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A composite of cubic spinel MnFe₂O₄ and carbon nanotubes (CNTs) was synthesized, denoted MnFe₂O₄/CNTs. This study evaluates the efficacy of MnFe₂O₄/CNT for electrocatalytic degradation of phenol, investigating the mechanism of electrocatalytic oxygen reduction to generate H₂O₂ and its subsequent activation into ·OH. The aim is to identify a highly efficient and stable cathode material suitable for electrocatalytic degradation of organic pollutants. Results demonstrate that under optimized conditions (MnFe₂O₄:CNT mass ratio = 19:2, applied voltage = -0.9V, pH = 3, catalyst loading = 0.44mg/cm², O₂ flow rate = 0.5L/min), MnFe₂O₄/CNTs achieved a remarkable phenol degradation efficiency of 99.9% within 30minutes and a total organic carbon (TOC) removal rate of 72.4% after 90minutes. Notably, the composite maintained 84.5% degradation efficiency of phenol after five consecutive cycles. The incorporation of CNTs not only improve electron transfer efficiency within the system, but leads to electron transfer between MnFe₂O₄ and CNTs induces an increase in the relative concentration of non-lattice oxygen species within MnFe₂O₄. Under the above dual effects, MnFe₂O₄/CNTs boost the capability to electrocatalytically reduce O₂ to H₂O₂ and subsequently activate it in situ to generate ·OH, surpassing the performance of pristine MnFe₂O₄. The activation of H₂O₂ is mainly accomplished through a combined process of homogeneous activation involving Mn²⁺ and Fe²⁺ and heterogeneous activation excited by active sites such as non-lattice oxygen in MnFe₂O₄/CNT. The ·OH generated by the activation achieves a relatively thorough oxidation and decomposition of phenol.

, authors=Jia-hao CHEN¹, Zheng-hao LU², Li-ting LING¹, Xiao-mei ZHENG^{1, *}, Yong-hao WANG^{1, *}, authorsList=Jia-hao CHEN, Zheng-hao LU, Li-ting LING, Xiao-mei ZHENG, Yong-hao WANG, authorCompany=null, correspAuthors=Xiao-mei ZHENG, Yong-hao WANG, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1314922093582577702, articleId=1314922093100232740, tenantId=1146029695717560320, journalId=1234093305789726721, language=CN, title=MnFe₂O₄/CNT电芬顿降解苯酚的原位H₂O₂生成及活化机制, columnId=1234106386565624579, journalTitle=中国环境科学, columnName=水污染与控制, runingTitle=null, highlight=null, articleAbstract=

制备了立方相MnFe₂O₄与碳纳米管（CNT）的复合材料MnFe₂O₄/CNT，评估MnFe₂O₄/CNT的电催化降解苯酚的效能，探讨其电催化还原氧气生成H₂O₂并活化为·OH的机理，旨在筛选出一种高效、稳定的可用于电催化降解有机污染物的阴极材料．结果表明，在最佳实验条件为MnFe₂O₄：CNT=19：2、外加电压为-0.9V、pH=3、催化剂负载量为0.44mg/cm²和氧气通量为0.5L/min时，30min内MnFe₂O₄/CNT对苯酚的降解率达99.9%，90min内TOC去除率为72.4%，5次循环实验后MnFe₂O₄/CNT的电催化降解效率仍可达84.5%．CNT的引入不仅提升了MnFe₂O₄/CNT对电子的传递效率，而且致使MnFe₂O₄与CNT之间发生了电子转移，从而引起MnFe₂O₄中非晶格氧的相对含量增加，在上述双重作用下，MnFe₂O₄/CNT呈现出优于MnFe₂O₄的电催化还原O₂生成H₂O₂并原位将其活化为·OH的能力；H₂O₂的活化主要通过Mn²⁺和Fe²⁺参与的均相活化和MnFe₂O₄/CNT的非晶格氧等活性位点激发的非均相活化过程共同完成，活化产生的·OH对苯酚实现了较为彻底的氧化分解．

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陈嘉浩（2000-），男，福建龙岩人，福州大学硕士研究生，研究方向为污水资源化．230627038@fzu.edu.cn.

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陈嘉浩（2000-），男，福建龙岩人，福州大学硕士研究生，研究方向为污水资源化．230627038@fzu.edu.cn.

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