Article(id=1297139230396936405, tenantId=1146029695717560320, journalId=1296801528146919473, issueId=1297139203754709410, articleNumber=null, orderNo=null, doi=10.12377/1671-4393.26.06.17, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=null, receivedDateStr=null, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1787191692207, onlineDateStr=2026-08-20, pubDate=1782316800000, pubDateStr=2026-06-25, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1787191692207, onlineIssueDateStr=2026-08-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1787191692207, creator=13701087609, updateTime=1787191692207, updator=13701087609, issue=Issue{id=1297139203754709410, tenantId=1146029695717560320, journalId=1296801528146919473, year='2026', volume='', issue='6', pageStart='3', pageEnd='156', issueExtLink='null', onlineDate='null', pubDate='1782316800000', pubDateStr='2026-06-25', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=1, specialIssue=null, createTime=1787191685856, creator='13701087609', updateTime=1787192210976, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1297141406343131394, tenantId=1146029695717560320, journalId=1296801528146919473, issueId=1297139203754709410, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1297141406343131395, tenantId=1146029695717560320, journalId=1296801528146919473, issueId=1297139203754709410, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=134, endPage=140, ext={EN=ArticleExt(id=1297139230610845910, articleId=1297139230396936405, tenantId=1146029695717560320, journalId=1296801528146919473, language=EN, title=Research on the Method for Determining the Contents of 4 Types of Sugar Alcohols in Infant Formula by Ion Chromatography, columnId=1297134031947194991, journalTitle=China Dairy, columnName=QUALITY CONTROL, runingTitle=null, highlight=null, articleAbstract=
[Objective]

To establish an ion chromatography method for the determination of xylitol, erythritol, sorbitol and maltitol in infant formula.

[Method]

Dionex CarboPacTM MA1 sugar column guard column (4 mm×50 mm) and Dionex CarboPacTM MA1 sugar analysis column (4 mm×250 mm) were used as chromatographic columns, 480mmol/L sodium hydroxide eluent was used for isocratic elution, the flow rate was 0.45mL/min, the injection volume was 10μL, the column temperature was 30℃, and the electrochemical detector was detected.

[Results]

The mass concentration showed a good linear relationship with its peak area in the range of 0.2~20 μg/mL (r2≥0.99969) , the detection limit was between 0.01~0.20 μg/mL, the average recovery rate was 91.8%~99.1%, and the relative standard deviation (RSD) was in the range of 0.9%~2.9%.

[Conclusion]

This method was simple to operate, had high sensitivity and good stability, and could provide a reference for the quality control of infant formula.

, authors=Chunfu TANG1, Lan LIU1, Zhou ZHOU2, Jing YU1, authorsList=Chunfu TANG, Lan LIU, Zhou ZHOU, Jing YU, authorCompany=null, correspAuthors=null, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1297139230996721879, articleId=1297139230396936405, tenantId=1146029695717560320, journalId=1296801528146919473, language=CN, title=离子色谱法测定婴幼儿配方乳粉中4种糖醇含量的方法研究, columnId=1297134032135938673, journalTitle=中国乳业, columnName=质量安全, runingTitle=null, highlight=null, articleAbstract=
[目的]

建立离子色谱法测定婴幼儿配方乳粉中木糖醇、赤藓糖醇、山梨糖醇、麦芽糖醇的分析方法。

[方法]

选择DionexCarboPacTM MA1糖柱保护柱(4 mm×50 mm)和Dionex CarboPacTM MA1糖分析柱(4 mm×250 mm)为色谱柱,480 mmol/L氢氧化钠淋洗液等度洗脱,流速为0.45 mL/min,进样量10 μL,柱温30 ℃,采用电化学检测器检测。

[结果]

质量浓度在0.2~20 μg/mL范围内与峰面积呈现良好的线性关系(r2≧0.99969),检出限在0.01~0.20 μg/mL之间,平均回收率为91.8%~99.1%,相对标准偏差(RSD)在0.9%~2.9%范围内。

[结论]

该方法操作简便、灵敏度高、稳定性好,可为婴幼儿配方乳粉的质量控制提供参考方法。

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汤春甫(1986-),男,湖南衡阳人,硕士,工程师,研究方向为食品安全与质量检测

刘兰(1986-),女,湖南娄底人,硕士,高级工程师,研究方向为食品安全与质量检测

周洲(1989-),女,湖南长沙人,硕士,工程师,研究方向为食品安全与质量检测

余婧(1987-),女,湖南长沙人,硕士,高级工程师,研究方向为食品安全与质量检测。

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离子色谱法测定婴幼儿配方乳粉中4种糖醇含量的方法研究
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汤春甫 1 , 刘兰 1 , 周洲 2 , 余婧 1
中国乳业 | 质量安全 2026,(6): 134-140
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中国乳业 |质量安全 2026 , (6) : 134 -140
离子色谱法测定婴幼儿配方乳粉中4种糖醇含量的方法研究
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余婧(1987-),女,湖南长沙人,硕士,高级工程师,研究方向为食品安全与质量检测。

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余婧(1987-),女,湖南长沙人,硕士,高级工程师,研究方向为食品安全与质量检测。

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汤春甫1, 刘兰1, 周洲2, 余婧1
作者信息
  • 1.湖南省产商品质量检验研究院,湖南 长沙 410007
  • 2.长沙市食品药品检验所,湖南 长沙 410006
作者简介:

汤春甫(1986-),男,湖南衡阳人,硕士,工程师,研究方向为食品安全与质量检测

刘兰(1986-),女,湖南娄底人,硕士,高级工程师,研究方向为食品安全与质量检测

周洲(1989-),女,湖南长沙人,硕士,工程师,研究方向为食品安全与质量检测

余婧(1987-),女,湖南长沙人,硕士,高级工程师,研究方向为食品安全与质量检测。

Research on the Method for Determining the Contents of 4 Types of Sugar Alcohols in Infant Formula by Ion Chromatography
Chunfu TANG1, Lan LIU1, Zhou ZHOU2, Jing YU1
Affiliations
  • 1.Hunan provincial institute of product and goods quality inspection, Hunan Changsha 410007
  • 2.Changsha institute for food and drug control, Hunan Changsha 410006
出版时间: 2026-06-25 doi: 10.12377/1671-4393.26.06.17
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[目的]

建立离子色谱法测定婴幼儿配方乳粉中木糖醇、赤藓糖醇、山梨糖醇、麦芽糖醇的分析方法。

[方法]

选择DionexCarboPacTM MA1糖柱保护柱(4 mm×50 mm)和Dionex CarboPacTM MA1糖分析柱(4 mm×250 mm)为色谱柱,480 mmol/L氢氧化钠淋洗液等度洗脱,流速为0.45 mL/min,进样量10 μL,柱温30 ℃,采用电化学检测器检测。

[结果]

质量浓度在0.2~20 μg/mL范围内与峰面积呈现良好的线性关系(r2≧0.99969),检出限在0.01~0.20 μg/mL之间,平均回收率为91.8%~99.1%,相对标准偏差(RSD)在0.9%~2.9%范围内。

[结论]

该方法操作简便、灵敏度高、稳定性好,可为婴幼儿配方乳粉的质量控制提供参考方法。

离子色谱法  /  婴幼儿配方乳粉  /  木糖醇  /  赤藓糖醇  /  山梨糖醇  /  麦芽糖醇
[Objective]

To establish an ion chromatography method for the determination of xylitol, erythritol, sorbitol and maltitol in infant formula.

[Method]

Dionex CarboPacTM MA1 sugar column guard column (4 mm×50 mm) and Dionex CarboPacTM MA1 sugar analysis column (4 mm×250 mm) were used as chromatographic columns, 480mmol/L sodium hydroxide eluent was used for isocratic elution, the flow rate was 0.45mL/min, the injection volume was 10μL, the column temperature was 30℃, and the electrochemical detector was detected.

[Results]

The mass concentration showed a good linear relationship with its peak area in the range of 0.2~20 μg/mL (r2≥0.99969) , the detection limit was between 0.01~0.20 μg/mL, the average recovery rate was 91.8%~99.1%, and the relative standard deviation (RSD) was in the range of 0.9%~2.9%.

[Conclusion]

This method was simple to operate, had high sensitivity and good stability, and could provide a reference for the quality control of infant formula.

ion chromatography  /  infant formula  /  xylitol  /  erythritol  /  sorbitol  /  maltitol
汤春甫, 刘兰, 周洲, 余婧. 离子色谱法测定婴幼儿配方乳粉中4种糖醇含量的方法研究. 中国乳业, 2026 , (6) : 134 -140 . DOI: 10.12377/1671-4393.26.06.17
Chunfu TANG, Lan LIU, Zhou ZHOU, Jing YU. Research on the Method for Determining the Contents of 4 Types of Sugar Alcohols in Infant Formula by Ion Chromatography[J]. China Dairy, 2026 , (6) : 134 -140 . DOI: 10.12377/1671-4393.26.06.17
  • 湖南省产商品质量检验研究院科研资助计划项目(Y2026N02)
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2026年第卷第6期
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doi: 10.12377/1671-4393.26.06.17
  • 首发时间:2026-08-20
  • 出版时间:2026-06-25
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湖南省产商品质量检验研究院科研资助计划项目(Y2026N02)
作者信息
    1.湖南省产商品质量检验研究院,湖南 长沙 410007
    2.长沙市食品药品检验所,湖南 长沙 410006
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2种不同金属材料的力学参数

Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)

Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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