Article(id=1199661549309756177, tenantId=1146029695717560320, journalId=1185652524569653253, issueId=1199661546335994621, articleNumber=1009-5438(2022)01-0039-05, orderNo=null, doi=null, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1637510400000, receivedDateStr=2021-11-22, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1763951201989, onlineDateStr=2025-11-24, pubDate=1645718400000, pubDateStr=2022-02-25, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1763951201989, onlineIssueDateStr=2025-11-24, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1763951201989, creator=13701087609, updateTime=1763951201989, updator=13701087609, issue=Issue{id=1199661546335994621, tenantId=1146029695717560320, journalId=1185652524569653253, year='2022', volume='48', issue='1', pageStart='1', pageEnd='98', issueExtLink='null', onlineDate='null', pubDate='null', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1763951201279, creator=13701087609, updateTime=1763959528511, updator=13701087609, preIssue=null, nextIssue=null, ext={EN=IssueExt(id=1199696473341391309, tenantId=1146029695717560320, journalId=1185652524569653253, issueId=1199661546335994621, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1199696473341391310, tenantId=1146029695717560320, journalId=1185652524569653253, issueId=1199661546335994621, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null}, startPage=39, endPage=43, ext={EN=ArticleExt(id=1199661549691437850, articleId=1199661549309756177, tenantId=1146029695717560320, journalId=1185652524569653253, language=EN, title=Study on High Power Hydrogen Storage Alloy Powder, columnId=1187340472918880861, journalTitle=Science & Technology of Baotou Steel, columnName=Production Practice and Management, runingTitle=null, highlight=null, articleAbstract=

In this paper, a kind of high power hydrogen storage alloy powder is studied, its components such as main elements of rare earth and nickel as well as auxiliary elements of Co, Mn, Al and Fe are analyzed by inductively coupled plasma (ICP), its texture is analyzed by X-Ray Diffraction (XRD) test and the platform pressure curve is analyzed by reaction with the hydrogen. Moreover, the high power hydrogen storage electrode alloy is developed by carrying out the tests of particle size and specific surface area for hydrogen storage alloy powder as well as analyzing the electrochemical characteristics of alloy electrode. It is determined to meet the requirements of high power and current for Ni-MH battery by constant power test of battery. The charge-discharge performance with high current of Ni-MH battery is realized by optimizing the preparation technology of cathode.

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文章研究了一种高功率储氢合金粉,通过ICP测试对合金粉的主要元素稀土和镍、辅助元素钴、锰、铝、铁等成分进行分析,通过XRD测试进行合金粉组织结构分析,通过与氢气反应进行平台压曲线分析;同时进行储氢合金粉粒度和比表面积测试,以及合金电极的电化学特性分析,开发了高功率储氢电极合金。通过电池恒功率测试确定该高功率储氢电极合金可满足镍氢电池对高功率大电流的要求。通过优化负极电极制备工艺,实现镍氢电池的大电流充放电性能。

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元素	试验设计要求	实际测量值
RE	30.0~34.0	32.2
Ni	58.0~61.0	59.7
Co	1.0~1.5	1.3
Mn	4.0~5.0	4.2
Al	1.0~1.5	1.2
Zr	0.3~0.5	0.36
Fe	≤0.1	0.003

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储氢合金元素含量标准要求(质量分数) %

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元素	试验设计要求	实际测量值
RE	30.0~34.0	32.2
Ni	58.0~61.0	59.7
Co	1.0~1.5	1.3
Mn	4.0~5.0	4.2
Al	1.0~1.5	1.2
Zr	0.3~0.5	0.36
Fe	≤0.1	0.003

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半峰宽	a/Å	c/Å	V/Å3
0.158	5.020 5	3.982 1	86.92

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XRD测试曲线数据

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半峰宽	a/Å	c/Å	V/Å3
0.158	5.020 5	3.982 1	86.92

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最大吸氢量Wmax /%	平台压力P /MPa	斜率F	滞后系数Hf
1.269	0.028	0.921 4	0.042 1

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PCT测试具体数据

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最大吸氢量Wmax /%	平台压力P /MPa	斜率F	滞后系数Hf
1.269	0.028	0.921 4	0.042 1

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粒度 型号	筛分粒度分布(质量分数)/%
	<0.106 mm	<0.075 mm	<0.053 mm	<0.038 mm
150型	≥90.0	60.0±5.0	33.0±5.0	<23.0
180型	≥92.0	63.0±5.0	38.0±5.0	25.0±2.0
200型	100.0	>95.0	66.0±5.0	45.0±3.0

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储氢合金粉筛分粒度分布

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粒度 型号	筛分粒度分布(质量分数)/%
	<0.106 mm	<0.075 mm	<0.053 mm	<0.038 mm
150型	≥90.0	60.0±5.0	33.0±5.0	<23.0
180型	≥92.0	63.0±5.0	38.0±5.0	25.0±2.0
200型	100.0	>95.0	66.0±5.0	45.0±3.0

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粒度型号	激光粒度分布/%
	D10	D50	D90
150型	22.0±2.0	64.0±5.0	145.0±10.0
180型	18.0±2.0	55.0±4.0	125.0±15.0
200型	12.0±2.0	35.0±2.0	75.0±4.0

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储氢合金粉激光粒度分布

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粒度型号	激光粒度分布/%
	D10	D50	D90
150型	22.0±2.0	64.0±5.0	145.0±10.0
180型	18.0±2.0	55.0±4.0	125.0±15.0
200型	12.0±2.0	35.0±2.0	75.0±4.0

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半电池	3C放电容量	5C放电容量	10C放电容量
常规合金粉半电池	252	146
高功率合金粉半电池	273	232	151

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半电池倍率放电对比表 mAh/g

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半电池	3C放电容量	5C放电容量	10C放电容量
常规合金粉半电池	252	146
高功率合金粉半电池	273	232	151

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