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With Pr₆O₁₁ and CeO₂ as additives, B₄C matrix composite materials were prepared at 2 200 ℃, 1 900 ℃, and 1 700 ℃ by adopting techniques of pressureless sintering, hot pressing sintering, and spark plasma sintering, respectively. The relative microstructure and mechanical properties were also studied. It is found that PrB₆ and CeB₆ formed in situ can fill the pores between B₄C grains, and improve the density of the composites. Compared with pressureless sintering and hot pressing sintering, the technique of spark plasma sintering can bring the prepared composites with higher density. The fracture toughness of B₄C-CeB₆ composites can be improved due to its high relative density, as well as the deflection, branching and bridging of cracks occuring along CeB₆, which extends the expansion path of cracks and reduces stress concentration. The B₄C-CeB₆ composite prepared by spark plasma sintering has good comprehensive mechanical properties, with the relative density, vickers hardness, bending strength and fracture toughness reaching 99.3%, 34.7 GPa, 451 MPa and 4.38 MPa·m^1/2, respectively.

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分别以Pr₆O₁₁和CeO₂为添加剂，采用无压烧结、热压烧结和放电等离子烧结法分别在2 200 ℃、1 900 ℃和1 700 ℃制备了B₄C基复合材料，并对其微观结构和力学性能进行了研究。结果表明，通过原位反应形成的PrB₆和CeB₆可以填充B₄C晶粒之间的孔隙，提高复合材料的致密性；与无压烧结和热压烧结相比，放电等离子烧结制备的复合材料具有更高的致密性；B₄C-CeB₆复合材料断裂韧性得以提高的原因是实现了高致密以及裂纹沿着CeB₆发生了偏转、分枝和桥联，最终延长了裂纹的扩展路径，降低了应力集中。采用放电等离子烧结制备的B₄C-CeB₆复合材料综合力学性能较好，相对密度、维氏硬度、抗弯强度和断裂韧性分别达到了99.3%、34.7 GPa、451 MPa和4.38 MPa·m^1/2。

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黄樱（1982—），女，河南郑州人，副教授，硕士研究生，主要从事汽车技术服务与营销、汽车检测与维修技术研究。

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黄樱（1982—），女，河南郑州人，副教授，硕士研究生，主要从事汽车技术服务与营销、汽车检测与维修技术研究。

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