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Due to its late discovery, wide distribution, large reserves, complex composition, and low grade, the comprehensive development and utilization of clay type lithium mines still lack systematic research. A systematic study was conducted on the optimization of enhanced leaching process parameters for clay type lithium ore in Liuzhi Special District, Liupanshui City, Guizhou Province. The effects of roasting process conditions such as roasting temperature and time, as well as the effects of leaching process conditions such as leaching agent hydrochloric acid concentration, leaching temperature and time, stirring speed, and liquid volume to solid mass ratio on the experimental results were investigated. The results show that roasting can destroy the crystal lattice of minerals such as kaolinite, superphosphate, diopside, and lithium chlorite in clay type lithium ores, which is beneficial for the sufficient contact between lithium containing phases and leaching agents during subsequent leaching processes, thereby improving their leaching efficiency;After high-temperature roasting at 600 ℃ for 90 min, the clay type lithium ore was subjected to optimal leaching conditions of 60 min, leaching temperature of 80 ℃, hydrochloric acid concentration of 4 mol/L, stirring speed of 400 r/min, and liquid volume to solid mass ratio of 6∶1. The lithium leaching rate can reach 93.48% and the leaching effect is good. The method does not require any additives during the calcination process, which can reduce pollution and lower costs. It has certain promotion and application value.

, authors=Shan ZHU, Yanxia ZHU, Chenhu ZHANG, authorsList=Shan ZHU, Yanxia ZHU, Chenhu ZHANG, authorCompany=null, correspAuthors=null, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1311350741911036417, articleId=1311350741361582591, tenantId=1146029695717560320, journalId=1146120122248306696, language=CN, title=低品位黏土型锂矿的焙烧—浸出工艺优化研究, columnId=1152626641328501305, journalTitle=湿法冶金, columnName=试验研究, runingTitle=null, highlight=null, articleAbstract=

黏土型锂矿因发现晚、分布广、储量大、成分复杂、品位低，导致其综合开发利用尚缺乏系统性研究。以贵州省六盘水市六枝特区黏土型锂矿为对象，系统研究优化了其焙烧—浸出工艺参数，考察了焙烧温度和时间等焙烧工艺条件，以及浸出剂盐酸浓度、浸出温度和时间、搅拌速度、液固体积质量比等浸出工艺条件对试验结果的影响。结果表明：焙烧能破坏黏土型锂矿中的高岭石、透磷钙石、地开石、锂绿泥石等矿物晶格，有利于后续浸出过程中含锂物相与浸出剂充分接触，从而提升其浸出效果；黏土型锂矿在600 ℃下焙烧90 min，再在浸出温度80 ℃、盐酸浓度4 mol/L、搅拌速度400 r/ min、液固体积质量比6∶1的最佳条件下浸出60 min，锂浸出率可达93.48%，浸出效果较好。该法在焙烧过程中无需添加剂，可减少污染、降低成本，具有一定推广利用价值。

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朱山（1989—），男，博士，教授，主要研究方向为有色金属湿法冶金。

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朱山（1989—），男，博士，教授，主要研究方向为有色金属湿法冶金。

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