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Recycling spent LiFePO₄ batteries is crucial for mitigating resource shortages and lowering environmental pollution. Leaching lithium from the spent LiFePO₄ batteries using succinic acid-hydrogen peroxide system was investigated. The effects of succinic acid concentration, hydrogen peroxide volume fraction, solid mass to liquid volume ratio, leaching temperature and time on lithium leaching rate were examined. The leaching mechanism was further clarified through kinetic analysis and SEM. The results indicate that under the optimal leaching conditions of succinic acid of 0.8 mol/L, hydrogen peroxide of 2%, solid mass to liquid volume ratio of 4 mg/1 mL, leaching temperature of 80 ℃, and time of 40 min, the conditions, lithium leaching rate is more than 98%, while iron leaching rate is less than 2%. Kinetic analysis reveals that the leaching process is primarily diffusion-controlled. Overall, these findings demonstrate that the synergistic succinic acid-hydrogen peroxide system offers high efficiency and sustainability in LiFePO₄ leaching, providing a feasible route for the green recycling of spent LiFePO₄ batteries.

, authors=Pengfei YANG, Huichen LIANG, Wanli LU, Youming YE, Xuezhen XIE, Yanmeng CHEN, Xiaoshu WANG, authorsList=Pengfei YANG, Huichen LIANG, Wanli LU, Youming YE, Xuezhen XIE, Yanmeng CHEN, Xiaoshu WANG, authorCompany=null, correspAuthors=Xiaoshu WANG, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1305178375602066121, articleId=1305178374759011015, tenantId=1146029695717560320, journalId=1146120122248306696, language=CN, title=丁二酸与过氧化氢协同作用在废旧磷酸铁锂电池回收中的应用研究, columnId=1152626641328501305, journalTitle=湿法冶金, columnName=试验研究, runingTitle=null, highlight=null, articleAbstract=

废旧磷酸铁锂电池的回收对缓解资源短缺和降低环境污染具有重要意义。研究了用丁二酸/过氧化氢体系从废旧磷酸铁锂电池中回收锂，考察了浸出过程中丁二酸浓度、过氧化氢添加量、液固体积质量比、浸出温度和时间对锂浸出率的影响，并通过动力学分析和扫描电子显微镜（SEM）表征，揭示了浸出机制。试验结果表明，在丁二酸浓度0.8 mol/L、过氧化氢添加量为2%、液固体积质量比为4 mg/1 mL、浸出温度80 ℃、浸出时间40 min最佳条件下，Li浸出率达98%以上，而Fe浸出率仅在2%以内。动力学分析结果表明，浸出过程主要受内扩散控制。该体系具有高效性与可持续性，可为实现废旧磷酸铁锂电池的绿色回收提供一种可行路径。

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杨鹏飞（1993—），男，硕士，讲师，主要研究方向为湿法冶金。

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杨鹏飞（1993—），男，硕士，讲师，主要研究方向为湿法冶金。

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