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The effect of laser remelting (LR) on the microstructure property and thermal stability of Ti-6Al-4V alloy prepared by laser powder bed fusion (LPBF) was investigated. The results show that after LR treatment, the thermal stability of the α′ phase within the LRed-Ti-6Al-4V titanium alloy samples is significantly improved, and the temperature at which β-Ti phase appears is up from 500 ℃ to 700 ℃. After heat treatment, the grains in LPBF-Ti-6Al-4V titanium alloy grow continuously, and obviously appear to be “short bar-like” and “coarse lamellar” at the temperature above 700 ℃; while the grains in the melting zone of the surface layer of the LRed-Ti-6Al-4V sample are still maintain equiaxial, and the relatively uniform and fine needle-like microstructure are observed in the melting zone and heat affected zone above 700 ℃. The surface microhardness of those two groups of samples decreases with the increased temperature, especially significant at 700 ℃ and 850 ℃ respectively. It is found that the rapid coarsening of β-Ti grains is the main reason for the falling down of hardness.
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研究了激光重熔(LR)对激光粉末床熔合(LPBF)制备Ti-6Al-4V合金的组织性能和热稳定性的影响。结果表明,LR处理后,LRed-Ti-6Al-4V钛合金样品内α′相热稳定性显著提升,β-Ti相出现的温度点由500 ℃升至700 ℃。热处理后,LPBF-Ti-6Al-4V钛合金内晶粒持续生长,700 ℃以上出现明显的“短棒状”和“粗层片状”特征;而LRed-Ti-6Al-4V样品表层熔化区内晶粒仍维持等轴特征,700 ℃以上的熔化区和热影响区内呈现较为均匀细小的针状组织。两组样品的表面显微硬度值随温度升高而不断降低,并且分别在700 ℃和850 ℃显著下降,β-Ti晶粒的迅速粗化是引起硬度下降的主要原因。
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詹宇星(2001—),女,湖南长沙人,硕士研究生,主要研究方向为增材制造钛合金。E-mail:xyzxax13333@163.com
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詹宇星(2001—),女,湖南长沙人,硕士研究生,主要研究方向为增材制造钛合金。E-mail:xyzxax13333@163.com
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样品热处理前XRD图像, figureFileSmall=G1isheMo4bYI4rpSlFv6og==, figureFileBig=5b5YqErr5t/md/L3lHzI2Q==, tableContent=null), ArticleFig(id=1240651348413313048, tenantId=1146029695717560320, journalId=1235980550691926019, articleId=1240631734715347724, language=EN, label=null, caption=null, figureFileSmall=lkoNPk+lR0ebT1CrRJ5slw==, figureFileBig=W6Fjj6walk7sLQLKrs3a0Q==, tableContent=null), ArticleFig(id=1240651348681748529, tenantId=1146029695717560320, journalId=1235980550691926019, articleId=1240631734715347724, language=CN, label=图2, caption=
2组样品不同温度下热处理后的XRD图像(a)LPBF-Ti-6Al-4V样品;(b)LRed-Ti-6Al-4V样品
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LPBF-Ti-6Al-4V合金热处理前后显微组织形貌(a),(b)热处理前;(c)500 ℃热处理后;(d)600 ℃热处理后;(e)700 ℃热处理后;(f)850 ℃热处理后
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LRed-Ti-6Al-4V合金热处理前后显微组织形貌(a),(b)热处理前;(c)500 ℃热处理后;(d)600 ℃热处理后;(e)700 ℃热处理后;(f)850 ℃热处理后
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样品不同温度热处理前后表面显微硬度(a)LPBF-Ti-6Al-4V样品;(b)LRed-Ti-6Al-4V样品
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| 样品名称 | 退火温度/℃ | β相峰强度 | α(α′)相峰强度 |
|---|
| LPBF-Ti-6Al-4V | 500 ℃ | 251 | 1 154 |
| 600 ℃ | 739 | 1 591 |
| 700 ℃ | 864 | 1 766 |
| 850 ℃ | 418 | 646 |
| LRed-Ti-6Al-4V | 500 ℃ | — | — |
| 600 ℃ | — | — |
| 700 ℃ | 105 | 1 249 |
| 850 ℃ | 291 | 1 460 |
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2组样品内β相、α(α′)相衍射峰强度
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| 样品名称 | 退火温度/℃ | β相峰强度 | α(α′)相峰强度 |
|---|
| LPBF-Ti-6Al-4V | 500 ℃ | 251 | 1 154 |
| 600 ℃ | 739 | 1 591 |
| 700 ℃ | 864 | 1 766 |
| 850 ℃ | 418 | 646 |
| LRed-Ti-6Al-4V | 500 ℃ | — | — |
| 600 ℃ | — | — |
| 700 ℃ | 105 | 1 249 |
| 850 ℃ | 291 | 1 460 |
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