Article(id=1236319267805778737, tenantId=1146029695717560320, journalId=1235980550691926019, issueId=1236316193171239730, articleNumber=null, orderNo=null, doi=10.3969/j.issn.0253-6099.2023.03.014, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1670774400000, receivedDateStr=2022-12-12, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1772691083146, onlineDateStr=2026-03-05, pubDate=1685548800000, pubDateStr=2023-06-01, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1772691083146, onlineIssueDateStr=2026-03-05, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1772691083146, creator=13701087609, updateTime=1772691083146, updator=13701087609, issue=Issue{id=1236316193171239730, tenantId=1146029695717560320, journalId=1235980550691926019, year='2023', volume='43', issue='3', pageStart='1', pageEnd='179', issueExtLink='null', onlineDate='null', pubDate='null', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1772690350096, creator=13701087609, updateTime=1772691872061, updator=13701087609, preIssue=null, nextIssue=null, ext={EN=IssueExt(id=1236322576809652696, tenantId=1146029695717560320, journalId=1235980550691926019, issueId=1236316193171239730, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1236322576809652697, tenantId=1146029695717560320, journalId=1235980550691926019, issueId=1236316193171239730, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null}, startPage=61, endPage=66, ext={EN=ArticleExt(id=1236319268053242688, articleId=1236319267805778737, tenantId=1146029695717560320, journalId=1235980550691926019, language=EN, title=Treatment of Butyl Xanthate Wastewater with Chalcopyrite Activated Persulfate, columnId=1236276106932842717, journalTitle=Mining and Metallurgical Engineering, columnName=MINERAL PROCESSING, runingTitle=null, highlight=null, articleAbstract=

Natural chalcopyrite (CuFeS₂) was used as a catalyst to activate persulfate (PS) for butyl xanthate wastewater treatment. The influences of CuFeS₂ dosage, PS dosage and initial pH of solution on the removal rate of butyl xanthate in CuFeS₂/PS system were investigated, and the recyclability of CuFeS₂ was also evaluated. The results show that CuFeS₂ can significantly activate PS. After 10 min reaction with initial pH of 3, CuFeS₂ dosage of 4 g/L and PS dosage of 5 mmol/L, the removal rate of butyl xanthate reached 99.23%, while the removal rate of total organic carbon (TOC) was only 31.29%. After the reaction time was extended to 60 min, the TOC removal rate reached 68.31%, and CuFeS₂ still sustained good catalytic activity after being recycled for five times. The UV-Visible absorption spectra of butyl xanthate wastewater degradation showed that butyl xanthate was initially oxidized to alcohols, then decomposed and mineralized to carbon dioxide and water. X-ray diffraction and fourier transform infra-red spectroscopy analysis showed that CuFeS₂ reacted with PS without surface passivation, thus could be reused. A free radical quenching test and an electron spin resonance analysis showed that the removal mechanism of xanthate included free radical degradation and CuFeS₂ physisorption, in which sulfate radical (SO₄^-·) and hydroxyl radical (HO·) were the main active substances to promote xanthate degradation, and the SO₄^-· played a dominant role.

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以天然黄铜矿（CuFeS₂）作为催化剂活化过硫酸盐（PS）处理丁基黄药废水，考察了CuFeS₂用量、PS用量和溶液初始pH值对CuFeS₂/PS体系中丁基黄药去除率的影响，并对CuFeS₂可重复利用性进行了评价。结果表明，CuFeS₂对PS有显著的活化作用，在CuFeS₂用量4 g/L、PS用量5 mmol/L、溶液初始pH=3条件下反应10 min，丁基黄药去除率达99.23%，TOC去除率仅31.29%；继续增加反应时间至60 min，TOC去除率达到68.31%，且CuFeS₂重复利用5次后仍有较好的催化活性。丁基黄药废水降解过程的紫外-可见吸收光谱研究结果表明，丁基黄药首先被氧化为醇类有机物，后被分解矿化为二氧化碳和水。XRD和FTIR分析结果表明，CuFeS₂与PS反应后表面没有发生钝化，可重复利用。自由基猝灭试验和电子自旋共振分析（ESR）结果表明，黄药的去除机理包括自由基的化学降解作用和CuFeS₂的物理吸附作用，其中，硫酸根自由基（SO₄^-·）和羟基自由基（HO·）是促使黄药降解的主要活性物质，且SO₄^-·起主导作用。

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文晓飞（1997—），男，陕西宝鸡人，硕士研究生，主要研究方向为硫化矿浮选分离、二次资源回收利用等。

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文晓飞（1997—），男，陕西宝鸡人，硕士研究生，主要研究方向为硫化矿浮选分离、二次资源回收利用等。

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