Article(id=1314908097848640432, tenantId=1146029695717560320, journalId=1235980550691926019, issueId=1314907935172551117, articleNumber=null, orderNo=null, doi=10.3969/j.issn.0253-6099.2026.03.035, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1763568000000, receivedDateStr=2025-11-20, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1791428120338, onlineDateStr=2026-10-08, pubDate=null, pubDateStr=null, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1791428120338, onlineIssueDateStr=2026-10-08, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1791428120338, creator=13701087609, updateTime=1791428120338, updator=13701087609, issue=Issue{id=1314907935172551117, tenantId=1146029695717560320, journalId=1235980550691926019, year='2026', volume='46', issue='3', pageStart='1', pageEnd='297', issueExtLink='null', onlineDate='null', pubDate='1780243200000', pubDateStr='2026-06-01', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1791428081553, creator='13701087609', updateTime=1791430444568, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1314917846770082179, tenantId=1146029695717560320, journalId=1235980550691926019, issueId=1314907935172551117, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1314917846770082180, tenantId=1146029695717560320, journalId=1235980550691926019, issueId=1314907935172551117, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=232, endPage=237, ext={EN=ArticleExt(id=1314908098154824625, articleId=1314908097848640432, tenantId=1146029695717560320, journalId=1235980550691926019, language=EN, title=Comparison Between Electrolytic Reduction and Lithothermal Reduction of Antimony Oxide in Molten Lithium Chloride, columnId=1236276106727321817, journalTitle=Mining and Metallurgical Engineering, columnName=METALLURGY, runingTitle=null, highlight=null, articleAbstract=

To explore the reduction process of antimony oxide（Sb₂O₃）in high-temperature molten lithium chloride, Sb₂O₃ was reduced to metallic antimony by electrolytic reduction and lithothermal reduction process respectively. The phase structure of products was analyzed by XRD, and electrochemical signals of Sb₂O₃ powder were accurately measured using molybdenum cavity electrode. Based on thermodynamic analysis and E-pO^2-diagrams, it is confirmed that Sb₂O₃ can be effectively reduced by electrolysis, yielding metallic Sb at potentials below 1.65 V (vs. Li/Li⁺). With a potential of 0.94 V (vs. Li/Li⁺) and electrolysis duration of 6 h, the antimony reduction rate can reach 82.0%. The conditions for lithium thermal reduction are as follows:metallic lithium is added at the theoretical dosage, reaction temperature of 923 K, and reaction time of 6 h. And the antimony reduction rate can reach 77.0% under these conditions.

, authors=Guangzhi REN, Jitang XU, Benlin YAO, Yiqun XIAO, Yanhong JIA, Hui CHEN, Zhenfang SHEN, Bin LI, Hui HE, Jia LI, authorsList=Guangzhi REN, Jitang XU, Benlin YAO, Yiqun XIAO, Yanhong JIA, Hui CHEN, Zhenfang SHEN, Bin LI, Hui HE, Jia LI, authorCompany=null, correspAuthors=Benlin YAO, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1314908098511340466, articleId=1314908097848640432, tenantId=1146029695717560320, journalId=1235980550691926019, language=CN, title=熔融氯化锂中氧化锑的电解还原与锂热还原比较, columnId=1236276107322913000, journalTitle=矿冶工程杂志, columnName=冶金, runingTitle=null, highlight=null, articleAbstract=

为了探索氧化锑（Sb₂O₃）在高温氯化锂熔盐中的还原过程，采用电解还原技术和锂热还原法将Sb₂O₃还原为Sb，并通过XRD对产物结构进行了表征。通过金属钼空腔电极准确测定了氧化锑粉末的电化学信号，结合热力学分析和E-pO^2-图，发现Sb₂O₃可以通过电解的方式被还原，实验中控制电位低于1.65 V（vs. Li/Li⁺）可以获得金属单质Sb，电位0.94 V（vs. Li/Li⁺）、电解时间6 h条件下，锑还原率可达82.0%。锂热还原条件为：Li金属加入量为理论用量、反应温度923 K、反应时间6 h，在此条件下，锑还原率可达77.0%。

, authors=任广治, 徐纪瑭, 姚本林, 肖益群, 贾艳虹, 陈辉, 沈振芳, 李斌, 何辉, 李佳, authorsList=任广治, 徐纪瑭, 姚本林, 肖益群, 贾艳虹, 陈辉, 沈振芳, 李斌, 何辉, 李佳, authorCompany=null, correspAuthors=姚本林, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=8ViNrjnDt/PHxGBKFRRP5A==, magXml=hh5k2SjEYDKIhHZtSKqtWw==, pdfUrl=null, pdf=/SZJc9cEVICqmuCwh6tRFg==, pdfFileSize=958301, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=em1Cl2r7BoKrbWHB8ZjjCg==, mapNumber=null, fund=null)}, authors=[Author(id=1314908098859467703, tenantId=1146029695717560320, journalId=1235980550691926019, articleId=1314908097848640432, orderNo=0, firstName=null, middleName=null, lastName=null, nameCn=null, orcid=null, stid=null, country=null, authorPic=null, dead=0, email=renguangzhi@cnncmail.cn, emailSecond=null, emailThird=null, correspondingAuthor=0, authorType=1, ext={EN=AuthorExt(id=1314908100683989946, tenantId=1146029695717560320, journalId=1235980550691926019, articleId=1314908097848640432, authorId=1314908098859467703, language=EN, stringName=Guangzhi REN, firstName=Guangzhi, middleName=null, lastName=REN, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=null, address=Department of Radiochemistry, China Institute of Atomic Energy, Beijing 102413, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1314908100784653244, tenantId=1146029695717560320, journalId=1235980550691926019, articleId=1314908097848640432, authorId=1314908098859467703, language=CN, stringName=任广治, firstName=null, middleName=null, lastName=null, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=null, address=中国原子能科学研究院 放射化学研究所，北京 102413, bio={"content":"

任广治（1993—），男，河北沧州人，博士，助理研究员，主要从事乏燃料干法后处理工作。E-mail: renguangzhi@cnncmail.cn

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任广治（1993—），男，河北沧州人，博士，助理研究员，主要从事乏燃料干法后处理工作。E-mail: renguangzhi@cnncmail.cn

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