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Article(id=1311350432337854894, tenantId=1146029695717560320, journalId=1146120122248306696, issueId=1311350424792301947, articleNumber=null, orderNo=null, doi=10.13355/j.cnki.sfyj.2026.02.010, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1761494400000, receivedDateStr=2025-10-27, revisedDate=1765209600000, revisedDateStr=2025-12-09, acceptedDate=null, acceptedDateStr=null, onlineDate=1790579906782, onlineDateStr=2026-09-28, pubDate=1776614400000, pubDateStr=2026-04-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1790579906782, onlineIssueDateStr=2026-09-28, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1790579906782, creator=13701087609, updateTime=1790579906782, updator=13701087609, issue=Issue{id=1311350424792301947, tenantId=1146029695717560320, journalId=1146120122248306696, year='2026', volume='45', issue='2', pageStart='129', pageEnd='272', issueExtLink='null', onlineDate='null', pubDate='1776614400000', pubDateStr='2026-04-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1790579904983, creator='13701087609', updateTime=1790588502603, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1311386485903942043, tenantId=1146029695717560320, journalId=1146120122248306696, issueId=1311350424792301947, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1311386485903942044, tenantId=1146029695717560320, journalId=1146120122248306696, issueId=1311350424792301947, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=208, endPage=214, ext={EN=ArticleExt(id=1311350432543375791, articleId=1311350432337854894, tenantId=1146029695717560320, journalId=1146120122248306696, language=EN, title=Extraction of Rare Earths from NdFeB Waste by Ultrasonic Enhanced Hydrochloric Acid Leaching Method, columnId=1152626641181700664, journalTitle=Hydrometallurgy of China, columnName=Experiment Research, runingTitle=null, highlight=null, articleAbstract=

To address the issues of long leaching time and high consumption of hydrochloric acid in the conventional hydrochloric acid leaching method for neodymium-iron-boron (NdFeB) waste, the ultrasonic-enhanced hydrochloric acid solubilization method was studied for the leaching of rare earths from it. The effects of ultrasonic power, hydrochloric acid concentration, temperature, liquid volume to solid mass ratio, leaching time, particle size and other factors on the leaching rate of rare earths were investigated, and the optimal leaching parameters were determined. The results show that ultrasonic assistance significantly enhances the leaching process. Under the optimal conditions of ultrasonic power of 60 W, hydrochloric acid concentration of 2 mol/L, temperature of 85 ℃, liquid volume to solid mass ratio of 10 mL/1 g, leaching time of 105 min, and particle size of -0.074 mm, the rare earth leaching rate reaches 97.94%, which is 8 percentage points higher than that of the conventional hydrochloric acid leaching method under its best conditions. The method is an efficient and feasible green process for rare earth recovery and provides a new approach for the resource utilization of NdFeB waste.

, authors=Qi WU1, 2, Wenjun FAN1, 2, 3, Chengye ZHANG1, 2, Chengcheng ZHANG1, 2, Xiaowei ZHANG1, 2, 3, Zhongxing LIU1, 2, 3, authorsList=Qi WU, Wenjun FAN, Chengye ZHANG, Chengcheng ZHANG, Xiaowei ZHANG, Zhongxing LIU, authorCompany=null, correspAuthors=Wenjun FAN, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1311350432836977072, articleId=1311350432337854894, tenantId=1146029695717560320, journalId=1146120122248306696, language=CN, title=用超声强化盐酸优溶法浸出钕铁硼废料中的稀土, columnId=1152626641328501305, journalTitle=湿法冶金, columnName=试验研究, runingTitle=null, highlight=null, articleAbstract=

针对钕铁硼废料盐酸优溶法浸出时间长、盐酸消耗量大等问题，研究采用超声强化盐酸优溶法从中浸出稀土。考察了超声波功率、盐酸浓度、温度、液固体积质量比、浸出时间、粒径等因素对稀土浸出率的影响，确定了最佳的浸出参数。结果表明：超声辅助可显著强化浸出过程，在超声波功率60 W、盐酸浓度2 mol/L、温度85 ℃、液固体积质量比10 mL/1 g、浸出时间105 min、粒径-0.074 mm最佳条件下，稀土浸出率达97.94%，比最佳条件下的常规盐酸优溶法的稀土浸出率提高8个百分点。该法是一种高效、可行的稀土回收绿色工艺，可为钕铁硼废料的资源化利用提供一种新途径。

, authors=吴琦1, 2, 樊文军1, 2, 3, 张成业1, 2, 张成成1, 2, 张晓伟1, 2, 3, 刘中兴1, 2, 3, authorsList=吴琦, 樊文军, 张成业, 张成成, 张晓伟, 刘中兴, authorCompany=null, correspAuthors=樊文军, authorNote=

吴琦（2000—），男，硕士，主要研究方向为稀土绿色冶金。

, correspAuthorsNote=
樊文军（1976—），男，硕士，副教授，主要研究方向为钕铁硼绿色回收。E-mail: 。
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吴琦（2000—），男，硕士，主要研究方向为稀土绿色冶金。

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吴琦（2000—），男，硕士，主要研究方向为稀土绿色冶金。

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2.Key Laboratory of Full-cycle Green Development & High-Efficiency Utilization of Light Rare-Earth Resources (Inner Mongolia University of Science and Technology), Baotou　014010, China
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用超声强化盐酸优溶法浸出钕铁硼废料中的稀土
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吴琦 1, 2 , 樊文军 1, 2, 3 , 张成业 1, 2 , 张成成 1, 2 , 张晓伟 1, 2, 3 , 刘中兴 1, 2, 3
湿法冶金 | 试验研究 2026,45(2): 208-214
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湿法冶金 |试验研究 2026 , 45 (2) : 208 -214
用超声强化盐酸优溶法浸出钕铁硼废料中的稀土
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吴琦1, 2, 樊文军1, 2, 3 , 张成业1, 2, 张成成1, 2, 张晓伟1, 2, 3, 刘中兴1, 2, 3
作者信息
  • 1．内蒙古科技大学 稀土产业学院（稀土工程技术学院），内蒙古 包头　014010
  • 2．轻稀土资源全周期绿色高效开发利用教育部重点实验室（内蒙古科技大学），内蒙古 包头　014010
  • 3．内蒙古自治区工程研究中心，内蒙古 包头　014010
通讯作者:
樊文军（1976—），男，硕士，副教授，主要研究方向为钕铁硼绿色回收。E-mail: 。
作者简介:

吴琦（2000—），男，硕士，主要研究方向为稀土绿色冶金。

Extraction of Rare Earths from NdFeB Waste by Ultrasonic Enhanced Hydrochloric Acid Leaching Method
Qi WU1, 2, Wenjun FAN1, 2, 3 , Chengye ZHANG1, 2, Chengcheng ZHANG1, 2, Xiaowei ZHANG1, 2, 3, Zhongxing LIU1, 2, 3
Affiliations
  • 1.Institute of Rare Earth Industry(College of Rare Earth Engineering and Technology), Inner Mongolia University of Science and Technology, Baotou　014010, China
  • 2.Key Laboratory of Full-cycle Green Development & High-Efficiency Utilization of Light Rare-Earth Resources (Inner Mongolia University of Science and Technology), Baotou　014010, China
  • 3.Engineering Research Center of Inner Mongolia Autonomous Region, Baotou　014010, China
出版时间: 2026-04-20 doi: 10.13355/j.cnki.sfyj.2026.02.010
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针对钕铁硼废料盐酸优溶法浸出时间长、盐酸消耗量大等问题，研究采用超声强化盐酸优溶法从中浸出稀土。考察了超声波功率、盐酸浓度、温度、液固体积质量比、浸出时间、粒径等因素对稀土浸出率的影响，确定了最佳的浸出参数。结果表明：超声辅助可显著强化浸出过程，在超声波功率60 W、盐酸浓度2 mol/L、温度85 ℃、液固体积质量比10 mL/1 g、浸出时间105 min、粒径-0.074 mm最佳条件下，稀土浸出率达97.94%，比最佳条件下的常规盐酸优溶法的稀土浸出率提高8个百分点。该法是一种高效、可行的稀土回收绿色工艺，可为钕铁硼废料的资源化利用提供一种新途径。

超声强化  /  钕铁硼废料  /  盐酸优溶法  /  稀土  /  绿色高效  /  浸出

To address the issues of long leaching time and high consumption of hydrochloric acid in the conventional hydrochloric acid leaching method for neodymium-iron-boron (NdFeB) waste, the ultrasonic-enhanced hydrochloric acid solubilization method was studied for the leaching of rare earths from it. The effects of ultrasonic power, hydrochloric acid concentration, temperature, liquid volume to solid mass ratio, leaching time, particle size and other factors on the leaching rate of rare earths were investigated, and the optimal leaching parameters were determined. The results show that ultrasonic assistance significantly enhances the leaching process. Under the optimal conditions of ultrasonic power of 60 W, hydrochloric acid concentration of 2 mol/L, temperature of 85 ℃, liquid volume to solid mass ratio of 10 mL/1 g, leaching time of 105 min, and particle size of -0.074 mm, the rare earth leaching rate reaches 97.94%, which is 8 percentage points higher than that of the conventional hydrochloric acid leaching method under its best conditions. The method is an efficient and feasible green process for rare earth recovery and provides a new approach for the resource utilization of NdFeB waste.

ultrasonic enhancement  /  NdFeB waste  /  hydrochloric acid solubilization method  /  rare earth  /  green and efficient  /  leaching
吴琦, 樊文军, 张成业, 张成成, 张晓伟, 刘中兴. 用超声强化盐酸优溶法浸出钕铁硼废料中的稀土. 湿法冶金, 2026 , 45 (2) : 208 -214 . DOI: 10.13355/j.cnki.sfyj.2026.02.010
Qi WU, Wenjun FAN, Chengye ZHANG, Chengcheng ZHANG, Xiaowei ZHANG, Zhongxing LIU. Extraction of Rare Earths from NdFeB Waste by Ultrasonic Enhanced Hydrochloric Acid Leaching Method[J]. Hydrometallurgy of China, 2026 , 45 (2) : 208 -214 . DOI: 10.13355/j.cnki.sfyj.2026.02.010
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  • 国家自然科学基金项目(51964039)
  • 内蒙古自治区自然科学基金重点联合基金项目(2025ZDLH011)
  • 自治区直属高校基本科研业务费项目(2024XKJX011)
  • 科技厅-重点研发和成果转化-科技支撑黄河流域生态保护和高质量发展项目(2025YFHH0018)
  • 科技厅-内蒙古自然科学基金-重点联合基金项目(2025ZDLH011)
  • 一流学科科研专项-重点项目(YLXKZX-NKD-002)
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2026年第45卷第2期
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doi: 10.13355/j.cnki.sfyj.2026.02.010
  • 接收时间：2025-10-27
  • 首发时间：2026-09-28
  • 出版时间：2026-04-20
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  • 收稿日期：2025-10-27
  • 修回日期：2025-12-09
基金
国家自然科学基金项目(51964039)
内蒙古自治区自然科学基金重点联合基金项目(2025ZDLH011)
自治区直属高校基本科研业务费项目(2024XKJX011)
科技厅-重点研发和成果转化-科技支撑黄河流域生态保护和高质量发展项目(2025YFHH0018)
科技厅-内蒙古自然科学基金-重点联合基金项目(2025ZDLH011)
一流学科科研专项-重点项目(YLXKZX-NKD-002)
作者信息
    1．内蒙古科技大学 稀土产业学院（稀土工程技术学院），内蒙古 包头　014010
    2．轻稀土资源全周期绿色高效开发利用教育部重点实验室（内蒙古科技大学），内蒙古 包头　014010
    3．内蒙古自治区工程研究中心，内蒙古 包头　014010

通讯作者:

樊文军（1976—），男，硕士，副教授，主要研究方向为钕铁硼绿色回收。E-mail: 。
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https://castjournals.cast.org.cn/joweb/sfyj/CN/10.13355/j.cnki.sfyj.2026.02.010
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2种不同金属材料的力学参数
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Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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