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The out-of-life saggar after repeated use for LiCoO₂ sintering in industry was taken to explore its erosion mechanism during high temperature synthesis of LiCoO₂ by adopting fluorescence analysis, chemical composition analysis, X-ray diffraction analysis, microstructure and energy spectrum analysis. Results show that when saggar is used to hold basic cobalt carbonate and lithium carbonate and calcined at 950 ℃ for 15 h, it is eroded and damaged after 15 times of operation. During LiCoO₂ synthesis, saggar is mainly eroded by lithium ions, with the dominant erosion products including tetragonal LiAlO_2, α-LiAlO_2, LiAlSiO_4, Li₃AlSiO₅ and Li_3.17Si_0.7S_0.3O_4. Cobalt ions are not involved in the chemical erosion but the synthesized lithium cobalt compounds migrate along the pores and also deposit along the migrating pores of saggar.

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以工业上用于烧结合成LiCoO₂、经反复多次使用报废的匣钵为研究对象，通过荧光分析、化学成分分析、物相分析、微观结构以及能谱分析等研究了LiCoO₂高温合成过程对匣钵的侵蚀机理。结果表明，用于盛装碱式碳酸钴和碳酸锂并在950 ℃下煅烧15 h的匣钵在使用15次后发生侵蚀损毁，在LiCoO₂合成过程中，对匣钵的侵蚀主要为锂离子侵蚀，侵蚀产物主要有四方晶系LiAlO₂、α-LiAlO₂、LiAlSiO₄、Li₃AlSiO₅和Li_3.17Si_0.7S_0.3O₄；钴离子不参与侵蚀反应，但合成的锂钴化合物会沿着匣钵的孔道进行迁移，并沿着迁移孔道沉积。

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张丽芬（1983—），女，广东清远人，硕士，高级工程师，主要从事有色金属冶金及固废资源回收研究。

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张丽芬（1983—），女，广东清远人，硕士，高级工程师，主要从事有色金属冶金及固废资源回收研究。

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