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Supported bimetallic Pd-Rh catalysts were prepared using the impregnation method. The effects of the active components content and the carrier on the catalytic activity of the bimetallic Pd-Rh catalysts were investigated with 4-fluorophenol (4-FP) as the representative fluorinated organic compounds (FOCs). The results showed that the presence of Rh significantly enhanced their catalytic activity for the hydrodefluorination (HDF) of 4-FP, and 2% Pd-1% Rh/AC exhibited good catalytic activity for the HDF of 4-FP, and the conversion of 4-FP over 2% Pd-1% Rh/AC reached 95.62% within 90min. Furthermore, the type of the carrier played a significant role on the catalytic activity of bimetallic Pd-Rh catalysts. 2%Pd-1%Rh/CB exhibited the highest catalytic activity for the HDF of 4-FP when carbon black (CB) was used as a carrier, and thus the complete HDF of 4-FP was achieved within 80min. Catalyst characterization (BET, ICP-MS, RS, TEM, and XPS) indicated that the carriers with more surface defects favored the catalysts exhibited higher catalytic activity, which in turn enabled 2%Pd-1%Rh/CB and 2%Pd-1%Rh/CNTs to exhibit higher catalytic activity for the HDF of 4-FP. Moreover, 2%Pd-1%Rh/CB possessed more Pd⁰, which is more conducive to the activation of the H₂, and in turn promoted catalytic HDF of 4-FP. Thus, 2%Pd-1%Rh/CB possessed the highest catalytic activity for the HDF of 4-FP.

, authors=Su-jing LIU¹, Gui-ying MA², Rui-ning YIN¹, Xin-bei LI³, Xu-tao GONG¹, Ying LIU¹, Xuan-xuan MA^{1, *}, Chuan-hai XIA^{1, **}, authorsList=Su-jing LIU, Gui-ying MA, Rui-ning YIN, Xin-bei LI, Xu-tao GONG, Ying LIU, Xuan-xuan MA, Chuan-hai XIA, authorCompany=null, correspAuthors=Xuan-xuan MA, Chuan-hai XIA, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1314917494742147193, articleId=1314917492527554679, tenantId=1146029695717560320, journalId=1234093305789726721, language=CN, title=负载型Pd-Rh催化剂催化4-氟苯酚加氢脱氟降解, columnId=1234106386565624579, journalTitle=中国环境科学, columnName=水污染与控制, runingTitle=null, highlight=null, articleAbstract=

采用浸渍法制备了负载型Pd-Rh双金属催化剂，并以4-氟苯酚（4-FP）为模型化合物，研究了活性组分Pd-Rh含量、载体等对Pd-Rh双金属催化剂催化4-FP加氢脱氟的影响．结果表明，Rh的存在显著提升催化剂对4-FP加氢脱氟的催化活性，且2%Pd-1%Rh/AC对4-FP的加氢脱氟表现出较好的催化活性，其催化4-FP在90min时的加氢脱氟转化率为95.62%．碳载体类型对Pd-Rh双金属催化剂的催化活性有着重要影响，炭黑（CB）作为载体时2%Pd-1%Rh/CB表现出最高的催化活性，2%Pd-1%Rh/CB催化下4-FP在80min内即可完全加氢脱氟．催化剂表征（BET、ICP-MS、RS、TEM和XPS）表明，这可能与CB载体的表面缺陷有关，载体表面缺陷越多，催化剂的催化活性越高；而且当Pd更多地以Pd⁰形式存在时，被Pd⁰吸附并活化产生的活性H*越多，越有利于4-FP的加氢脱氟降解，因而2%Pd-1%Rh/CB对4-FP的加氢脱氟表现出最高的催化活性．

, authors=刘苏静¹, 马贵营², 殷瑞宁¹, 李昕蓓³, 公绪涛¹, 刘莺¹, 马宣宣^{1, *}, 夏传海^{1, **}, authorsList=刘苏静, 马贵营, 殷瑞宁, 李昕蓓, 公绪涛, 刘莺, 马宣宣, 夏传海, authorCompany=null, correspAuthors=马宣宣, 夏传海, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=ZOpBtKkBfsjgKR4pF8RwOg==, magXml=68OFjTXajHdqgJHd+EN/Rg==, pdfUrl=null, pdf=BL4uvphIksXYJWz/pWDU0Q==, pdfFileSize=3100611, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=J5U4rJd/6atO4NxLxyF9hw==, mapNumber=null, fund=null)}, authors=[Author(id=1314917495329349764, tenantId=1146029695717560320, journalId=1234093305789726721, articleId=1314917492527554679, orderNo=0, firstName=null, middleName=null, lastName=null, nameCn=null, orcid=null, stid=null, country=null, authorPic=null, dead=0, email=liusujingldu@163.com, emailSecond=null, emailThird=null, correspondingAuthor=0, authorType=1, ext={EN=AuthorExt(id=1314917495811694726, tenantId=1146029695717560320, journalId=1234093305789726721, articleId=1314917492527554679, authorId=1314917495329349764, language=EN, stringName=Su-jing LIU, firstName=Su-jing, middleName=null, lastName=LIU, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=¹, address=^1.School of Resources and Environmental Engineering, Ludong University, Yantai 264025, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1314917496122073223, tenantId=1146029695717560320, journalId=1234093305789726721, articleId=1314917492527554679, authorId=1314917495329349764, language=CN, stringName=刘苏静, firstName=null, middleName=null, lastName=null, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=¹, address=^1.鲁东大学资源与环境工程学院，山东 烟台 264025, bio={"content":"

刘苏静（1980-），女，山东威海人，讲师，博士，主要从事有机卤代污染物控制研究．发表论文10余篇．liusujingldu@163.com.

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刘苏静（1980-），女，山东威海人，讲师，博士，主要从事有机卤代污染物控制研究．发表论文10余篇．liusujingldu@163.com.

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