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CiteSpace, as a bibliometric analysis tool, was firstly used to quantitatively analyze and visualize keyword clusters, co-citation relationships and burst terms for scientific literature on Laves phase used for high-temperature materials in the Web of Science from 2003 to 2023. A timeline chart of keyword clustering reflects the fundamental development status of Laves phase research in the search interval, revealing two hot topics in frontier research: one is improvement of room temperature brittleness or synergistic improvement of strength and plasticity of multi-phase high-entropy alloys reinforced by Laves phases, another is the effect of Laves phase precipitates on the microstructure and properties of heat-resistant alloy steels (P92, 12Cr and G115) at 600-650 ℃, at which creep occurs. The timeline chart of keyword clustering is consistent with the chart of relationship between literature and author in citation networks, both reflecting the activity of Laves phase research. In the future, those key authors and publications with high-quality achievement mined by the visualized patterns and trend should be paid more attention.

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首次利用CiteSpace文献计量分析软件对Web of Science中2003—2023年高温结构材料用Laves相研究文献的关键词、文献共被引、作者和期刊共被引进行了定量和可视化网络图谱分析。关键词聚类时间线图反映了检索区间内Laves相研究的基本发展状况，揭示两大热点前沿主题分别是Laves相增强的多相高熵合金的室温脆性改善或强度-塑性协同提升问题，以及Laves相析出物对600～650 ℃蠕变服役条件下P92、12Cr和G115等新型耐热合金钢组织与性能的影响。关键词聚类时间线图与文献、作者共被引网络图具备一致性，共同反映Laves相研究的活跃性。未来，应关注可视化图谱挖掘的高质量成果产出的关键作者和期刊。

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肖璇（1979—），男，湖北随州人，博士，副教授，主要从事先进高温结构材料的强韧化和难变形材料的成形理论及工艺优化工作。E-mail：

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肖璇（1979—），男，湖北随州人，博士，副教授，主要从事先进高温结构材料的强韧化和难变形材料的成形理论及工艺优化工作。E-mail：

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肖璇（1979—），男，湖北随州人，博士，副教授，主要从事先进高温结构材料的强韧化和难变形材料的成形理论及工艺优化工作。E-mail：

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tenantId=1146029695717560320, journalId=1235980550691926019, articleId=1240631879695651175, language=EN, label=Table 1, caption=

Top nine journals by co-citation frequency

, figureFileSmall=null, figureFileBig=null, tableContent=
序号共被引频次期刊影响因子
11 620MAT SCI ENG A-STRUCT6.4
21 313ACTA MATER9.4
31 173J ALLOY COMPD6.2
41 046METALL MATER TRANS A2.8
5947INTERMETALLICS4.4
6899SCRIPTA MATER6.0
7710MATER CHARACT4.7
8698MATER DESING8.4
9567J MATER SCI4.5
), ArticleFig(id=1240651350745337992, tenantId=1146029695717560320, journalId=1235980550691926019, articleId=1240631879695651175, language=CN, label=表1, caption=

高频次共被引期刊

, figureFileSmall=null, figureFileBig=null, tableContent=
序号共被引频次期刊影响因子
11 620MAT SCI ENG A-STRUCT6.4
21 313ACTA MATER9.4
31 173J ALLOY COMPD6.2
41 046METALL MATER TRANS A2.8
5947INTERMETALLICS4.4
6899SCRIPTA MATER6.0
7710MATER CHARACT4.7
8698MATER DESING8.4
9567J MATER SCI4.5
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基于CiteSpace的高温结构材料用Laves相合金的文献计量和可视化
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肖璇 1 , 金毛毛 1 , 秦文洲 1 , 邓莉萍 2 , 姚敬 2
矿冶工程杂志 | 材料 2025,45(1): 153-159
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矿冶工程杂志 | 材料 2025, 45(1): 153-159
基于CiteSpace的高温结构材料用Laves相合金的文献计量和可视化
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肖璇1 , 金毛毛1, 秦文洲1, 邓莉萍2, 姚敬2
作者信息
  • 1.南昌航空大学　航空制造工程学院，江西　南昌　330063
  • 2.南昌航空大学　材料科学与工程学院，江西　南昌　330063

    • 肖璇（1979—），男，湖北随州人，博士，副教授，主要从事先进高温结构材料的强韧化和难变形材料的成形理论及工艺优化工作。E-mail：

CiteSpace-Based Bibliometrics and Visualization of Laves Phases for High Temperature Applications
Xuan XIAO1 , Maomao JIN1, Wenzhou QIN1, Liping DENG2, Jing YAO2
Affiliations
  • 1.School of Aeronautic Manufacturing Engineering, Nanchang Hangkong University, Nanchang 330063, Jiangxi, China
  • 2.School of Material Science and Engineering, Nanchang Hangkong University, Nanchang 330063, Jiangxi, China
出版时间: 2025-02-01 doi: 10.3969/j.issn.0253-6099.2025.01.029
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摘要
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首次利用CiteSpace文献计量分析软件对Web of Science中2003—2023年高温结构材料用Laves相研究文献的关键词、文献共被引、作者和期刊共被引进行了定量和可视化网络图谱分析。关键词聚类时间线图反映了检索区间内Laves相研究的基本发展状况，揭示两大热点前沿主题分别是Laves相增强的多相高熵合金的室温脆性改善或强度-塑性协同提升问题，以及Laves相析出物对600～650 ℃蠕变服役条件下P92、12Cr和G115等新型耐热合金钢组织与性能的影响。关键词聚类时间线图与文献、作者共被引网络图具备一致性，共同反映Laves相研究的活跃性。未来，应关注可视化图谱挖掘的高质量成果产出的关键作者和期刊。

Laves相  /  金属间化合物  /  文献综述  /  文献计量  /  可视化网络  /  高温结构材料  /  CiteSpace  /  AB2

CiteSpace, as a bibliometric analysis tool, was firstly used to quantitatively analyze and visualize keyword clusters, co-citation relationships and burst terms for scientific literature on Laves phase used for high-temperature materials in the Web of Science from 2003 to 2023. A timeline chart of keyword clustering reflects the fundamental development status of Laves phase research in the search interval, revealing two hot topics in frontier research: one is improvement of room temperature brittleness or synergistic improvement of strength and plasticity of multi-phase high-entropy alloys reinforced by Laves phases, another is the effect of Laves phase precipitates on the microstructure and properties of heat-resistant alloy steels (P92, 12Cr and G115) at 600-650 ℃, at which creep occurs. The timeline chart of keyword clustering is consistent with the chart of relationship between literature and author in citation networks, both reflecting the activity of Laves phase research. In the future, those key authors and publications with high-quality achievement mined by the visualized patterns and trend should be paid more attention.

Laves phase  /  intermetallic compound  /  literature review  /  bibliometrics  /  network visualization  /  high-temperature material  /  CiteSpace  /  AB2
肖璇, 金毛毛, 秦文洲, 邓莉萍, 姚敬. 基于CiteSpace的高温结构材料用Laves相合金的文献计量和可视化. 矿冶工程杂志, 2025 , 45 (1) : 153 -159 . DOI: 10.3969/j.issn.0253-6099.2025.01.029
Xuan XIAO, Maomao JIN, Wenzhou QIN, Liping DENG, Jing YAO. CiteSpace-Based Bibliometrics and Visualization of Laves Phases for High Temperature Applications[J]. Mining and Metallurgical Engineering, 2025 , 45 (1) : 153 -159 . DOI: 10.3969/j.issn.0253-6099.2025.01.029
正文
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20世纪早期，奥地利矿物与晶体学家Fritz Laves首次描述并解释了复杂立方MgCu2与复杂六方MgZn2和MgNi2的某些金属间化合物具备晶体结构相似性和紧密关系[1]。随后，著名金属学家Gustav Schulze提出将化学式为AB2的这类特殊金属间化合物命名为“Laves相”[2-3]。近年来，Laves相因低密度、良好热稳定性和高温蠕变抗力以及优异的储氢性能等备受关注[4-6]。特别是在航空航天、火电核电等领域的高温结构材料应用场合，Laves相金属间化合物有望替代镍基高温合金，成为有应用潜力的新型超高温应用候选结构材料之一。
Laves相合金的制备、性能优化以及实用化等方面仍面临诸多挑战和待解决的问题[7-9]。目前有关Laves相研究的全面性综述较为匮乏，研究成果发表时间也相对较早，并且更偏向于定性归纳与主观总结。本文基于文献计量学角度开展Laves相研究文献的知识图谱可视化研究，快速准确定位本领域的开创性和标志性论文，识别对Laves相研究发展至关重要的成果，明确主流主题和研究前沿的演变，以挖掘揭示Laves相的研究现状和发展趋势，为未来Laves相金属间化合物的研究提供参考和决策指导。
1　数据来源与研究方法
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CiteSpace是一个在文献信息分析领域有独特影响力的数据分析和可视化应用软件[10]，与该软件最匹配的数据来自Web of Science（WoS）数据库[11]。本研究的数据来源于WoS核心合集数据库（Web of Science Core Collection），该合集提供全面的引文网络，涵盖所收录出版物的被引用参考文献并完整索引所有作者及其机构信息。检索主题设定为“Laves phase”，时间跨度为2003—2023年，文献类型包括“Article”“Proceeding Paper”和“Review”，检索截止日期为2023年6月28日，经初步筛选，共得4 832篇文献。鉴于本研究关注Laves相作为高温结构材料的应用，排除无关文献后最终筛选出有效数据文献共2 080篇。
利用CiteSpace 6.2.R4文献计量软件进行知识图谱的可视化构建。首先，将2 080条研究数据以纯文本格式导入软件。然后，按照年度进行时间切片，并以标题、摘要、作者和关键词为术语来源，选择了Keyword（关键词）、Reference（被引文献）、Cited Author（被引作者）和Cited Journal（被引期刊）等节点类型。在关键词聚类时间线图和文献、作者及期刊共被引网络的构建过程中，使用Pathfinder（探路者剪切）算法对关键词聚类时间线图进行修剪，以突出重要的学术路径。为了构建作者与期刊之间的共被引网络，选用Minimum Spanning Tree（最小生成树剪切）算法处理网络，进而揭示领域内的核心结构。同时，采用Cluster View-Static（集群视图-静态）和Show Merged Network（显示合并的网络）等模式参数进行可视化绘制。最后，通过调整控制面板的各项阈值，使得图谱内容更加清晰有序，并获得了相应的Laves相研究可视化分析结果与最新研究动态。
2　关键词演化与趋势分析
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关键词聚类是基于词条共现分析，利用对数似然比算法（LLR）分析结构特征、关键节点和集群之间的关联度，以发现对应研究领域的热点主题[12]。图1是2003—2023年研究Laves相文献的关键词聚类时间线图，它将聚类包含的关键词按照时间顺序展开，反映了该聚类在检索区间内的发展成果和演变过程。图中包含了660个节点和1 142条连线，最上方时间标签表示下方关键词在此数据集中首次出现的时间。左上方显示的网络集群模块值（Modularity Q）为0.768 9（>0.3），说明划分的聚类结构是合理的；轮廓值（Silhouette S）为0.895 2（>0.7），表明所构建的聚类网络具有较高的均质性，因此聚类结果可靠且效率高[13]。需要注意的是，图中还显示了跨集群之间存在一些连线，表明不同集群之间存在实质性的相互作用和研究热点的集中现象。
从图1还可以看出，由集群规模从大到小筛选出依序排布的8个聚类分别是：#0 g115 steel（G115钢），#1 electronic structure（电子结构），#2 inconel 718 alloy（inconel 718合金），#3 mechanical properties（力学性能），#4 creep behavior（蠕变行为），#5 elastic properties（弹性性能），#6 high entropy alloys（高熵合金）和#7 laves phase（Laves相）。其中分别位于聚类#1、#2和#3左侧的较大节点关键词electronic structure（电子结构）、precipitation（析出物）和mechanical properties（力学性能）是除了主题词“Laves phase”之外在时间线左端2003—2004年首次出现的重要关键词。这些早期阶段的高频关键词不仅为Laves相研究提供了关键线索，而且与材料科学研究的基本范式相契合。需要注意的是，时间线图还反映了2010—2013年是另一个高频关键词涌现的时间段，整合实际含义相同的关键词后发现这一时间段有三个高频关键词，分别是microstructure evolution（微观组织演变）、high entropy alloys（高熵合金）和solid solution（固溶体）。
上述两个时期的典型关键词相互交叉和推进，为Laves相研究的热点主题提供了清晰的视角。具有独特的结构和物理性质的Laves相金属间化合物有3种结构类型，即密排六方的C14型（也称为MgZn2型六方晶系）、密排立方的C15型（MgCu2型立方晶系）和双密排六方的C36型（MgNi2型六方晶系）[5]。高温结构应用Laves相合金的力学性能、热稳定性和相变行为受电子结构直接影响。充分理解电子态密度、能带结构等关键信息对合金性能微观调控和优化至关重要，可为合金的设计和应用提供重要的指导和基础[14-17]。此外，在聚类#0和#2呈现了Laves相析出物对新型耐热合金钢和镍基高温合金的应用开发也具有重要意义。它们在制备过程中或长期高温服役产生的Laves相析出物不仅产生强化效应，Laves相的过量析出或晶粒长大可能严重降低合金的高温性能，甚至导致热时效致脆，从而过早失效。因此，重新评估并深入研究析出物的形成机制、演变规律以及对材料性能的影响，有助于改进合金的高温强度、蠕变持久性、抗氧化和抗腐蚀性能，进而指导合金的设计、制备工艺和性能优化[18-22]。
3　共被引网络可视化分析
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3.1　文献共被引可视化分析
当两篇文献同时被第三篇文献引用时，这两篇文献之间就存在共被引关系。文献的被引频次反映了该文献在学术领域的认可程度和网络地位[23]。将检索获取的2 080条WoS数据导入CiteSpace中，节点类型设为Reference（被引文献），控制图谱可视化的筛选阈值Threshold为20，表示图谱显示的标签节点的共被引频次不小于20，由此得到图2所示的Laves相研究文献共被引的可视化网络图谱。从图2可以看出，高被引文献主要分布于2013—2021年。图中每一个圆形节点表示一篇文献，节点灰度表示年份，节点大小表示文献的总被引次数，节点越大则文献被引次数越多，表明文献的研究结论得到学界的普遍关注和认可。共被引网络中节点大小和位置决定了该文献在本知识域的地位。带有深色外环圈的部分节点表示文献的中心性，也就是该文献在整体知识结构中占据重要位置，也可以看作Laves相研究领域具有重要意义的研究成果。
图2的文献共被引图谱大致可分为两个区域，在同一区域内的节点连线越密集，说明各自区域所代表的文献研究主题关系越密切甚至倾向于一致。右上角的区域以节点最大且突出的Miracle D B和Senkov O N等为代表，反映了对高熵合金或难熔高熵合金中析出高温强化Laves相的研究现状[24-25]。在多相高熵合金中普遍析出的Laves相会导致合金耐高温能力显著提高，同时在常温下塑性或延展性急剧降低。这一区域的共被引文献关注于如何深入理解和有效控制Laves相在合金中的形成机制、相转变、相稳定性和力学行为，以实现高熵合金性能的优化和应用拓展[26-27]。在固溶强化效应减弱的高温条件下，析出强化是一种关键的强化机制。通过设计多相结构和热机械过程，可以显著提高难熔高熵合金的高温强度，从而沉淀出精细的、热稳定的第二相颗粒。通过调控Laves相的形貌、尺寸和分布，可以优化高熵合金的强度、韧性和塑性等力学性能，Laves相合金或Laves相增强的多相或双相高熵合金的室温脆性改善或强度-塑性协同提升问题是极活跃的研究前沿和发展趋势之一[1,25]。例如，双相或共晶高熵合金CoCrFeNiNbx或AlCoCrFeNiNbx（x=0～0.8），随着Nb含量逐渐增加，合金微观组织由单一FCC固溶体向FCC+Laves相两相转变，Laves相为C14结构的NbM2（M=Co，Cr，Fe，Ni），而不是常见的Fe2Nb。CoCrFeNiNb0.5合金，压缩断裂强度和应变分别可达2 300 MPa和23.6%以上。所设计的合金表现出优异的室温强度与塑性匹配的综合力学性能[28-29]。
具有复杂多相结构的有序固溶体和/或金属间化合物相存在于很多高熵合金中，高混合熵并不是控制相形成的唯一因素。在以FCC或BCC为主导的多相高熵合金中，常见的强化相是复杂有序相B2、σ、C14型或C15型Laves相、L21相等，在多组元条件下这些强化相的形成机制各有特殊性。在组元中包含Cr、Nb、Ti、Co、Fe等元素时容易产生Laves相增强相[1,25]。目前基于Hume-Rothery规则和热力学参数的唯象判据以及机器学习普遍集中于高熵合金中固溶体相形成的预测上，而对合金中广泛生成的各种类型金属间化合物的相形成判据的研究却很少。文献[30-31]熔铸制备了由Al和Ⅳ～Ⅵ族元素组成的AlCrxNbTiV和AlxCrNbTiVZr（x=0～1.5）高熵合金，经1 200 ℃+24 h均匀化处理后获得BCC+Laves相双相组织，其中AlCrNbTiV和AlCr1.5NbTiV分别析出体积分数为13%和35%的C14型富Cr和Nb的Laves相颗粒存在于体心立方基体中。相组成实验结果验证了由原子尺寸失配度（>5.0%）和Allen电负性差（>7.0%）参数预测高熵合金中Laves相形成门槛值的正确性，但这一判据并不能预测合金中其他有序金属间相的形成。在低密度耐高温难熔高熵合金中广泛添加一定浓度的Cr元素有利于Laves相形成，而Al的合金化可能会促进析出Laves相由C14型向C15型转变。另外，在大规模工业生产铸锭高熵合金的要求下，含Laves相的共晶或多相高熵合金能够改善多组元混合引起的成分不均匀性，并且提高熔体的流动性和可铸性[32-33]。
图2中左下角区域以节点较大的Isik M I和Prat O等为代表，主要研究Laves相析出物对600～650 ℃的蠕变服役条件下P92、12Cr和G115等新型耐热合金钢组织与性能的影响。这些耐热钢广泛应用于火力、核电等能源动力场合的关键部件，必须在600～650 ℃承受机械载荷的蠕变服役条件下运行[18,34-35]。如何控制长期高温服役产生的Laves相析出物和提高高温蠕变性能是重要的热点主题之一。质量分数9%～12%Cr马氏体耐热钢在奥氏体化和回火热处理的初始相组成中并没有Laves相，但在高温热暴露或高温蠕变条件下会在紧邻典型晶界碳化物M23C6（M主要是Cr，也会富Mo和Fe）的位置形核长大为短棒状纳米级Laves相颗粒，Isik等人利用原子探针层析成像技术证实了在Laves相成核之前，微量Si和Mo首先偏析于晶界进而改变Laves相形成的热力学和动力学条件，有利于耐热钢在M23C6碳化物旁边析出提升高温承载能力的Laves相颗粒[35]。文献[36]认为Laves相颗粒易出现在M23C6碳化物旁是由于吞噬生长机制，即Laves相倾向于直接吞噬相邻的M23C6相，且优先沿M23C6与基体界面开始，然后逐渐扩展到M23C6的中心。从图2左下角区域的大节点和高中心性的高被引文献可以发现，为了解决长期高温服役产生的Laves相的过量析出或晶粒长大严重降低新型耐热合金钢的高温性能（蠕变或热时效致脆失效）的问题，首先发现Laves相倾向形成于M23C6附近，然后分析探寻导致这一现象的原因是Mo、Si和P在晶界的微量偏析促使Laves相颗粒在碳化物旁边形成，进一步深入研究Laves相颗粒倾向在M23C6碳化物附近析出的生长机制，共同构成了对这一问题的探究脉络[35-39]。这两个区域的划分也反映了文献共被引可视化结果与图1的关键词聚类时间线结果是一致的。
3.2　作者与期刊共被引可视化分析
作者共被引分析不仅能够揭示某一领域高被引作者的分布情况，还可以识别有影响力的作者。而期刊共被引分析则能够展示研究领域关键知识来源的分布及互动状况[40]。图3和图4分别为由CiteSpace绘制的2003—2023年Laves相相关文献作者和发表期刊的共被引网络，其中作者共被引网络中共有896个节点、1 917条连线，每个节点代表一位作者，两位作者之间的连线表示共被引关系。期刊共被引网络包括851个节点和2 924条连线，相对较大的节点标识的是引文计数大于200的期刊，节点越大，期刊越重要。
从图3和图4可以看出，密集的网络节点反映了Laves相相关研究在检索区间内相当活跃。图3按照作者节点大小进行排序，共引频次相对较高的分别是ABE F（频次300）、YEH J W（275）、ZHANG Y（270）、PERDEW J P（222）、STEIN F（217）、HALD J（198）、SENKOV O N（197）、MIRACLE D B（189）和CANTOR B（162），这些作者主要是高熵合金和耐热合金领域有影响力的作者，例如YEH J W和CANTOR B是高熵合金的开创者，也表明Laves相研究与这些领域有密切联系的知识结构。特别的是，在图2和图3中共同出现ZHANG Y、STEIN F、SENKOV O N和MIRACLE D B这4位作者，说明他们不仅有数量丰富的论文，在论文中还包含相对更高质量的研究成果。表1是高频次共被引期刊，按照期刊节点大小进行排序，共被引频次达到500次以上的9种期刊高质量和高影响力期刊是Laves相研究领域的重要信息源，促进了该领域的学术交流和知识传播。
4　结论
收起
不同于已有的Laves相叙述性综述，本文首次利用CiteSpace文献计量分析软件对Web of Science中2003—2023年高温结构材料用Laves相金属间化合物相关研究文献的关键词、文献共被引、作者和期刊共被引进行了可视化回顾和分析。由关键词时间线图解析获悉关键词聚集涌现的2个重要时间段分别是早期的2003—2004年和中期的2010—2013年。这2个阶段的高频关键词与8个聚类的可视化结果共同构建了Laves相相关研究的知识框架，揭示2003—2023年Laves相研究的两大热点主题和新兴前沿。具体而言，这包括Laves相析出强化的多相高熵合金的室温脆性改善或强度-塑性综合性能提升问题，以及Laves相析出物对600～650 ℃蠕变服役条件下P92、12Cr和G115等新型耐热合金钢组织与性能的影响。这两者反映了重新评估Laves相析出物形成机制、演变规律以及对高温结构材料性能影响的重要性，有助于指导合金的设计、制备工艺和性能优化。
文献共被引、作者和期刊共被引的可视化网络图谱与关键词图谱显示较高的一致性，密集的网络节点反映了Laves相相关研究相当活跃。共被引频次高的作者同时也是上述两个热点方向具有影响力的研究者。以ZHANGY、STEINF、SENKOVON和MIRACLE D B为代表的作者以及MAT SCI ENG A-STRUCT、ACTA MATER等为代表的期刊备受学界关注与认可，构成了国际上Laves相研究知识基础与结构的重要来源。今后意向从事Laves相研究的学者应更多关注这些能够产出更高质量研究成果的作者和期刊。
基金
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  • 国家自然科学基金(52161021)
  • 南昌航空大学轻合金加工科学与技术国防重点学科实验室开放课题(EG202201333)
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参考文献 引证文献
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2025年第45卷第1期
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doi: 10.3969/j.issn.0253-6099.2025.01.029
  • 接收时间：2024-08-12
  • 首发时间：2026-03-17
  • 出版时间：2025-02-01
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  • 收稿日期：2024-08-12
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国家自然科学基金(52161021)
南昌航空大学轻合金加工科学与技术国防重点学科实验室开放课题(EG202201333)
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    1.南昌航空大学　航空制造工程学院，江西　南昌　330063
    2.南昌航空大学　材料科学与工程学院，江西　南昌　330063
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2种不同金属材料的力学参数
科
Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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