | 1.03 |
| S21 | 0.23 | 0.012 | 2.06 | 0.13 | 0.04 | 1.59 | 9.07 | 0.25 | 2.76 | 8.27 | 0.24 | 0.14 | 1.10 |
| S22 | 0.15 | 0.025 | 2.01 | 0.17 | 0.05 | 1.55 | 8.67 | 0.27 | 1.89 | 7.89 | 0.27 | 0.15 | 1.16 |
| S23 | 0.26 | 0.027 | 2.26 | 0.15 | 0.05 | 1.92 | 8.53 | 0.27 | 3.46 | 8.31 | 0.27 | 0.16 | 1.22 |
| S24 | 0.19 | 0.008 | 1.02 | 0.12 | 0.04 | 0.53 | 5.76 | 0.23 | 1.61 | 6.01 | 0.23 | 0.09 | 4.71 |
| S25 | 0.11 | 0.020 | 1.89 | 0.18 | 0.06 | 1.63 | 5.51 | 0.21 | 1.79 | 7.26 | 0.28 | 0.15 | 1.17 |
| S26 | 0.08 | 0.020 | 1.91 | 0.16 | 0.05 | 1.60 | 6.94 | 0.25 | 2.23 | 6.65 | 0.25 | 0.12 | 0.85 |
| S27 | 0.31 | 0.009 | 1.35 | 0.08 | 0.03 | 1.01 | 5.65 | 0.17 | 2.48 | 6.03 | 0.18 | 0.10 | 1.02 |
| S28 | 0.13 | 0.011 | 1.77 | 0.16 | 0.05 | 1.51 | 6.57 | 0.24 | 2.55 | 7.14 | 0.27 | 0.14 | 1.06 |
| S29 | 0.10 | 0.012 | 1.65 | 0.18 | 0.06 | 1.40 | 6.75 | 0.48 | 2.57 | 7.08 | 0.28 | 0.13 | 1.32 |
| S30 | 0.13 | 0.013 | 2.03 | 0.20 | 0.07 | 1.76 | 7.63 | 0.48 | 3.58 | 8.38 | 0.33 | 0.15 | 1.53 |
| S31 | 0.06 | 0.009 | 1.60 | 0.16 | 0.05 | 1.33 | 7.05 | 0.50 | 2.27 | 5.53 | 0.25 | 0.08 | 1.44 |
| S32 | 0.06 | 0.006 | 1.67 | 0.17 | 0.06 | 1.37 | 6.69 | 0.51 | 2.63 | 6.01 | 0.29 | 0.09 | 1.40 |
| S33 | 0.04 | 0.015 | 1.56 | 0.21 | 0.07 | 1.22 | 6.33 | 0.47 | 3.38 | 7.18 | 0.33 | 0.12 | 1.60 |
| S34 | 0.05 | 0.011 | 1.34 | 0.17 | 0.05 | 0.86 | 7.33 | 0.49 | 2.78 | 6.54 | 0.30 | 0.09 | 1.22 |
| S35 | 0.08 | 0.008 | 1.68 | 0.17 | 0.06 | 1.40 | 4.23 | 0.40 | 1.87 | 7.39 | 0.35 | 0.12 | 1.54 |
| S36 | 0.05 | 0.020 | 1.52 | 0.25 | 0.08 | 1.21 | 4.05 | 0.25 | 1.64 | 7.23 | 0.42 | 0.17 | 3.02 |
| S37 | 0.09 | 0.011 | 2.26 | 0.18 | 0.04 | 1.89 | 6.91 | 0.27 | 2.67 | 8.82 | 0.35 | 0.15 | 2.31 |
| S38 | 0.07 | 0.010 | 0.74 | 0.16 | 0.06 | 0.35 | 3.61 | 0.23 | 1.58 | 4.52 | 0.29 | 0.08 | 5.55 |
| S39 | 0.65 | 0.010 | 1.67 | 0.23 | 0.08 | 0.04 | 5.77 | 0.34 | 1.71 | 5.87 | 0.35 | 0.14 | 1.52 |
| S40 | 0.04 | 0.017 | 1.41 | 0.29 | 0.09 | 0.87 | 8.24 | 0.45 | 2.23 | 6.19 | 0.41 | 0.11 | 0.94 |
| S41 | 0.04 | 0.014 | 0.96 | 0.37 | 0.12 | 1.58 | 5.79 | 0.50 | 2.00 | 5.17 | 0.49 | 0.10 | 1.21 |
| S42 | 0.03 | 0.013 | 0.98 | 0.29 | 0.10 | 1.61 | 5.57 | 0.35 | 2.59 | 6.02 | 0.44 | 0.11 | 0.85 |
| S43 | 0.29 | 0.007 | 1.30 | 0.25 | 0.09 | 1.05 | 4.64 | 0.31 | 1.49 | 4.87 | 0.36 | 0.11 | 1.16 |
| S44 | 0.04 | 0.015 | 1.18 | 0.43 | 0.13 | 2.51 | 5.88 | 0.58 | 1.44 | 4.62 | 0.49 | 0.12 | 2.85 |
| S45 | 2.49 | 0.033 | 0.41 | 0.14 | 0.06 | 0.60 | 11.64 | 0.30 | 0.18 | 8.58 | 0.21 | 0.17 | 3.49 |
| S46 | 0.41 | 0.023 | 1.05 | 0.22 | 0.08 | 0.95 | 6.43 | 0.47 | 3.23 | 5.03 | 0.36 | 0.10 | 1.29 |
| S47 | 2.00 | 0.028 | 1.77 | 0.10 | 0.05 | 0.30 | 6.68 | 0.20 | 3.20 | 7.78 | 0.17 | 0.18 | 1.87 |
| S48 | 3.80 | 0.038 | 2.18 | 0.12 | 0.05 | 1.09 | 10.79 | 0.23 | 4.22 | 9.53 | 0.20 | 0.22 | 3.17 |
| S49 | 0.47 | 0.016 | 1.44 | 0.29 | 0.10 | 0.66 | 5.08 | 0.27 | 2.97 | 6.60 | 0.34 | 0.35 | 2.89 |
| S50 | 0.40 | 0.015 | 3.01 | 0.31 | 0.10 | 0.76 | 9.29 | 0.45 | 3.11 | 9.28 | 0.43 | 0.44 | 2.51 |
| S51 | 0.29 | 0.007 | 1.30 | 0.25 | 0.09 | 1.08 | 4.64 | 0.31 | 1.49 | 4.87 | 0.36 | 0.11 | 1.16 |
| S52 | 0.04 | 0.015 | 1.18 | 0.43 | 0.13 | 1.01 | 5.88 | 0.58 | 1.44 | 4.62 | 0.49 | 0.12 | 2.85 |
| S53 | 0.65 | 0.046 | 0.86 | 0.11 | 0.15 | 1.46 | 1.46 | 0.22 | 1.85 | 3.78 | 0.49 | 0.59 | 3.65 |
| S54 | 0.05 | 0.038 | 1.36 | 0.27 | 0.08 | 1.07 | 5.13 | 0.32 | 1.76 | 5.25 | 0.34 | 0.26 | 1.59 |
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