Article(id=1236334642412974951, tenantId=1146029695717560320, journalId=1235980550691926019, issueId=1236334630450819368, articleNumber=null, orderNo=null, doi=10.3969/j.issn.0253-6099.2023.06.028, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1685548800000, receivedDateStr=2023-06-01, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1772694748737, onlineDateStr=2026-03-05, pubDate=1701360000000, pubDateStr=2023-12-01, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1772694748737, onlineIssueDateStr=2026-03-05, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1772694748737, creator=13701087609, updateTime=1772694748737, updator=13701087609, issue=Issue{id=1236334630450819368, tenantId=1146029695717560320, journalId=1235980550691926019, year='2023', volume='43', issue='6', pageStart='1', pageEnd='183', issueExtLink='null', onlineDate='null', pubDate='null', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1772694745886, creator=13701087609, updateTime=1772694896382, updator=13701087609, preIssue=null, nextIssue=null, ext={EN=IssueExt(id=1236335261735506524, tenantId=1146029695717560320, journalId=1235980550691926019, issueId=1236334630450819368, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1236335261735506525, tenantId=1146029695717560320, journalId=1235980550691926019, issueId=1236334630450819368, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null}, startPage=128, endPage=132, ext={EN=ArticleExt(id=1236334642819822455, articleId=1236334642412974951, tenantId=1146029695717560320, journalId=1235980550691926019, language=EN, title=Separation of Manganese and Lead from Electrolytic Manganese Anode Slime by Reduction Roasting and Acid Leaching Process, columnId=1236276106727321817, journalTitle=Mining and Metallurgical Engineering, columnName=METALLURGY, runingTitle=null, highlight=null, articleAbstract=

Electrolytic manganese anode slime (EMAS) was processed by adopting sulfur-based reduction roasting and sulfuric acid leaching to separate manganese and lead therein. The effects of roasting temperature, molar ratio of sulfur to manganese, roasting time, particle size of EMAS, stirring speed in leaching, leaching temperature, leaching time, solid-liquid ratio and sulfuric acid concentration on separation of manganese and lead were studied. The results show that with the optimized roasting conditions, including roasting temperature of 550 ℃, molar ratio of sulfur to manganese at 1∶1, roasting time of 50 min, EMAS at particle size of -0.177 mm, and optimized acid leaching conditions including stirring speed of 350 r/min, leaching temperature of 40 ℃, leaching time of 20 min, solid-liquid ratio at 1∶20, and sulfuric acid concentration of 2.5 mol/L, the leaching rate of manganese from EMAS can reach 97.4%, and the concentration of manganese ions in filtrate is 38.84 g/L, while the content of Pb in leaching residue is 45.26%. As a result, the effective separation between manganese and lead can be actualized.

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采用硫磺还原焙烧-硫酸浸出处理电解锰阳极泥（EMAS），实现其中锰、铅分离。研究了焙烧过程中焙烧温度、硫磺与锰物质的量比、焙烧时间、EMAS粒径以及浸出过程中搅拌速度、浸出温度、浸出时间、固液比及硫酸浓度对锰、铅分离的影响。结果表明，焙烧优化条件为：焙烧温度550 ℃、硫磺与锰物质的量比1∶1、焙烧时间50 min、EMAS粒径-0.177 mm，酸浸优化条件为：搅拌转速350 r/min、浸出温度40 ℃、浸出时间20 min、固液比1∶20、硫酸浓度2.5 mol/L，此条件下阳极泥中锰浸出率达97.4%（滤液中锰离子浓度为38.84 g/L），浸出渣中Pb含量达45.26%，有效实现了锰与铅的分离。

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龙腾发（1977—），男，广西桂林人，博士，副教授，主要从事固体废弃物处理及资源化研究。

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龙腾发（1977—），男，广西桂林人，博士，副教授，主要从事固体废弃物处理及资源化研究。

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