Article(id=1236330611611325327, tenantId=1146029695717560320, journalId=1235980550691926019, issueId=1236330603000418795, articleNumber=null, orderNo=null, doi=10.3969/j.issn.0253-6099.2023.04.027, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1677168000000, receivedDateStr=2023-02-24, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1772693787720, onlineDateStr=2026-03-05, pubDate=1690819200000, pubDateStr=2023-08-01, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1772693787720, onlineIssueDateStr=2026-03-05, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1772693787720, creator=13701087609, updateTime=1772693787720, updator=13701087609, issue=Issue{id=1236330603000418795, tenantId=1146029695717560320, journalId=1235980550691926019, year='2023', volume='43', issue='4', pageStart='1', pageEnd='189', issueExtLink='null', onlineDate='null', pubDate='null', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1772693785667, creator=13701087609, updateTime=1772696855253, updator=13701087609, preIssue=null, nextIssue=null, ext={EN=IssueExt(id=1236343477835985022, tenantId=1146029695717560320, journalId=1235980550691926019, issueId=1236330603000418795, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1236343477835985023, tenantId=1146029695717560320, journalId=1235980550691926019, issueId=1236330603000418795, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null}, startPage=125, endPage=130, ext={EN=ArticleExt(id=1236330611900732325, articleId=1236330611611325327, tenantId=1146029695717560320, journalId=1235980550691926019, language=EN, title=Recovery of Antimony and Alkali from Arsenic-Alkali Slag and Solidification of Arsenic, columnId=1236276106727321817, journalTitle=Mining and Metallurgical Engineering, columnName=METALLURGY, runingTitle=null, highlight=null, articleAbstract=

In order to achieve utilization of antimony and alkali in arsenic-alkali slag and solidification of arsenic, a new processing technique, consisting of separation antimony by water leaching, arsenic precipitation by hydrothermal reaction with lime, and alkali extraction by evaporation, was proposed to treat arsenic-alkali slag. Results show that water leaching at 90 ℃ for 5 h with liquid-solid ratio of 3∶1 can result in the leaching rate of arsenic up to 97.96% and the leaching rate of antimony just 0.72%. The obtained leaching residue only contains 0.09% arsenic, presenting effective separation between antimony and arsenic. With calcium and arsenic in a molar ratio of 1.43, hydrothermal reaction at 170 ℃ for 2 h can lead to an arsenic precipitation rate up to 99.68% and the solution after precipitation with arsenic and alkali in a mass ratio of 1.65‰, also presenting a good separation effect. Finally, the concentration and crystallization process by evaporation can generate crystalized alkali containing only 0.14‰ arsenic, which can meet the technical requirement for alkali in antimony refining.

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为实现砷碱渣中锑、碱的资源化和砷的固化，采用水浸分锑-水热石灰沉砷-浓缩结晶提碱工艺处理砷碱渣。结果表明，在浸出温度90 ℃、浸出液固比3∶1、浸出时间5 h条件下水浸，砷浸出率达到97.96%，锑浸出率仅为0.72%，所得浸出渣含砷量仅为0.09%，实现了锑与砷、碱的有效分离；在钙和砷物质的量比1.43、反应温度170 ℃、反应时间2 h条件下沉砷，砷沉淀率达到99.68%，沉砷后液砷碱质量比仅为1.65∶1 000，砷、碱分离效果优异；利用浓缩结晶法，可获得砷含量0.14‰的结晶碱，满足锑精炼用碱的技术要求。

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康东升（1973—），男，湖南新化人，工程师，主要从事锑、锌清洁冶炼技术研究。

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康东升（1973—），男，湖南新化人，工程师，主要从事锑、锌清洁冶炼技术研究。

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