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Spent lithium iron phosphate batteries were taken in a research on lithium extraction by selective leaching process and preparation of high-purity lithium phosphate. It is shown that by adopting a process consisting of leaching with sulfuric acid and hydrogen peroxide, neutralization for impurity removal, and precipitation with sodium phosphate, the lithium leaching rate can reach 98.07% and the iron leaching rate is just 0.28%, after leaching at room temperature with sulfuric acid at a concentration of 0.3 mol/L, hydrogen peroxide at a dosage of 0.50 mL/g, and liquid-solid ratio of 8 mL/g, showing that separation of lithium and iron can be actualized by selective leaching. Then, after the leachate is neutralized with sodium hydroxide for removing impurities, and subjected to precipitation process at a temperature of 90 ℃ for 60 min, with an initial pH of 10.5, sodium phosphate and lithium in a molar ratio of 1∶1, the lithium precipitation rate reaches 96.64%, and a high-purity lithium phosphate product with a lithium content of 16.16% is prepared. It is concluded that by adopting such process, lithium can be efficiently recovered from spent lithium iron phosphate batteries.

, authors=Zhan DONG^{1, 2, 3}, Lushuai YAO^{1, 2, 3}, Qianwen LI^{1, 2, 3}, Qing XIONG^{1, 2, 3}, Enhao LI^{1, 2, 3}, Huiyang LIN^{1, 2, 3}, Zishuai LIU^{1, 2, 3}, authorsList=Zhan DONG, Lushuai YAO, Qianwen LI, Qing XIONG, Enhao LI, Huiyang LIN, Zishuai LIU, authorCompany=null, correspAuthors=Zishuai LIU, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1314907212061967023, articleId=1314907211118248621, tenantId=1146029695717560320, journalId=1235980550691926019, language=CN, title=退役磷酸铁锂电池选择性浸出提锂及制备磷酸锂试验研究, columnId=1236276107322913000, journalTitle=矿冶工程杂志, columnName=冶金, runingTitle=null, highlight=null, articleAbstract=

以退役磷酸铁锂电池为研究对象，开展选择性浸出提锂及制备高纯磷酸锂的研究。结果表明，采用硫酸-过氧化氢浸出、中和除杂、磷酸钠沉淀的联合工艺，在硫酸浓度0.3 mol/L、过氧化氢用量0.50 mL/g、液固比8 mL/g、常温浸出条件下，锂浸出率达98.07%、铁浸出率仅0.28%，实现了锂和铁的选择性浸出分离；选择性浸出液经氢氧化钠中和除杂后，在沉淀初始pH=10.5、磷酸钠与锂物质的量比1∶1、沉淀温度90 ℃、沉淀时间60 min条件下，锂沉淀率为96.64%，并制备了锂含量16.16%的高纯磷酸锂产品，实现了退役磷酸铁锂电池中锂的高效回收。

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董战（2001—），男，江苏徐州人，硕士研究生，主要研究方向为锂钽铌等稀有金属综合回收。E-mail: 2303912011@qq.com

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董战（2001—），男，江苏徐州人，硕士研究生，主要研究方向为锂钽铌等稀有金属综合回收。E-mail: 2303912011@qq.com

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^2．江西理工大学资源与环境工程学院，江西 赣州 341000
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^2．江西理工大学资源与环境工程学院，江西 赣州 341000
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^2．江西理工大学资源与环境工程学院，江西 赣州 341000
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