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In this study, the degradation efficiency and mechanism of oxytetracycline（OTC）in the Fe（Ⅲ）/peracetic acid（PAA）system were investigated, and the effects of initial pH, reagents dosage and water components on OTC degradation were also explored. The results suggested that in the degradation of OTC by Fe（Ⅲ）/PAA system, Fe（Ⅲ）complexed with OTC to form Fe（Ⅲ）-OTC complex, which reduced Fe（Ⅲ）to Fe（II）through internal electron transfer. Subsequently, the generated Fe（II）catalyzed PAA to produce reactive species, thus accelerating the degradation of OTC. The results of chemical probe and radical quenching experiments showed that organic radicals（CH₃C（O）O^• and CH₃C（O）OO^•）, HO^• and Fe（IV）played major roles for the degradation of OTC in Fe（III）/PAA system. Acidic conditions were beneficial to the degradation of OTC in this system, while the removal of OTC under neutral and weakly alkaline conditions was mainly due to the PAA oxidation. The removal efficiency of OTC increased gradually with the increase of PAA or Fe（Ⅲ）dosage, but their excess concentration would inhibit OTC degradation. The presence of Cl^- and natural organic matter in Fe（Ⅲ）/PAA systeminhibited the degradation of OTC, while NO₃^-, SO₄^2- and HCO₃^- had little effect on OTC removal. The Fe（Ⅲ）/PAA system also ha d a good treatment effect on the other tetracycline pollutants.

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考察了Fe(Ⅲ)/过氧乙酸(PAA)体系对土霉素(OTC)的降解效能与机理，以及初始pH值、药剂投加量、水体基质对OTC降解的影响.结果表明：Fe(Ⅲ)/PAA体系降解OTC过程中，Fe(Ⅲ)与OTC发生络合形成Fe(Ⅲ)-OTC络合物，该络合物通过内部电子转移使Fe(Ⅲ)还原为Fe(Ⅱ)，生成的Fe(Ⅱ)催化PAA产生活性物种，从而加快了OTC的降解.化学探针和自由基淬灭实验结果表明，有机自由基(CH₃C(O)O^•和CH₃C(O)OO^•)、HO^•和Fe(Ⅳ)为该体系的主要活性物种.酸性条件有利于该体系对OTC的降解，在中性及弱碱性条件下，OTC在该体系中的去除主要是由于PAA氧化作用.随着PAA、Fe(Ⅲ)投加量的提高，OTC的去除效率逐渐增加，但是其过量则会抑制OTC降解.水中Cl^-和天然有机物的存在会抑制OTC的降解，而NO₃^-、SO₄^2-和HCO₃^-对OTC的降解几乎没有影响.Fe(Ⅲ)/PAA体系对其他四环素类污染物也有较好的处理效果.

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胡虹(1996-)，女，四川自贡人，西南交通大学硕士研究生，研究方向为水污染控制.huh@my.swjtu.edu.cn.

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胡虹(1996-)，女，四川自贡人，西南交通大学硕士研究生，研究方向为水污染控制.huh@my.swjtu.edu.cn.

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Beijing: Beijing Jiaotong University，2016., articleTitle=Effect of Fe(II/III) on the degradation of tetracycline antibiotics and its mechanism, refAbstract=null)], funds=[Fund(id=1241116669666447439, tenantId=1146029695717560320, journalId=1234093305789726721, articleId=1241116652398498523, awardId=2023YFB2390100, language=CN, fundingSource=国家重点研发计划(2023YFB2390100), fundOrder=null, country=null), Fund(id=1241116669762916443, tenantId=1146029695717560320, journalId=1234093305789726721, articleId=1241116652398498523, awardId=2682024QZ007, language=CN, fundingSource=西南交通大学新型交叉学科培育基金项目(2682024QZ007), fundOrder=null, country=null)], companyList=[AuthorCompany(id=1241116663215608340, tenantId=1146029695717560320, journalId=1234093305789726721, articleId=1241116652398498523, xref=null, ext=[AuthorCompanyExt(id=1241116663270134301, tenantId=1146029695717560320, journalId=1234093305789726721, articleId=1241116652398498523, companyId=1241116663215608340, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=School of Environmental Science and Engineering, Southwest Jiaotong University, Chengdu 611756, China), AuthorCompanyExt(id=1241116663295300129, tenantId=1146029695717560320, journalId=1234093305789726721, articleId=1241116652398498523, companyId=1241116663215608340, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=西南交通大学环境科学与工程学院，四川 成都 611756)])], figs=[ArticleFig(id=1241116667367969639, tenantId=1146029695717560320, journalId=1234093305789726721, articleId=1241116652398498523, language=EN, label=Fig.1, caption=Degradation of OTC in different systems, and change of UV-vis spectrum of OTC in Fe（Ⅲ）/PAA system, figureFileSmall=hZTm41D3P5rI79QaytCEMA==, figureFileBig=hPrSbUDUe7Vzgt7V+EeXFQ==, tableContent=null), ArticleFig(id=1241116667493798774, tenantId=1146029695717560320, journalId=1234093305789726721, articleId=1241116652398498523, language=CN, label=图1, caption=不同体系下OTC降解及Fe（Ⅲ）/PAA体系中OTC紫外-可见光谱变化

实验条件：[Fe(Ⅲ)]₀ = 10µmol/L，[PAA]₀ = 0.3mmol/L，[H₂O₂]₀ =0.42mmol/L，[OTC]₀ = 40µmol/L，pH₀ = 4.0，T = 25℃

, figureFileSmall=hZTm41D3P5rI79QaytCEMA==, figureFileBig=hPrSbUDUe7Vzgt7V+EeXFQ==, tableContent=null), ArticleFig(id=1241116667724485522, tenantId=1146029695717560320, journalId=1234093305789726721, articleId=1241116652398498523, language=EN, label=Fig.2, caption=Changes of Fe and PAA concentrations during OTC degradation in Fe（Ⅲ）/PAA system, and effects of different chelating agents on OTC degradation in Fe（Ⅲ）/PAA system, figureFileSmall=2ld2A92nZc7My4rdVm+mlg==, figureFileBig=iWQ7deXAcqHy5Q+pk2i7tQ==, tableContent=null), ArticleFig(id=1241116667997115297, tenantId=1146029695717560320, journalId=1234093305789726721, articleId=1241116652398498523, language=CN, label=图2, caption=Fe（Ⅲ）/PAA降解OTC过程中铁和PAA浓度的变化及不同络合剂对Fe（Ⅲ）/PAA降解OTC的影响

实验条件：[Fe(Ⅲ)]₀ = 10µmol/L，[PAA]₀ = 0.3mmol/L，[OTC]₀ = [EDTA]₀ = [NTA]₀ = 40µmol/L，pH₀ = 4.0，T = 25℃

, figureFileSmall=2ld2A92nZc7My4rdVm+mlg==, figureFileBig=iWQ7deXAcqHy5Q+pk2i7tQ==, tableContent=null), ArticleFig(id=1241116668143915952, tenantId=1146029695717560320, journalId=1234093305789726721, articleId=1241116652398498523, language=EN, label=Fig.3, caption=Changes of PMSO and PMSO₂ concentrations in Fe（Ⅲ）/PAA system, and effects of different scavengers on OTC degradation in Fe（Ⅲ）/PAA system, figureFileSmall=MRvJQtwkNS5RqhriC6Y6mQ==, figureFileBig=WCpV5lwvYGHVNAdCAtFxMg==, tableContent=null), ArticleFig(id=1241116668244579258, tenantId=1146029695717560320, journalId=1234093305789726721, articleId=1241116652398498523, language=CN, label=图3, caption=Fe（Ⅲ）/PAA体系中PMSO和PMSO₂浓度变化及不同淬灭剂对Fe（Ⅲ）/PAA降解OTC的影响

实验条件：[Fe(Ⅲ)]₀ = 10µmol/L，[PAA]₀ = 0.3mmol/L，[OTC]₀ =[PMSO]₀ = 40µmol/L，[MeOH]₀ = [TBA]₀ = 100mmol/L，NB =1mmol/L，pH₀ = 4.0，T = 25℃

, figureFileSmall=MRvJQtwkNS5RqhriC6Y6mQ==, figureFileBig=WCpV5lwvYGHVNAdCAtFxMg==, tableContent=null), ArticleFig(id=1241116668370408388, tenantId=1146029695717560320, journalId=1234093305789726721, articleId=1241116652398498523, language=EN, label=Fig.4, caption=Degradation mechanism of OTC in Fe（Ⅲ）/PAA system, figureFileSmall=vmIbGoeU3Gs8osJ6uZt8bg==, figureFileBig=hCN+hFqZLdkkHRtSHP4LBw==, tableContent=null), ArticleFig(id=1241116668504626133, tenantId=1146029695717560320, journalId=1234093305789726721, articleId=1241116652398498523, language=CN, label=图4, caption=Fe（Ⅲ）/PAA体系降解OTC的机理, figureFileSmall=vmIbGoeU3Gs8osJ6uZt8bg==, figureFileBig=hCN+hFqZLdkkHRtSHP4LBw==, tableContent=null), ArticleFig(id=1241116668634649568, tenantId=1146029695717560320, journalId=1234093305789726721, articleId=1241116652398498523, language=EN, label=Fig.5, caption=Effect of initial pH on OTC degradation in Fe（Ⅲ）/PAA and PAA alone systems, figureFileSmall=zQgawAp8wTdu/r/kpQl5xw==, figureFileBig=5V7HGjp05RXi4ZLIYw+y2A==, tableContent=null), ArticleFig(id=1241116668756284399, tenantId=1146029695717560320, journalId=1234093305789726721, articleId=1241116652398498523, language=CN, label=图5, caption=初始pH值对Fe（Ⅲ）/PAA与单独PAA降解OTC的影响

实验条件：[Fe(Ⅲ)]₀ = 10µmol/L，[PAA]₀ = 0.3mmol/L，[OTC]₀ = 40µmol/L，T = 25℃

, figureFileSmall=zQgawAp8wTdu/r/kpQl5xw==, figureFileBig=5V7HGjp05RXi4ZLIYw+y2A==, tableContent=null), ArticleFig(id=1241116668882113532, tenantId=1146029695717560320, journalId=1234093305789726721, articleId=1241116652398498523, language=EN, label=Fig.6, caption=Effects of PAA, Fe（Ⅲ）and OTC dosages on OTC degradation in Fe（Ⅲ）/PAA sytem, figureFileSmall=cS/yKvZeFCp0CarxvQariQ==, figureFileBig=WP7fqunpnoxjLYwoFSrQKA==, tableContent=null), ArticleFig(id=1241116668995358726, tenantId=1146029695717560320, journalId=1234093305789726721, articleId=1241116652398498523, language=CN, label=图6, caption=不同浓度的PAA, Fe（Ⅲ）和OTC对Fe（Ⅲ）/PAA降解OTC的影响

实验条件：[Fe(Ⅲ)]₀ = 10µmol/L(图b除外)，[PAA]₀ = 0.3mmol/L(图a除外)，[OTC]₀ = 40µmol/L(图c除外)，pH₀ = 4.0，T = 25℃

, figureFileSmall=cS/yKvZeFCp0CarxvQariQ==, figureFileBig=WP7fqunpnoxjLYwoFSrQKA==, tableContent=null), ArticleFig(id=1241116669137965074, tenantId=1146029695717560320, journalId=1234093305789726721, articleId=1241116652398498523, language=EN, label=Fig.7, caption=Effect of water matrix on OTC degradation in Fe（Ⅲ）/PAA system, figureFileSmall=y+mcqttlVoWQNEx8l/agSw==, figureFileBig=u0cq1DVSYOCY7EdKVwYbJA==, tableContent=null), ArticleFig(id=1241116669255405603, tenantId=1146029695717560320, journalId=1234093305789726721, articleId=1241116652398498523, language=CN, label=图7, caption=水体成分对Fe（Ⅲ）/PAA体系降解OTC的影响

实验条件：[Fe(Ⅲ)]₀ = 10µmol/L，[PAA]₀ = 0.3mmol/L，[OTC]₀ = 40µmol/L，pH₀ = 4.0，T = 25℃

, figureFileSmall=y+mcqttlVoWQNEx8l/agSw==, figureFileBig=u0cq1DVSYOCY7EdKVwYbJA==, tableContent=null), ArticleFig(id=1241116669381234738, tenantId=1146029695717560320, journalId=1234093305789726721, articleId=1241116652398498523, language=EN, label=Fig.8, caption=Degradation of other tetracycline antibiotics by Fe（Ⅲ）/PAA system, figureFileSmall=pTGxWSb7uhwlIOJJZaWIxg==, figureFileBig=agD6F5M9NfdGpAMvWqnJrw==, tableContent=null), ArticleFig(id=1241116669519646786, tenantId=1146029695717560320, journalId=1234093305789726721, articleId=1241116652398498523, language=CN, label=图8, caption=Fe（Ⅲ）/PAA体系对其他四环素类抗生素的降解

实验条件：[Fe(Ⅲ)]₀ = 10µmol/L，[PAA]₀ = 0.3mmol/L，[TC]₀ = [OTC]₀ =[CTC]₀ = 40µmol/L，pH₀ = 4.0，T = 25℃

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