Article(id=1236330606846603596, tenantId=1146029695717560320, journalId=1235980550691926019, issueId=1236330603000418795, articleNumber=null, orderNo=null, doi=10.3969/j.issn.0253-6099.2023.04.032, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1676217600000, receivedDateStr=2023-02-13, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1772693786583, onlineDateStr=2026-03-05, pubDate=1690819200000, pubDateStr=2023-08-01, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1772693786583, onlineIssueDateStr=2026-03-05, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1772693786583, creator=13701087609, updateTime=1772693786583, updator=13701087609, issue=Issue{id=1236330603000418795, tenantId=1146029695717560320, journalId=1235980550691926019, year='2023', volume='43', issue='4', pageStart='1', pageEnd='189', issueExtLink='null', onlineDate='null', pubDate='null', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1772693785667, creator=13701087609, updateTime=1772696855253, updator=13701087609, preIssue=null, nextIssue=null, ext={EN=IssueExt(id=1236343477835985022, tenantId=1146029695717560320, journalId=1235980550691926019, issueId=1236330603000418795, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1236343477835985023, tenantId=1146029695717560320, journalId=1235980550691926019, issueId=1236330603000418795, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null}, startPage=147, endPage=153, ext={EN=ArticleExt(id=1236330607274422625, articleId=1236330606846603596, tenantId=1146029695717560320, journalId=1235980550691926019, language=EN, title=Preparation of Anode Material with Fine Flake Graphite from Inner Mongolia, columnId=1236276108207902848, journalTitle=Mining and Metallurgical Engineering, columnName=MATERIALS, runingTitle=null, highlight=null, articleAbstract=

A kind of flake graphite with grain size D₅₀ of 40.3 μm from Inner Mongolia was taken in a spherification test by adopting a QCJ vortex micropulverizer, and two kinds of spherical products with D₅₀ of 16.42 μm and 11.68 μm respectively were obtained, of which the corresponding tapped density increased from 0.46 g/cm³ to 0.95 g/cm³ and 0.80 g/cm³ respectively, presenting a total spherification rate of 50.48%. The spherical products were purified with mixed acid, with the fixed carbon content therein up to 99.95% and 99.97% respectively, and then the electrochemical performance of the products was tested. The anode material with those two products delivered initial discharge specific capacities of 366.60 mAh/g and 364.30 mAh/g, respectively, and presented initial charge-discharge efficiency of 93.40% and 92.32%, respectively. It is shown that the capacity retention rate can exceed 99% after 30 cycles at 0.1C current.

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采用QCJ气流涡旋微粉机对内蒙古某D₅₀为40.3 μm的微细鳞片石墨进行球形化试验，得到D₅₀分别为16.42 μm和11.68 μm的2种球形化产品，对应的振实密度由原始的0.46 g/cm³分别提高到0.95 g/cm³和0.80 g/cm³，总成球率50.48%。采用混酸法将该球形产品提纯至固定碳含量99.95%与99.97%，随后进行电化学性能测试，产品负极材料首次放电容量分别为366.60 mAh/g和364.30 mAh/g，首次充放电效率分别为93.40%和92.32%；在0.1C电流下，经过30次充放电循环后，容量保持率均在99%以上。

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张宇（1997—），男，山东菏泽人，硕士研究生，主要研究方向为非金属矿选矿提纯及深加工。

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张宇（1997—），男，山东菏泽人，硕士研究生，主要研究方向为非金属矿选矿提纯及深加工。

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