Article(id=1160646992850931932, tenantId=1146029695717560320, journalId=1146120122248306696, issueId=1148109987349520431, articleNumber=1009-2617(2025)01-0010-07, orderNo=null, doi=10.13355/j.cnki.sfyj.2025.01.002, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1727193600000, receivedDateStr=2024-09-25, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1754649406874, onlineDateStr=2025-08-08, pubDate=1740672000000, pubDateStr=2025-02-28, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1754649406874, onlineIssueDateStr=2025-08-08, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1754649406874, creator=13701087609, updateTime=1754649406874, updator=13701087609, issue=Issue{id=1148109987349520431, tenantId=1146029695717560320, journalId=1146120122248306696, year='2025', volume='44', issue='1', pageStart='1', pageEnd='131', issueExtLink='null', onlineDate='null', pubDate='null', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1751660351836, creator=13701087609, updateTime=1758246034872, updator=13701087609, preIssue=null, nextIssue=null, ext={EN=IssueExt(id=1175732344108499276, tenantId=1146029695717560320, journalId=1146120122248306696, issueId=1148109987349520431, language=EN, specialIssueTitle=, coverIllustrator=, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1175732344108499277, tenantId=1146029695717560320, journalId=1146120122248306696, issueId=1148109987349520431, language=CN, specialIssueTitle=, coverIllustrator=, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null}, startPage=10, endPage=16, ext={EN=ArticleExt(id=1160646993085812958, articleId=1160646992850931932, tenantId=1146029695717560320, journalId=1146120122248306696, language=EN, title=Preparation of Yellowcake by Vacuum Filtration Dewatering of Precipitation Slurry from In-Situ Leaching Uranium Mine, columnId=1152626641181700664, journalTitle=Hydrometallurgy of China, columnName=Experiment Research, runingTitle=null, highlight=null, articleAbstract=
In order to solve the issue of low automation in the hydrometallurgical process in in-situ leaching of uranium, especially in the preparation of yellowcake from precipitation slurry using plate and frame filter presses, a horizontal belt vacuum filter was selected for the first time in an in-situ leaching of uranium mine to conduct a filtration dewatering experiment on sodium diuranate precipitation slurry. The influence of different operating conditions on moisture content of yellow cake products was investigated. The results show that under the conditions of a filtration vacuum of -0.06~-0.08 MPa, a filter cloth precision of 38 μm, a slurry residence time of 640 s, a feed flow rate of 353~589 kg/h, and a backwash and sealing circulation water flowrate of 10 m3/h, the entire process from cloth feeding to filtration, dewatering, cake discharge, and cloth backwashing can be automatically cycled and run continuously and stably. The product moisture content meets the first-grade standard, satisfying the dewatering capacity requirements for a mine producing about 500 t of metallic uranium per year. The technical feasibility of using belt vacuum filter to dehydrate the precipitated slurry has been preliminatively confirmed. The technical feasibility of using belt vacuum filter for dewatering the precipitation slurry has been preliminatively confirmed. The filtration dewatering process can reduce the labor intensity of operators, reduce the radiation hazard, and improve the automation of the entire hydrometallurgy process, it has value for promotion and application.
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μm、浆体停留时间640 s、进料流量353~589 kg/h、反洗及密封循环水量10 m
3/h条件下,从布料—抽滤—卸料—滤布反洗全过程可自动循环、连续稳定运行,产品含水量能达到一级品标准,满足年产500 t左右金属铀的矿山对沉淀浆体脱水能力要求,初步证实了采用带式真空过滤机对沉淀浆体进行脱水的技术可行性。该抽滤脱水工艺能减轻作业人员劳动强度,降低辐射危害,提高整个水冶流程自动化程度,具有一定推广应用价值。, correspAuthors=null, authorNote=null, correspAuthorsNote=
原渊(1986—),男,硕士,正高级工程师,主要研究方向为地浸采铀技术及管理。
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王亚安(1994—),男,博士,高级工程师,主要研究方向为地浸采铀及化工机械。
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1 Beijing Research Institute of Chemical Engineering and Metallurgy, CNNC, Beijing 101149, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1174444184279855310, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, authorId=1174444184103694539, language=CN, stringName=王亚安, firstName=null, middleName=null, lastName=null, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
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王亚安(1994—),男,博士,高级工程师,主要研究方向为地浸采铀及化工机械。
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1 Beijing Research Institute of Chemical Engineering and Metallurgy, CNNC, Beijing 101149, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1174444185517175005, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, authorId=1174444185114521818, language=CN, stringName=原渊, firstName=null, middleName=null, lastName=null, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
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2 中核铀业有限责任公司, 北京 100010, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null)}, companyList=[AuthorCompany(id=1174444183944310980, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, xref=2, ext=[AuthorCompanyExt(id=1174444183952699589, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, companyId=1174444183944310980, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=
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3 中核内蒙古矿业有限公司, 内蒙古 呼和浩特 014010, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null)}, companyList=[AuthorCompany(id=1174444184028197063, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, xref=3, ext=[AuthorCompanyExt(id=1174444184036585672, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, companyId=1174444184028197063, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=
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1 核工业北京化工冶金研究院, 北京 101149)]), AuthorCompany(id=1174444183944310980, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, xref=2, ext=[AuthorCompanyExt(id=1174444183952699589, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, companyId=1174444183944310980, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=
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2 中核铀业有限责任公司, 北京 100010)]), AuthorCompany(id=1174444184028197063, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, xref=3, ext=[AuthorCompanyExt(id=1174444184036585672, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, companyId=1174444184028197063, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=
3 CNNC Inner Mongolia Mineral Co., Ltd., Hohhot 014010, China), AuthorCompanyExt(id=1174444184040779977, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, companyId=1174444184028197063, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=
3 中核内蒙古矿业有限公司, 内蒙古 呼和浩特 014010)])], figs=[ArticleFig(id=1174444188679680259, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, language=EN, label=Fig.1, caption=
Composition schematic diagram of belt vacuum filtration system, figureFileSmall=99ZCH1A9lnJHMoIIm0bdaw==, figureFileBig=+9ttQ0Lqkg9LohoZpUGD8w==, tableContent=null), ArticleFig(id=1174444188730011908, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, language=CN, label=图1, caption=
带滤机系统组成示意, figureFileSmall=99ZCH1A9lnJHMoIIm0bdaw==, figureFileBig=+9ttQ0Lqkg9LohoZpUGD8w==, tableContent=null), ArticleFig(id=1174444188780343557, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, language=EN, label=Fig.2, caption=
Photo of belt vacuum filter, figureFileSmall=iOE0POwZSx8Qhdu0+GqexA==, figureFileBig=RHxBCTWcVuePxGRhcEwGyQ==, tableContent=null), ArticleFig(id=1174444188834869510, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, language=CN, label=图2, caption=
带滤机照片, figureFileSmall=iOE0POwZSx8Qhdu0+GqexA==, figureFileBig=RHxBCTWcVuePxGRhcEwGyQ==, tableContent=null), ArticleFig(id=1174444188935532807, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, language=EN, label=Fig.3, caption=
Operation steps of horizontal belt vacuum filtration system, figureFileSmall=xto3ujgREXEnlpJox2MQ/Q==, figureFileBig=XQfWZnhm7tJUtmX+HGBDVA==, tableContent=null), ArticleFig(id=1174444189006835976, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, language=CN, label=图3, caption=
水平带式真空过滤机系统操作步骤, figureFileSmall=xto3ujgREXEnlpJox2MQ/Q==, figureFileBig=XQfWZnhm7tJUtmX+HGBDVA==, tableContent=null), ArticleFig(id=1174444189057167625, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, language=EN, label=Fig.4, caption=
Crystal size distribution in slurry at different locations of precipitation tank, figureFileSmall=Y3el5TAjUk3tDtvpkZBYGA==, figureFileBig=5VB8cms+lYJPWc9nPegOtA==, tableContent=null), ArticleFig(id=1174444189115887882, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, language=CN, label=图4, caption=
沉淀罐不同部位浆体中晶体粒径分布, figureFileSmall=Y3el5TAjUk3tDtvpkZBYGA==, figureFileBig=5VB8cms+lYJPWc9nPegOtA==, tableContent=null), ArticleFig(id=1174444189174608139, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, language=EN, label=Fig.5, caption=
Filter through phenomenon of slurry with 75 μm precision filter cloth, figureFileSmall=mIIecU9GjIjQSSDTE/r0cA==, figureFileBig=0cF5FMN8hjknLUcG9wTbAg==, tableContent=null), ArticleFig(id=1174444189224939788, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, language=CN, label=图5, caption=
使用75 μm精度滤布时浆体的穿滤现象 a—真空抽滤管道;b—气液分离罐。
, figureFileSmall=mIIecU9GjIjQSSDTE/r0cA==, figureFileBig=0cF5FMN8hjknLUcG9wTbAg==, tableContent=null), ArticleFig(id=1174444189287854349, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, language=EN, label=Fig.6, caption=
Appearance of filter cake with 38 μm precision filter cloth, figureFileSmall=7TE6a25hQLT6g17hPFsZFw==, figureFileBig=/Sl7I3rpIetlU32r3NsTcQ==, tableContent=null), ArticleFig(id=1174444189346574606, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, language=CN, label=图6, caption=
使用38 μm精度滤布时的滤饼样貌, figureFileSmall=7TE6a25hQLT6g17hPFsZFw==, figureFileBig=/Sl7I3rpIetlU32r3NsTcQ==, tableContent=null), ArticleFig(id=1174444189413683471, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, language=EN, label=Fig.7, caption=
Appearance of slurry and filter cake with different residence times a—120 s;b—360 s;c—750 s。
, figureFileSmall=FQ3QQOhV+0oG5Dnj0deDPQ==, figureFileBig=npLHOszs+Lo94jvOXArD+g==, tableContent=null), ArticleFig(id=1174444189526929680, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, language=CN, label=图7, caption=
不同停留时间下浆体及滤饼样貌, figureFileSmall=FQ3QQOhV+0oG5Dnj0deDPQ==, figureFileBig=npLHOszs+Lo94jvOXArD+g==, tableContent=null), ArticleFig(id=1174444189594038545, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, language=EN, label=Table 1, caption=
Main configuration and parameters of experimental belt vacuum filtration system
, figureFileSmall=null, figureFileBig=null, tableContent=
| 配置 | 参数 | 备注 |
| 带滤机主体 | 尺寸:7 580 mm×1 130 mm×1 360 mm | |
| 带滤机驱动电机 | 功率:4 kW | 系统自带 |
| 环形滤布 | 总长:17.7 m;宽度:73 mm | 孔隙直径可选 |
| 抽滤区 | 长度:3 300 mm | 滤布有效宽度50 mm |
| 2BEA202型真空泵 | 功率:18.5 kW | 系统自带 |
| 气液分离罐 | ϕ630 mm×2 170 mm | 系统自带,含气控阀 |
| 母液罐 | ϕ1 640 mm×950 mm | 新配置,供应洗水和冷却水 |
| LQF50型渣浆泵 | 流量:10 m3/h;扬程:80 m | 新配置 |
), ArticleFig(id=1174444189656953106, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, language=CN, label=表1, caption=
试验用带滤机系统的主要配置及参数
, figureFileSmall=null, figureFileBig=null, tableContent=
| 配置 | 参数 | 备注 |
| 带滤机主体 | 尺寸:7 580 mm×1 130 mm×1 360 mm | |
| 带滤机驱动电机 | 功率:4 kW | 系统自带 |
| 环形滤布 | 总长:17.7 m;宽度:73 mm | 孔隙直径可选 |
| 抽滤区 | 长度:3 300 mm | 滤布有效宽度50 mm |
| 2BEA202型真空泵 | 功率:18.5 kW | 系统自带 |
| 气液分离罐 | ϕ630 mm×2 170 mm | 系统自带,含气控阀 |
| 母液罐 | ϕ1 640 mm×950 mm | 新配置,供应洗水和冷却水 |
| LQF50型渣浆泵 | 流量:10 m3/h;扬程:80 m | 新配置 |
), ArticleFig(id=1174444189724061971, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, language=EN, label=Table 2, caption=
variation of crystal size parameters in the precipitated slurry corresponding to different circulation times
, figureFileSmall=null, figureFileBig=null, tableContent=
| 循环次数 | 粒径范围/μm | 平均粒径/μm | 峰值粒径/μm | D90/μm |
| 1 | 0.195~19.16 | 3.247 | 4.080 | 7.865 |
| 10 | 0.195~41.91 | 4.672 | 1.108 | 15.72 |
| 15 | 0.195~52.41 | 6.825 | 0.993 | 22.42 |
| 20 | 0.195~52.41 | 6.146 | 0.714 | 21.26 |
| 25 | 0.195~52.41 | 6.166 | 0.715 | 20.84 |
| 30 | 0.195~52.41 | 6.202 | 0.781 | 21.68 |
), ArticleFig(id=1174444189799559444, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, language=CN, label=表2, caption=
不同循环次数下沉淀浆体中晶体粒径参数变化
, figureFileSmall=null, figureFileBig=null, tableContent=
| 循环次数 | 粒径范围/μm | 平均粒径/μm | 峰值粒径/μm | D90/μm |
| 1 | 0.195~19.16 | 3.247 | 4.080 | 7.865 |
| 10 | 0.195~41.91 | 4.672 | 1.108 | 15.72 |
| 15 | 0.195~52.41 | 6.825 | 0.993 | 22.42 |
| 20 | 0.195~52.41 | 6.146 | 0.714 | 21.26 |
| 25 | 0.195~52.41 | 6.166 | 0.715 | 20.84 |
| 30 | 0.195~52.41 | 6.202 | 0.781 | 21.68 |
), ArticleFig(id=1174444189862474005, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, language=EN, label=Table 3, caption=
Effect of filter cloth precision on the moisture content of yellow cake products
, figureFileSmall=null, figureFileBig=null, tableContent=
| 滤布精度/μm | 穿滤情况 | 压力/MPa | 停留时间/s | 滤饼厚度/mm | 产品中w(水)/% |
| 75 | 严重 | -0.05~-0.06 | 640 | 4 | 27.87 |
| 48 | 少量 | -0.06~-0.07 | 640 | 4 | 28.20 |
| 38 | 微量 | -0.06~-0.08 | 640 | 5 | 25.86 |
), ArticleFig(id=1174444189925388566, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, language=CN, label=表3, caption=
滤布精度对黄饼产品含水量的影响
, figureFileSmall=null, figureFileBig=null, tableContent=
| 滤布精度/μm | 穿滤情况 | 压力/MPa | 停留时间/s | 滤饼厚度/mm | 产品中w(水)/% |
| 75 | 严重 | -0.05~-0.06 | 640 | 4 | 27.87 |
| 48 | 少量 | -0.06~-0.07 | 640 | 4 | 28.20 |
| 38 | 微量 | -0.06~-0.08 | 640 | 5 | 25.86 |
), ArticleFig(id=1174444190026051863, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, language=EN, label=Table 4, caption=
Effect of residence time on moisture content of yellow cake products
, figureFileSmall=null, figureFileBig=null, tableContent=
| 停留时间/s | 滤布精度/μm | 压力/MPa | 滤饼厚度/mm | 产品中w(水)/% |
| 120 | 38 | -(0.04~0.05) | | |
| 360 | 38 | -(0.06~0.08) | 4 | 34.57 |
| 640 | 38 | -(0.06~0.08) | 5 | 25.86 |
| 750 | 38 | -(0.05~0.07) | 5 | 25.32 |
), ArticleFig(id=1174444190105743640, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, language=CN, label=表4, caption=
停留时间对黄饼产品含水量的影响
, figureFileSmall=null, figureFileBig=null, tableContent=
| 停留时间/s | 滤布精度/μm | 压力/MPa | 滤饼厚度/mm | 产品中w(水)/% |
| 120 | 38 | -(0.04~0.05) | | |
| 360 | 38 | -(0.06~0.08) | 4 | 34.57 |
| 640 | 38 | -(0.06~0.08) | 5 | 25.86 |
| 750 | 38 | -(0.05~0.07) | 5 | 25.32 |
), ArticleFig(id=1174444190235767065, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, language=EN, label=Table 5, caption=
Effect of feed flow rate on the moisture content of yellow cake products
, figureFileSmall=null, figureFileBig=null, tableContent=
| 进料流量/(kg·h-1) | 滤布精度/μm | 压力/MPa | 停留时间/s | 滤饼厚度/mm | 产品中w(水)/% |
| 353.39 | 38 | -0.05~-0.07 | 640 | 3 | 28.22 |
| 471.18 | 38 | -0.06~-0.08 | 640 | 4 | 25.99 |
| 588.98 | 38 | -0.06~-0.08 | 640 | 5 | 25.86 |
| 706.78 | 38 | -0.06~-0.08 | 640 | 6 | 30.55 |
| 824.58 | 38 | -0.06~-0.08 | 640 | 7 | 32.25 |
), ArticleFig(id=1174444190336430362, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, language=CN, label=表5, caption=
进料流量对黄饼产品含水量的影响
, figureFileSmall=null, figureFileBig=null, tableContent=
| 进料流量/(kg·h-1) | 滤布精度/μm | 压力/MPa | 停留时间/s | 滤饼厚度/mm | 产品中w(水)/% |
| 353.39 | 38 | -0.05~-0.07 | 640 | 3 | 28.22 |
| 471.18 | 38 | -0.06~-0.08 | 640 | 4 | 25.99 |
| 588.98 | 38 | -0.06~-0.08 | 640 | 5 | 25.86 |
| 706.78 | 38 | -0.06~-0.08 | 640 | 6 | 30.55 |
| 824.58 | 38 | -0.06~-0.08 | 640 | 7 | 32.25 |
), ArticleFig(id=1174444190474842395, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, language=EN, label=Table 6, caption=
Measurement results of wet yellow cake density
, figureFileSmall=null, figureFileBig=null, tableContent=
| 序号 | 黄饼质量/g | V1/mL | V2/mL | ρ/(kg·m-3) |
| 1 | 56.16 | 100 | 115 | 3 744 |
| 2 | 61.55 | 100 | 118 | 3 419 |
| 3 | 80.41 | 150 | 175 | 3 655 |
), ArticleFig(id=1174444190600671516, tenantId=1146029695717560320, journalId=1146120122248306696, articleId=1160646992850931932, language=CN, label=表6, caption=
湿黄饼密度的测定结果
, figureFileSmall=null, figureFileBig=null, tableContent=
| 序号 | 黄饼质量/g | V1/mL | V2/mL | ρ/(kg·m-3) |
| 1 | 56.16 | 100 | 115 | 3 744 |
| 2 | 61.55 | 100 | 118 | 3 419 |
| 3 | 80.41 | 150 | 175 | 3 655 |
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