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2 Key Laboratory of Dairy Cattle Genetic, Breeding and Reproduction,Ministry of Agriculture and Rural Affairs,Beijing 100192;
3 Beijing Key Laboratory of Dairy Cattle Genetic, Breeding and Reproduction,Beijing 100192, correspAuthors=null, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1320063058131660871, articleId=1320063056307138630, tenantId=1146029695717560320, journalId=1296801528146919473, language=CN, title=测定牛奶和奶粉中甲基毒死蜱残留量的气相色谱串联质谱法研究, columnId=1297134032135938673, journalTitle=中国乳业, columnName=质量安全, runingTitle=null, highlight=null, articleAbstract=[目的]通过选取适宜的分析色谱柱,简化样品的前处理过程,选取合适的离子对进行监测,提高方法的灵敏度和准确度。[方法]测定样品平行性（精密度）、加标回收率（准确度）、方法检出限,对该检测方法进行验证。[结果]牛奶中添加甲基毒死蜱的回收率分别为105.3%、106.9%、108.2%,甲基毒死蜱在3 个添加水平上的变异系数分别为1.61%、3.06%、2.52%。奶粉中添加甲基毒死蜱的回收率分别为100.3%、89.8%、88.5%,甲基毒死蜱在3 个添加水平上的变异系数分别为2.14%、1.97%、1.82%。[结论]该方法精密度和准确度符合要求,可用于牛奶和奶粉中日常甲基毒死蜱残留的测定和质量控制。, authors=赵凤茹^1,2,3, 谢凯丽¹, 水明^1,2,3, 丛慧敏^1,2,3, 薛文强¹, 李琪琪¹, 代晶晶¹, 龙洋¹, 王婼依^1,2,3, authorsList=赵凤茹, 谢凯丽, 水明, 丛慧敏, 薛文强, 李琪琪, 代晶晶, 龙洋, 王婼依, authorCompany=1北京奶牛中心,北京 100192;
2农业农村部奶牛遗传育种与繁殖重点实验室,北京 100192;
3奶牛遗传育种与繁殖北京市重点实验室,北京 100192, correspAuthors=null, authorNote=赵凤茹（1971-）,女,北京人,硕士,高级畜牧师,研究方向为奶牛养殖与奶牛育种;谢凯丽（1993-）,女,北京人,本科,助理工程师,研究方向为乳品安全检测;水 明（1982-）,男,北京人,硕士,高级工程师,研究方向为乳品安全检测;丛慧敏（1976-）,女,山东巨野人,硕士,高级畜牧师,研究方向为奶牛养殖;薛文强（1997-）,男,河北定州人,本科,助理工程师,研究方向为乳及乳制品检测。李琪琪（1995-）,女,河北张家口人,大专,助理工程师,研究方向为乳品安全检测;代晶晶（1996-）,女,内蒙古巴彦淖尔人,本科,助理工程师,研究方向为乳品安全检测;龙 洋（1999-）,女,北京人,硕士,助理工程师,研究方向为乳品安全检测;王婼依（1994-）,女,内蒙古通辽人,本科,研究方向为奶牛育种。, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=fAB8WHLyVerj+xGQWzVBdA==, pdfFileSize=2341550, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=青年北京学者（NO.059）; 家畜产业技术体系北京市创新团队（BAIC05-2023）)}, authors=null, keywords=[Keyword(id=1320063058353958985, tenantId=1146029695717560320, 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