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The acid leaching solution of electrostatic precipitator dust from copper smelting has a high concentration of sulfuric acid, in which the iron and arsenic exist in the form of Fe³⁺and As⁵⁺, thus it is decided to adopt arsenic sulfide residue as the precipitant for copper precipitation. Firstly, an experiment was performed on the addition of arsenic sulfide residue in single Cu²⁺ and Fe³⁺ solution with different acid concentrations. Based on that, an experiment was performed for copper precipitation and arsenic leaching in the actual acid leaching solution. The results show that in the process of copper precipitation with arsenic sulfide residue, oxidation and reduction reactions between Fe³⁺ and S^2- occur firstly, which is followed by oxidation and reduction reactions of As⁵⁺ and S^2-, and finally a sulfurization reaction for precipitation of Cu²⁺. When the addition of arsenic sulfide residue is at an amount of 1.4 times the theoretical amount, it is shown that the copper precipitation rate is relatively higher, but the rate of arsenic dissolution is lower.

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针对高硫酸浓度且铁、砷以高价态Fe³⁺、As⁵⁺形式存在的酸浸液，采用硫化砷渣为沉铜剂沉铜。首先开展了不同酸浓度下单一Cu²⁺、Fe³⁺溶液中硫化砷渣加入量实验，在此基础上再进行了实际酸浸液沉铜、浸出砷实验。结果表明，采用硫化砷渣沉铜时，首先发生Fe³⁺与S^2-的氧化还原反应，其次是As⁵⁺与S^2-的氧化还原反应，最后是Cu²⁺的硫化沉淀反应；硫化砷渣加入量为理论量的1.4倍时，沉铜率较高，但砷溶出率较低。

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马云聪（1991—），男，湖南岳阳人，工程师，主要从事矿产资源湿法冶金资源回收利用研究。

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马云聪（1991—），男，湖南岳阳人，工程师，主要从事矿产资源湿法冶金资源回收利用研究。

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