Article(id=1314907973437186648, tenantId=1146029695717560320, journalId=1235980550691926019, issueId=1314907935172551117, articleNumber=null, orderNo=null, doi=10.3969/j.issn.0253-6099.2026.03.030, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1766160000000, receivedDateStr=2025-12-20, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1791428090675, onlineDateStr=2026-10-08, pubDate=null, pubDateStr=null, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1791428090675, onlineIssueDateStr=2026-10-08, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1791428090675, creator=13701087609, updateTime=1791428090675, updator=13701087609, issue=Issue{id=1314907935172551117, tenantId=1146029695717560320, journalId=1235980550691926019, year='2026', volume='46', issue='3', pageStart='1', pageEnd='297', issueExtLink='null', onlineDate='null', pubDate='1780243200000', pubDateStr='2026-06-01', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1791428081553, creator='13701087609', updateTime=1791430444568, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1314917846770082179, tenantId=1146029695717560320, journalId=1235980550691926019, issueId=1314907935172551117, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1314917846770082180, tenantId=1146029695717560320, journalId=1235980550691926019, issueId=1314907935172551117, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=204, endPage=209, ext={EN=ArticleExt(id=1314907975018439258, articleId=1314907973437186648, tenantId=1146029695717560320, journalId=1235980550691926019, language=EN, title=Evaluation of Measurement Uncertainty in Determining Gold Content in Gold Ore by Atomic Absorption Spectrometry, columnId=1236276106727321817, journalTitle=Mining and Metallurgical Engineering, columnName=METALLURGY, runingTitle=null, highlight=null, articleAbstract=

In accordance with GB/T 20899.1-2019, a mathematical model was established to analyze and calculate uncertainties from various sources in determining gold content in gold ores by fire assay combined with atomic absorption spectroscopy. Based on the combined calculation, it is shown that when the gold content of the ore samples is 2.28 g/t, the standard uncertainty of this method is 0.04 g/t, and with a coverage factor k = 2, the expanded uncertainty is 0.08 g/t. Comparison of uncertainty contributions indicates that repeatability of sample measurement and standard curve fitting are the major influencing factors. Therefore, it is recommended that measuring instruments should be kept in optimal condition, and the number of replicate measurements be increased to reduce measurement uncertainty.

, authors=Bin XU1, Chunyan LIU2, Binghong YANG1, Ying PENG1, Yanhua LIU1, Lin YANG1, Zhiyong ZHANG3, authorsList=Bin XU, Chunyan LIU, Binghong YANG, Ying PENG, Yanhua LIU, Lin YANG, Zhiyong ZHANG, authorCompany=null, correspAuthors=Zhiyong ZHANG, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1314907976310284891, articleId=1314907973437186648, tenantId=1146029695717560320, journalId=1235980550691926019, language=CN, title=原子吸收光谱法测定金矿石中金含量的测量不确定度评定, columnId=1236276107322913000, journalTitle=矿冶工程杂志, columnName=冶金, runingTitle=null, highlight=null, articleAbstract=

依据GB/T 20899.1—2019标准,针对火试金-原子吸收光谱技术测定金矿石中金含量的试验,通过构建数学模型,分析并计算了多种来源的测量不确定度。经过合成计算,当金矿石的金含量为2.28 g/t时,该方法的标准不确定度为0.04 g/t,包含因子k为2时,扩展不确定度为0.08 g/t。通过对比各来源的不确定度发现,样品重复性测量、标准曲线拟合对不确定度结果的影响较大。因此,建议确保测量仪器处于较佳状态,并增加重复测量次数,以降低测量不确定度。

, authors=许彬1, 刘春艳2, 杨炳红1, 彭颖1, 刘艳花1, 杨林1, 张志勇3, authorsList=许彬, 刘春艳, 杨炳红, 彭颖, 刘艳花, 杨林, 张志勇, authorCompany=null, correspAuthors=张志勇, authorNote=

许彬(1982—),女,湖南华容人,高级工程师,主要从事矿物化学成分分析、化学物相分析。E-mail:

, correspAuthorsNote=
张志勇(1979—),男,湖南茶陵人,博士,正高级工程师,主要研究方向为岩矿与冶金材料分析测试、矿物资源综合利用。E-mail:
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许彬(1982—),女,湖南华容人,高级工程师,主要从事矿物化学成分分析、化学物相分析。E-mail:

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许彬(1982—),女,湖南华容人,高级工程师,主要从事矿物化学成分分析、化学物相分析。E-mail:

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原子吸收光谱法测定金矿石中金含量的测量不确定度评定
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许彬 1 , 刘春艳 2 , 杨炳红 1 , 彭颖 1 , 刘艳花 1 , 杨林 1 , 张志勇 3
矿冶工程杂志 | 冶金 2026,46(3): 204-209
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矿冶工程杂志 |冶金 2026 , 46 (3) : 204 -209
原子吸收光谱法测定金矿石中金含量的测量不确定度评定
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许彬1 , 刘春艳2, 杨炳红1, 彭颖1, 刘艳花1, 杨林1, 张志勇3
作者信息
  • 1.长沙矿冶院检测技术有限责任公司,湖南 长沙 410012
  • 2.湖南化工职业技术学院,湖南 株洲 412000
  • 3.湖南安全技术职业学院,湖南 长沙 410151
通讯作者:
张志勇(1979—),男,湖南茶陵人,博士,正高级工程师,主要研究方向为岩矿与冶金材料分析测试、矿物资源综合利用。E-mail:
作者简介:

许彬(1982—),女,湖南华容人,高级工程师,主要从事矿物化学成分分析、化学物相分析。E-mail:

Evaluation of Measurement Uncertainty in Determining Gold Content in Gold Ore by Atomic Absorption Spectrometry
Bin XU1 , Chunyan LIU2, Binghong YANG1, Ying PENG1, Yanhua LIU1, Lin YANG1, Zhiyong ZHANG3
Affiliations
  • 1.Testing Technology Company of Changsha Research Institute of Mining and Metallurgy Co., Ltd., Changsha 410012, Hunan, China
  • 2.Hunan Chemical Vocational Technology College, Zhuzhou 412000, Hunan, China
  • 3.Hunan Vocational Institute of Safety Technology, Changsha 410151, Hunan, China
doi: 10.3969/j.issn.0253-6099.2026.03.030
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依据GB/T 20899.1—2019标准,针对火试金-原子吸收光谱技术测定金矿石中金含量的试验,通过构建数学模型,分析并计算了多种来源的测量不确定度。经过合成计算,当金矿石的金含量为2.28 g/t时,该方法的标准不确定度为0.04 g/t,包含因子k为2时,扩展不确定度为0.08 g/t。通过对比各来源的不确定度发现,样品重复性测量、标准曲线拟合对不确定度结果的影响较大。因此,建议确保测量仪器处于较佳状态,并增加重复测量次数,以降低测量不确定度。

原子吸收光谱  /  金矿石  /  金  /  不确定度  /  化学分析

In accordance with GB/T 20899.1-2019, a mathematical model was established to analyze and calculate uncertainties from various sources in determining gold content in gold ores by fire assay combined with atomic absorption spectroscopy. Based on the combined calculation, it is shown that when the gold content of the ore samples is 2.28 g/t, the standard uncertainty of this method is 0.04 g/t, and with a coverage factor k = 2, the expanded uncertainty is 0.08 g/t. Comparison of uncertainty contributions indicates that repeatability of sample measurement and standard curve fitting are the major influencing factors. Therefore, it is recommended that measuring instruments should be kept in optimal condition, and the number of replicate measurements be increased to reduce measurement uncertainty.

atomic absorption spectroscopy  /  gold ore  /  gold  /  uncertainty  /  chemical analysis
许彬, 刘春艳, 杨炳红, 彭颖, 刘艳花, 杨林, 张志勇. 原子吸收光谱法测定金矿石中金含量的测量不确定度评定. 矿冶工程杂志, 2026 , 46 (3) : 204 -209 . DOI: 10.3969/j.issn.0253-6099.2026.03.030
Bin XU, Chunyan LIU, Binghong YANG, Ying PENG, Yanhua LIU, Lin YANG, Zhiyong ZHANG. Evaluation of Measurement Uncertainty in Determining Gold Content in Gold Ore by Atomic Absorption Spectrometry[J]. Mining and Metallurgical Engineering, 2026 , 46 (3) : 204 -209 . DOI: 10.3969/j.issn.0253-6099.2026.03.030
  • 湖南省自然科学基金(2024JJ8042)
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doi: 10.3969/j.issn.0253-6099.2026.03.030
  • 接收时间:2025-12-20
  • 首发时间:2026-10-08
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  • 收稿日期:2025-12-20
基金
湖南省自然科学基金(2024JJ8042)
作者信息
    1.长沙矿冶院检测技术有限责任公司,湖南 长沙 410012
    2.湖南化工职业技术学院,湖南 株洲 412000
    3.湖南安全技术职业学院,湖南 长沙 410151

通讯作者:

张志勇(1979—),男,湖南茶陵人,博士,正高级工程师,主要研究方向为岩矿与冶金材料分析测试、矿物资源综合利用。E-mail:
参考文献
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2种不同金属材料的力学参数
科
Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)
属
Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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