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The hydrometallurgical process route of "alkaline conversion-acidic lead extraction-sulfuric acid lead separation" was studied for the separation and enrichment of lead from copper smelting slag. The principle of efficient transformation of lead in slag was mainly explored, and the effects of various factors in each process on the transformation, leaching and precipitation of lead were investigated. The optimal experimental conditions for each process were determined. The results show that by adding NaOH, the higher free alkalinity will cause PbSO₄ in the slag to enter the liquid phase in the form of plumbous acid, increasing lead loss and reducing recovery rate. In the acidic extraction stage, the reaction time and free acidity have a significant impact on the leaching rate. Under the conditions of free alkalinity of 15 g/L, liquid volume to solid mass ratio of 5/1, and temperature of 30 ℃, the alkaline transformation reaction is carried out for 3 h. Then, under the conditions of free acidity of 20 g/L, liquid volume to solid mass ratio of 5/1, and atemperature of 30 ℃, the slag are leached with nitric acid for 2 h. Finally, lead is precipitated with sulfuric acid under the conditions of a sulfuric acid coefficient of 0.8 to 1.0 and temperature of 30 ℃. The conversion rate and leaching rate of Pb in the slag can both reach over 95%. The process can efficiently separate and enrich lead from copper smelting slag, and the effect is good.

, authors=Taili XIE¹, Xiaolong LI², Zhaorong LUO¹, authorsList=Taili XIE, Xiaolong LI, Zhaorong LUO, authorCompany=null, correspAuthors=Xiaolong LI, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1311349786045939916, articleId=1311349785433571530, tenantId=1146029695717560320, journalId=1146120122248306696, language=CN, title=铜冶炼尾渣中铅的湿法分离富集研究, columnId=1152626641328501305, journalTitle=湿法冶金, columnName=试验研究, runingTitle=null, highlight=null, articleAbstract=

研究了采用“碱性转型—硝酸浸出—硫酸沉淀”的湿法工艺路线从铜冶炼尾渣中分离富集铅，重点探讨了尾渣中铅的高效转型原理，考察了各工序相关因素对铅转型、浸出、沉淀的影响，并确定了各工序的最佳试验条件。结果表明：加入NaOH，游离碱度升高，会使尾渣中的PbSO₄以铅酸根形式进入液相中，增加铅损失，降低回收率；硝酸浸出过程中，反应时间与游离酸度对铅浸出率影响较大；在游离碱度15 g/L、液固体积质量比5/1、温度30 ℃下碱性转型反应3 h，再在游离酸度20 g/L、液固体积质量比5/1、温度30 ℃下用硝酸浸出2 h，最后在硫酸系数为0.8~1.0、温度30 ℃条件下用硫酸沉淀铅，尾渣中铅转化率与浸出率均可达95%以上。该工艺能实现铜冶炼尾渣中铅的高效分离富集，效果较好。

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谢太李（1984—），男，本科，高级工程师，主要研究方向为稀贵稀散金属提取。

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谢太李（1984—），男，本科，高级工程师，主要研究方向为稀贵稀散金属提取。

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