Article(id=1236319265322758820, tenantId=1146029695717560320, journalId=1235980550691926019, issueId=1236316193171239730, articleNumber=null, orderNo=null, doi=10.3969/j.issn.0253-6099.2023.03.023, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1670601600000, receivedDateStr=2022-12-10, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1772691082553, onlineDateStr=2026-03-05, pubDate=1685548800000, pubDateStr=2023-06-01, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1772691082553, onlineIssueDateStr=2026-03-05, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1772691082553, creator=13701087609, updateTime=1772691082553, updator=13701087609, issue=Issue{id=1236316193171239730, tenantId=1146029695717560320, journalId=1235980550691926019, year='2023', volume='43', issue='3', pageStart='1', pageEnd='179', issueExtLink='null', onlineDate='null', pubDate='null', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1772690350096, creator=13701087609, updateTime=1772691872061, updator=13701087609, preIssue=null, nextIssue=null, ext={EN=IssueExt(id=1236322576809652696, tenantId=1146029695717560320, journalId=1235980550691926019, issueId=1236316193171239730, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1236322576809652697, tenantId=1146029695717560320, journalId=1235980550691926019, issueId=1236316193171239730, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null}, startPage=101, endPage=105, ext={EN=ArticleExt(id=1236319266572661443, articleId=1236319265322758820, tenantId=1146029695717560320, journalId=1235980550691926019, language=EN, title=Experimental Study on Purification of Crude Lithium Phosphate from Salt Lake, columnId=1236276106727321817, journalTitle=Mining and Metallurgical Engineering, columnName=METALLURGY, runingTitle=null, highlight=null, articleAbstract=

With sodium oxalate and D401 chelating resin as impurity removal materials, impurities of calcium and magnesium in crude lithium solution were removed by adopting a process consisting of chemical precipitation and ion exchange. In an experiment, reaction was firstly run at 25 ℃ for 60 min by adding sodium oxalate at an amount of 17.6 times the theoretical value, with pH of 6.5 and stirring rate of 300 r/min. And then, the lithium solution after filtration flowed through a resin column at a rate of 8 BV/h. As a result, the removal rates of calcium and magnesium reached 98.21% and 83.36%, respectively, and the lithium loss rate was 5.34%. The purified lithium solution was then recrystallized and purified, and the obtained lithium phosphate powder, with regular morphology and uniform dispersion, has its purity higher than 99.5%.

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以草酸钠、D401螯合树脂为除杂材料，采用化学沉淀-离子交换工艺去除粗制磷酸锂溶液中的钙、镁杂质。结果表明，在草酸钠使用量为理论用量的17.6倍、pH值6.5、反应温度25 ℃、搅拌速率300 r/min、反应时间60 min、过滤后锂溶液以8 BV/h的流速通过树脂柱条件下，钙、镁杂质去除率分别达到98.21%、83.36%，锂损失率为5.34%；除杂后的锂溶液经再结晶并纯化后，得到形貌规整、分散均匀、纯度大于99.5%的磷酸锂粉体。

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朱军（1963—），男，山东烟台人，博士，教授，主要从事冶金资源综合利用研究。

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朱军（1963—），男，山东烟台人，博士，教授，主要从事冶金资源综合利用研究。

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