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Pyrolysis is an important process for efficient remediation of petroleum-contaminated soil (PCS), but how to reuse the obtained carbonized soil (RCS) has not received enough attention. In this study, RCS was treated by ball milling to activate its environmental catalytic components, and the obtained carbonized soil (RBCS) was used to activate peroxymonosulfate (PMS) oxidation to treat organic wastewater. The results showed that when the dosage of RBCS was 2g/L and the dosage of PMS was 1.5g/L, the removal rate of aniline (AN, 100mg/L) reached 99.9 %. Compared with RCS, ball milling treatment significantly improved the activation performance of RBCS for PMS oxidation. Quenching experiments and EPR tests showed that 、·OH、¹O₂ and environmental permanent free radicals (EPFRs) existed in the RBCS/PMS system. Electrochemical experiments show that there is also an electron transfer mechanism in the RBCS/PMS system. Ball milling exposes more metal oxides, amorphous carbon and oxygen-containing groups on the surface of carbonized soil. Metal oxides and oxygen-containing groups can activate PMS to produce reactive oxygen species to attack AN, while graphitized carbon and EPFRs may promote PMS oxidation by accelerating direct electron transfer to degrade AN. This study provides an environmentally friendly, value-added transformation strategy and treatment method for RCS, which is expected to have a good application prospect.

, authors=Ling-fei FU¹, Xing-yu YANG¹, Xiao-juan CHAI^{2, *}, Ming-xin WANG^{1, *}, authorsList=Ling-fei FU, Xing-yu YANG, Xiao-juan CHAI, Ming-xin WANG, authorCompany=null, correspAuthors=Xiao-juan CHAI, Ming-xin WANG, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1314917623297573654, articleId=1314917622265774864, tenantId=1146029695717560320, journalId=1234093305789726721, language=CN, title=热解-球磨修复石油污染土壤并转化为过硫酸盐活化剂, columnId=1234106394572550190, journalTitle=中国环境科学, columnName=土壤污染与控制, runingTitle=null, highlight=null, articleAbstract=

对炭化土壤（RCS）进行球磨处理以激发其环境催化组分，并将所得炭化土壤（RBCS）用于活化过一硫酸盐（PMS）氧化处理有机废水．结果表明，当RBCS投加量为2g/L，PMS投加量为1.5g/L时，苯胺（AN，100mg/L）的去除率达到99.9%．与RCS相比，球磨处理显著提高了材料的PMS活化性能．猝灭实验和EPR测试表明，RBCS/PMS体系中存在、·OH、¹O₂和环境永久性自由基（EPFRs）．电化学实验表明，RBCS/PMS体系中还存在电子转移机制．球磨使炭化土壤表面暴露了更多的金属氧化物和含氧官能团，激活PMS产生活性氧攻击AN，石墨化碳和EPFRs则通过加速直接电子转移降解AN．研究结果为RCS提供一个环境友好的增值转化策略与处理方法，预期具有较好的应用前景．

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傅凌飞（1999-），男，江苏常州人，常州大学硕士研究生，主要研究土壤污染防治．3097436047@qq.com.

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傅凌飞（1999-），男，江苏常州人，常州大学硕士研究生，主要研究土壤污染防治．3097436047@qq.com.

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