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To enhance the rate capability and cycling stability of the high-voltage cathode material LiNi_0.5 Mn_1.5O₄ (LNMO), a V-Y co-doped LNMO cathode material was synthesized via the polymer soft-template method. The effects of V-Y co-doping on crystal structure, interfacial properties, and electrochemical performance were systematically investigated. The material was characterized by X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDS) among other techniques, and the electrochemical properties were analyzed via galvanostatic charge-discharge, cyclic voltammetry (CV), and electrochemical impedance spectroscopy (EIS). The results indicate that V-Y co-doping induces the formation of disordered Fd3m phase by effectively regulating LNMO, facilitates the morphology evolution of spinel from regular octahedron to truncated octahedron, and constructs a coherent interface, which significantly enhances the lithium-ion diffusion rate and electronic conductivity. Moreover, V-Y co-doping reduces the Mn³⁺content, suppresses Jahn-Teller effect and side reactions at the electrode/electrolyte interface, thereby enhancing the interfacial electrochemical stability. The 0.03V-Y sample (LiV_0.03 Ni_0.47 Y_0.01 Mn_1.49O₄) delivers an initial discharge capacity of 132 mAh/g at a 0.1C rate, retaining 94.7% of its capacity after 200 cycles. It also exhibits superior rate capability at a high rate of 5C. This study provides a novel approach for constructing a coherent interface and synergistically optimizing the electrochemical performance of LNMO via dual-element doping.

, authors=Zhende HUANG¹, Di PENG¹, Zhihang CHEN², authorsList=Zhende HUANG, Di PENG, Zhihang CHEN, authorCompany=null, correspAuthors=Di PENG, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1314908220632695490, articleId=1314908220100018880, tenantId=1146029695717560320, journalId=1235980550691926019, language=CN, title=V-Y共掺杂构建LiNi_0.5Mn_1.5O₄共格界面及其对电化学性能的影响, columnId=1236276110049202322, journalTitle=矿冶工程杂志, columnName=材料, runingTitle=null, highlight=null, articleAbstract=

为提升高电压正极材料LiNi_0.5Mn_1.5O₄（LNMO）的倍率性能与循环稳定性，采用高分子软模板法合成V-Y共掺杂LNMO正极材料，系统研究V、Y元素共掺杂对晶体结构、界面特性及电化学性能的影响。通过XRD、FTIR、SEM、EDS等手段表征材料结构，结合恒电流充放电、循环伏安（CV）和交流阻抗（EIS）等电化学测试分析其性能。结果表明，V-Y共掺杂有效调控LNMO形成无序Fd3m相，促进尖晶石由正八面体向截角八面体转变，形成共格界面，显著提升Li⁺扩散速率与电子电导率；V-Y共掺杂降低Mn³⁺含量，抑制Jahn-Teller效应及电极/电解液界面副反应，增强界面电化学稳定性。0.03V-Y样品（LiV_0.03Ni_0.47Y_0.01Mn_1.49O₄）在0.1C倍率下首次放电比容量达132 mAh/g，循环200次后容量保持率高达94.7%，在5C大倍率下仍表现出优异的倍率性能。本研究为通过双元素掺杂构建共格界面和协同优化LNMO电化学性能提供了新思路。

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黄振德（1976—），男，广西南宁人，副教授，主要研究方向为高能锂离子电池正极材料。E-mail: gxgyyhzd@163.com

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黄振德（1976—），男，广西南宁人，副教授，主要研究方向为高能锂离子电池正极材料。E-mail: gxgyyhzd@163.com

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