Article(id=1308543995589001701, tenantId=1146029695717560320, journalId=1146120122248306696, issueId=1308543982137860950, articleNumber=null, orderNo=null, doi=10.13355/j.cnki.sfyj.2025.05.012, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1730995200000, receivedDateStr=2024-11-08, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1789910800120, onlineDateStr=2026-09-20, pubDate=1760889600000, pubDateStr=2025-10-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1789910800120, onlineIssueDateStr=2026-09-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1789910800120, creator=13701087609, updateTime=1789910800120, updator=13701087609, issue=Issue{id=1308543982137860950, tenantId=1146029695717560320, journalId=1146120122248306696, year='2025', volume='44', issue='5', pageStart='583', pageEnd='705', issueExtLink='null', onlineDate='null', pubDate='1760889600000', pubDateStr='2025-10-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1789910796911, creator='13701087609', updateTime=1789955335202, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1308730789341266049, tenantId=1146029695717560320, journalId=1146120122248306696, issueId=1308543982137860950, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1308730789341266050, tenantId=1146029695717560320, journalId=1146120122248306696, issueId=1308543982137860950, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=666, endPage=671, ext={EN=ArticleExt(id=1308543995798716902, articleId=1308543995589001701, tenantId=1146029695717560320, journalId=1146120122248306696, language=EN, title=Reduction and Sulfation of Waste Lead Paste by Glucose-Sulfuric Acid System, columnId=1152626641181700664, journalTitle=Hydrometallurgy of China, columnName=Experiment Research, runingTitle=null, highlight=null, articleAbstract=

The composition and physicochemical properties of waste lead paste are complex, and its recycling and utilization are difficult. Among them, the reduction of high-valent PbO₂ is a key problem in the recycling and treatment process of waste lead paste. The reduction sulfation reaction of converting PbO₂ in waste lead paste to PbSO₄ using the glucose-sulfuric acid system at room temperature was studied. The effects of sulfuric acid concentration, glucose excess coefficient, liquid volume to solid mass ratio and reaction time on the reduction sulfation process of waste lead paste were investigated. The results show that under the optimal reaction conditions of waste lead paste of 5 g, sulfuric acid concentration of 85%, excess coefficient of glucose of 3, liquid volume to solid mass ratio of 3/1, and reaction time of 3 h, the reduction rate of PbO₂ is 91.88% and the mass fraction of PbSO₄ is 92.52%. The system can reduce and sulfate various complex components in waste lead paste to obtain PbSO₄ products of higher purity. It is green and efficient, and convenient for the subsequent recycling and treatment of waste lead paste.

, authors=Meimei PAN¹, Kui HUANG^{1, 2}, Haili DONG^{1, 2}, Zhangqing CHEN¹, Shanjin MAO¹, authorsList=Meimei PAN, Kui HUANG, Haili DONG, Zhangqing CHEN, Shanjin MAO, authorCompany=null, correspAuthors=Kui HUANG, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1308543996142649831, articleId=1308543995589001701, tenantId=1146029695717560320, journalId=1146120122248306696, language=CN, title=葡萄糖-硫酸体系对废铅膏的还原硫酸化研究, columnId=1152626641328501305, journalTitle=湿法冶金, columnName=试验研究, runingTitle=null, highlight=null, articleAbstract=

废铅膏的成分和理化性质复杂，回收利用困难，其中高价态PbO₂的还原更是废铅膏回收处理过程的关键难题。研究了在常温下，用葡萄糖-硫酸体系使废铅膏中的PbO₂转化为PbSO₄的还原硫酸化反应，考察了硫酸浓度、葡萄糖过量系数、液固体积质量比和反应时间对废铅膏还原硫酸化过程的影响。结果表明：取废铅膏5 g，在硫酸浓度85%、葡萄糖过量系数为3、液固体积质量比3/1、反应时间3 h的最佳反应条件下，PbO₂还原率为91.88%，PbSO₄质量分数为92.52%。该体系可将废铅膏中多种复杂成分还原硫酸化得到较高纯度的PbSO₄产物，绿色高效，方便废铅膏的后续回收处理。

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潘媚媚（1999—），女，硕士研究生，主要研究方向为铅酸蓄电池的资源化回收利用。

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潘媚媚（1999—），女，硕士研究生，主要研究方向为铅酸蓄电池的资源化回收利用。

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