Article(id=1311349787811733752, tenantId=1146029695717560320, journalId=1146120122248306696, issueId=1311349772552859828, articleNumber=null, orderNo=null, doi=10.13355/j.cnki.sfyj.2025.06.010, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1741622400000, receivedDateStr=2025-03-11, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1790579753114, onlineDateStr=2026-09-28, pubDate=1766160000000, pubDateStr=2025-12-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1790579753114, onlineIssueDateStr=2026-09-28, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1790579753114, creator=13701087609, updateTime=1790579753114, updator=13701087609, issue=Issue{id=1311349772552859828, tenantId=1146029695717560320, journalId=1146120122248306696, year='2025', volume='44', issue='6', pageStart='707', pageEnd='838', issueExtLink='null', onlineDate='null', pubDate='1766160000000', pubDateStr='2025-12-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1790579749477, creator='13701087609', updateTime=1790588567303, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1311386757267022261, tenantId=1146029695717560320, journalId=1146120122248306696, issueId=1311349772552859828, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1311386757267022262, tenantId=1146029695717560320, journalId=1146120122248306696, issueId=1311349772552859828, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=783, endPage=790, ext={EN=ArticleExt(id=1311349788013060345, articleId=1311349787811733752, tenantId=1146029695717560320, journalId=1146120122248306696, language=EN, title=Resource Recovery of Aluminum Electrolysis Spent Carbon Anode by Phase Transformation Roasting—Water Leaching Process, columnId=1152626641181700664, journalTitle=Hydrometallurgy of China, columnName=Experiment Research, runingTitle=null, highlight=null, articleAbstract=

Extracting fluorine from aluminium electrolysis spent carbon anode by phase transformation roasting—water leaching process was studied. The effects of various factors during phase transformation roasting and water leaching on fluoride leaching rate were investigated. The results indicate that under the optimal conditions of alkali fusion temperature of 700 ℃, alkali fusion time of 2 h, alkali-to-material mass ratio of 1.25, insoluble cryolite is transformed into soluble sodium fluoride and sodium meta-aluminate phases. Under the optimal conditions of water leaching temperature of 65 ℃, liquid volume to solid mass ratio of 22/1, water leaching time of 2 h, the fluorine leaching rate achieve 95.86%. XRD analysis of the leached residue reveal that the remaining fluoride existed as calcium fluoride. The soluble fluorine mass concentration in the residue is 48 mg/L, which can meet the harmless requirements. The harmless and resourceful recovery of carbon residue can be achieved by converting the fluoride occurrence form through calcination and combining it with a one-step water leaching process. The method offers advantages such as a simple process flow, rapid reaction kinetics, high treatment efficiency, and promising industrial application prospects.

, authors=Shuang SHENG¹, Lutong MA^{2, 3}, Yan LIN^{2, 3, 4}, authorsList=Shuang SHENG, Lutong MA, Yan LIN, authorCompany=null, correspAuthors=Yan LIN, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1311349788323438842, articleId=1311349787811733752, tenantId=1146029695717560320, journalId=1146120122248306696, language=CN, title=相变转化焙烧—水浸资源化回收铝电解炭渣试验研究, columnId=1152626641328501305, journalTitle=湿法冶金, columnName=试验研究, runingTitle=null, highlight=null, articleAbstract=

研究了用相变转化焙烧—水浸工艺从铝电解炭渣中提取氟，考察了相变转化焙烧和水浸过程中各因素对氟化物浸出率的影响。结果表明：在碱熔温度700 ℃、碱熔时间2 h、碱料质量比为1.25最佳条件下，氟化物由不溶性冰晶石相转化为可溶性氟化钠和偏铝酸钠相；在水浸温度65 ℃、液固体积质量比22/1、水浸时间2 h最佳条件下，氟浸出率达95.86%。浸出渣XRD物相分析结果表明，渣中残留的氟化物为氟化钙；浸出渣中可溶性氟质量浓度为48 mg/L，可满足无害化要求。通过焙烧转化氟化物赋存形态，再结合一步水浸工艺，可实现炭渣无害化和资源化回收。该工艺具有流程简单、反应速度快、处理效率高等优点，具有良好的工业化应用前景。

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盛双（1984—），女，硕士研究生，工程师，主要研究方向为生态学。

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盛双（1984—），女，硕士研究生，工程师，主要研究方向为生态学。

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