Article(id=1314907735007789392, tenantId=1146029695717560320, journalId=1235980550691926019, issueId=1314907656704324517, articleNumber=null, orderNo=null, doi=10.3969/j.issn.0253-6099.2026.01.033, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1753804800000, receivedDateStr=2025-07-30, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1791428033830, onlineDateStr=2026-10-08, pubDate=null, pubDateStr=null, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1791428033830, onlineIssueDateStr=2026-10-08, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1791428033830, creator=13701087609, updateTime=1791428033830, updator=13701087609, issue=Issue{id=1314907656704324517, tenantId=1146029695717560320, journalId=1235980550691926019, year='2026', volume='46', issue='1', pageStart='1', pageEnd='206', issueExtLink='null', onlineDate='null', pubDate='1769875200000', pubDateStr='2026-02-01', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1791428015160, creator='13701087609', updateTime=1791430491940, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1314918045139690301, tenantId=1146029695717560320, journalId=1235980550691926019, issueId=1314907656704324517, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1314918045139690302, tenantId=1146029695717560320, journalId=1235980550691926019, issueId=1314907656704324517, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=197, endPage=201, ext={EN=ArticleExt(id=1314907735876010321, articleId=1314907735007789392, tenantId=1146029695717560320, journalId=1235980550691926019, language=EN, title=Preparation Process Optimization for High-Performance Battery-Grade Iron Phosphate, columnId=1236276108207902848, journalTitle=Mining and Metallurgical Engineering, columnName=MATERIALS, runingTitle=null, highlight=null, articleAbstract=

To improve synthesis efficiency and performance of iron phosphate (FePO₄) product, a precursor for cathode materials of lithium-ion batteries, a two-step process consisting of oxidation-precipitation, and conversion was proposed to prepare iron phosphate with ferrous sulfate and ammonium phosphate as raw materials. The effects of key parameters, such as addition amount of hydrogen peroxide (oxidant), feeding rate, and reaction temperature, on the particle size distribution (D₅₀), purity, and Fe/P ratio of the product were investigated. The optimized process conditions were determined as follows:oxidation at a temperature of 40 ℃ for 2 h by adding hydrogen peroxide at an amount of 1.25 times the theoretical dosage and feeding material for 50 min in the oxidation stage; precipitation at a temperature of 40 ℃ by feeding ammonium phosphate for 50~55 min in the precipitation stage; and with phosphoric acid at concentration of 0.6 mol/L and a temperature of 90 ℃ for the conversion stage. As a result, a high-purity iron phosphate with D₅₀ of 3.0 μm, impurity content lower than 0.01%, and Fe/P at a molar ratio of 0.997 can be successfully prepared. SEM and XRD characterization results show that the product consists of regular spherical secondary particles formed with densely stacked primary lamellar crystals, presenting higher degree of crystallinity.

, authors=Huan HUANG¹, Zhongyi ZHANG¹, Qian LAN², Zhifu WANG^{3, 4, 5, 6}, Qi CHENG³, authorsList=Huan HUANG, Zhongyi ZHANG, Qian LAN, Zhifu WANG, Qi CHENG, authorCompany=null, correspAuthors=Qi CHENG, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1314907737046221138, articleId=1314907735007789392, tenantId=1146029695717560320, journalId=1235980550691926019, language=CN, title=高性能电池级磷酸铁制备工艺优化研究, columnId=1236276110049202322, journalTitle=矿冶工程杂志, columnName=材料, runingTitle=null, highlight=null, articleAbstract=

为提高锂离子电池正极材料前驱体磷酸铁（FePO₄）的合成效率与产品性能，以硫酸亚铁和磷酸铵为原料，采用“氧化沉淀-转化”两步法制备磷酸铁，探究了氧化剂过氧化氢添加量、投料速率、反应温度等关键参数对产物粒径分布（D₅₀）、纯度及铁磷比的影响。确定的优化工艺条件为：氧化阶段过氧化氢添加量为理论量的1.25倍、投料时长50 min、氧化温度40 ℃、氧化时间2 h，沉淀阶段磷酸铵投料时长50~55min、沉淀温度40 ℃，转化阶段转化温度90 ℃、磷酸浓度0.6 mol/L。在此条件下成功制备出D₅₀为3.0 μm、杂质含量低于0.01%、Fe/P物质的量比0.997的高纯度磷酸铁。SEM与XRD表征结果显示产品为片状一次颗粒堆积而成的规则球形二次颗粒，结晶度良好。

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黄欢（1988—），男，湖北武汉人，工程师，主要研究方向为锂电池检测及应用。E-mail: huanghuan@catarc.ac.cn

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黄欢（1988—），男，湖北武汉人，工程师，主要研究方向为锂电池检测及应用。E-mail: huanghuan@catarc.ac.cn

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