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A spherical Co-based catalyst (Co-BC) was successfully synthesized via ion-exchange and molding (drying, binding, rolling, calcination) using ZSM-5 as support and Co(NO₃)₂ as active component, with ultralow Co content (0.94wt.%). Multiple characterizations (EDS/XRD/ICP/XPS) demonstrated Co-BC's efficient PMS activation for aqueous acetone (CVOC model) degradation. Under the conditions of 5×10^-6acetone (initial pH=7), 7.5mmol/L PMS dosage, 10g/L Co-BC dosage, the removal efficiency of acetone can reach 100% in 2hours, with a pseudo first order kinetic constant of 0.077min^-1. Radical quenching experiment and electron spin-resonance spectrometer (ESR) characterization results indicated that the excellent performance was attributed to synergy of radicals (SO₄^·-, ^·OH, O₂^·-) and nonradical (¹O₂). Co-BC performed good removal efficiency (70%~100%) for acetone within a wide pH range (3~11). After being reused for 5times, Co-BC still exhibited a removal rate of 90% for acetone. The Co leaching amount from the Co-BC/PMS system was merely 0.61mg/L, well within the national wastewater discharge limit of 1mg/L and significantly lower than that (9.86mg/L) of the powder catalyst under identical conditions, demonstrating the superior catalytic performance and stability of Co-BC.

, authors=Shuai LIU, Ya-nan WANG, Hang YUAN, Hai-yang ZHANG, Zhen LI, Yan-lin JIAO, Jian WANG, Guang-fei YU, Qin DAI^*, Li-dong WANG, authorsList=Shuai LIU, Ya-nan WANG, Hang YUAN, Hai-yang ZHANG, Zhen LI, Yan-lin JIAO, Jian WANG, Guang-fei YU, Qin DAI, Li-dong WANG, authorCompany=null, correspAuthors=Qin DAI, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1314917502157680765, articleId=1314917501323014267, tenantId=1146029695717560320, journalId=1234093305789726721, language=CN, title=成型钴基小球催化剂活化过一硫酸盐去除水中含羰基VOCs, columnId=1234106386565624579, journalTitle=中国环境科学, columnName=水污染与控制, runingTitle=null, highlight=null, articleAbstract=

本研究通过离子交换和成型工艺（干燥、粘结、滚压和煅烧）成功制备了球形钴基催化剂（Co-BC），其中以ZSM-5分子筛为载体，Co（NO₃）₂为活性组分．该催化剂具有超低钴含量（0.94wt.%）．通过能量色散谱仪（EDS）、X射线衍射仪（XRD）、电感耦合等离子体发射光谱（ICP）和X射线光电子能谱仪（XPS）表征证实Co-BC可高效活化PMS降解液相丙酮（羰基挥发性有机化合物（CVOCs）模型污染物）．在丙酮初始浓度为5×10^-6（pH=7）、PMS为7.5mmol/L、催化剂为10g/L条件下，2h内丙酮去除率达100%（伪一级动力学常数为0.077min^-1）．淬灭实验和ESR分析表明，其优异性能源于自由基（SO₄^·-、^·OH、O₂^·-）和非自由基（¹O₂）的协同作用．Co-BC在宽pH值（3~11）范围内保持70%~100%的去除率，循环使用5次后仍达90%，且钴浸出量仅0.61mg/L（低于国标1mg/L限值），较粉末催化剂（9.86mg/L）显著降低，展现出优异的催化稳定性．

, authors=刘帅, 王亚囡, 袁航, 张海洋, 李贞, 焦燕麟, 王健, 于广飞, 代琴^*, 汪黎东, authorsList=刘帅, 王亚囡, 袁航, 张海洋, 李贞, 焦燕麟, 王健, 于广飞, 代琴, 汪黎东, authorCompany=null, correspAuthors=代琴, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=4wHjyZ1Uewnp5nDJdHqkqg==, magXml=AZJMcvqxjJRI3MINpQ3M3g==, pdfUrl=null, pdf=DofwKLzrB/XmDRjyxrOeJg==, pdfFileSize=1268538, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=XeEg/6cF9aV+WkTUCw95AA==, mapNumber=null, fund=null)}, authors=[Author(id=1314917503655047298, tenantId=1146029695717560320, journalId=1234093305789726721, articleId=1314917501323014267, orderNo=0, firstName=null, middleName=null, lastName=null, nameCn=null, orcid=null, stid=null, country=null, authorPic=null, dead=0, email=liushuai2418@foxmail.com, emailSecond=null, emailThird=null, correspondingAuthor=0, authorType=1, ext={EN=AuthorExt(id=1314917503730544772, tenantId=1146029695717560320, journalId=1234093305789726721, articleId=1314917501323014267, authorId=1314917503655047298, language=EN, stringName=Shuai LIU, firstName=Shuai, middleName=null, lastName=LIU, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=null, address=MOE Key Laboratory of Resources and Environmental Systems Optimization, College of Environmental Science and Engineering, North China Electric Power University, Beijing 102206, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1314917503818625157, tenantId=1146029695717560320, journalId=1234093305789726721, articleId=1314917501323014267, authorId=1314917503655047298, language=CN, stringName=刘帅, firstName=null, middleName=null, lastName=null, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=null, address=华北电力大学环境科学与工程学院，教育部资源与环境系统优化重点实验室，北京 102206, bio={"content":"

刘帅（1999-），男，河北石家庄人，华北电力大学硕士研究生，主要研究方向为高级氧化技术降解水中有机污染物．liushuai2418@foxmail.com.

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刘帅（1999-），男，河北石家庄人，华北电力大学硕士研究生，主要研究方向为高级氧化技术降解水中有机污染物．liushuai2418@foxmail.com.

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