Article(id=1236333413146358776, tenantId=1146029695717560320, journalId=1235980550691926019, issueId=1236333405122646435, articleNumber=null, orderNo=null, doi=10.3969/j.issn.0253-6099.2023.01.024, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1662048000000, receivedDateStr=2022-09-02, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1772694455657, onlineDateStr=2026-03-05, pubDate=1675180800000, pubDateStr=2023-02-01, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1772694455657, onlineIssueDateStr=2026-03-05, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1772694455657, creator=13701087609, updateTime=1772694455657, updator=13701087609, issue=Issue{id=1236333405122646435, tenantId=1146029695717560320, journalId=1235980550691926019, year='2023', volume='43', issue='1', pageStart='1', pageEnd='159', issueExtLink='null', onlineDate='null', pubDate='null', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1772694453745, creator=13701087609, updateTime=1772694772892, updator=13701087609, preIssue=null, nextIssue=null, ext={EN=IssueExt(id=1236334743785099547, tenantId=1146029695717560320, journalId=1235980550691926019, issueId=1236333405122646435, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1236334743785099548, tenantId=1146029695717560320, journalId=1235980550691926019, issueId=1236333405122646435, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null}, startPage=110, endPage=113, ext={EN=ArticleExt(id=1236333413515456514, articleId=1236333413146358776, tenantId=1146029695717560320, journalId=1235980550691926019, language=EN, title=Leaching of Intermediate of Nickel Hydroxide with Synergetic Effect of Nickel Sulfide, columnId=1236276106727321817, journalTitle=Mining and Metallurgical Engineering, columnName=METALLURGY, runingTitle=null, highlight=null, articleAbstract=

Research on redox leaching of intermediate of nickel hydroxide with synergetic effect of nickel sulfide was carried out, and optimum leaching conditions were obtained from tests, including intermediates of nickel sulfide and nickel hydroxide in a mass ratio of 1/10, initial acidity of 4 mol/L, temperature of 90 ℃, liquid and solid in a ratio of 2.0, and a reaction time of 5 h. Under such conditions, the leaching rate of manganese from nickel hydroxide can reach 99.88% and the utilization rate of nickel sulfide is also up to 79.50%. And the leaching residue can be returned as a reducing agent in the reduction and leaching of nickel hydroxide. By using this method, the consumption of both the reducing agent in leaching of nickel hydroxide and the oxidizing agent in leaching of nickel sulfide can be greatly reduced. In addition, the leaching of intermediate of nickel hydroxide can be achieved with synergetic effect of nickel sulfide, which is easy to operate and can be applied into industrial production.

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研究了氢氧化镍中间品和硫化镍中间品联合氧化还原浸出，得到适宜的浸出条件为：硫化镍中间品与氢氧化镍中间品质量比1/10、反应初始酸度4 mol/L、反应温度90 ℃、反应液固比2.0、反应时间5 h，此条件下氢氧化镍中间品中锰浸出率和硫化镍中间品利用率分别达到99.88%和79.50%，浸出渣可以返回继续还原浸出氢氧化镍中间品。该方法避免了氢氧化镍中间品单独浸出的还原剂消耗和硫化镍中间品单独浸出的氧化剂消耗，实现了氢氧化镍中间品和硫化镍中间品协同浸出，且操作简便，适于工业生产应用。

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付海阔（1984—），男，河南杞县人，硕士，高级工程师，主要研究方向为镍钴湿法冶炼。

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付海阔（1984—），男，河南杞县人，硕士，高级工程师，主要研究方向为镍钴湿法冶炼。

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