Article(id=1305177742874530340, tenantId=1146029695717560320, journalId=1146120122248306696, issueId=1305177706027578094, articleNumber=null, orderNo=null, doi=10.13355/j.cnki.sfyj.2026.04.013, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1769443200000, receivedDateStr=2026-01-27, revisedDate=1775491200000, revisedDateStr=2026-04-07, acceptedDate=null, acceptedDateStr=null, onlineDate=1789108222931, onlineDateStr=2026-09-11, pubDate=1787155200000, pubDateStr=2026-08-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1789108222931, onlineIssueDateStr=2026-09-11, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1789108222931, creator=13701087609, updateTime=1789108222931, updator=13701087609, issue=Issue{id=1305177706027578094, tenantId=1146029695717560320, journalId=1146120122248306696, year='2026', volume='45', issue='4', pageStart='455', pageEnd='612', issueExtLink='null', onlineDate='null', pubDate='1787155200000', pubDateStr='2026-08-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=1, specialIssue=null, createTime=1789108214146, creator='13701087609', updateTime=1789108456673, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1305178723335037263, tenantId=1146029695717560320, journalId=1146120122248306696, issueId=1305177706027578094, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1305178723335037264, tenantId=1146029695717560320, journalId=1146120122248306696, issueId=1305177706027578094, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=565, endPage=573, ext={EN=ArticleExt(id=1305177743080051237, articleId=1305177742874530340, tenantId=1146029695717560320, journalId=1146120122248306696, language=EN, title=Preparation Technology of High purity and High Dispersion Platinum Powder by Chemical Liquid Phase Reduction Method, columnId=1152626641181700664, journalTitle=Hydrometallurgy of China, columnName=Experiment Research, runingTitle=null, highlight=null, articleAbstract=

In order to accurately control the reduction, nucleation and growth process of platinum atoms in the preparation of high purity and high dispersion platinum powder, high purity and high dispersion platinum powder was prepared by chemical liquid phase reduction method with Na2PtCl6 aqueous solution as precursor, N2H4·H2O as reducing agent and PVP as dispersant. The effects of temperature, reaction system and feeding method on the morphology, particle size distribution and dispersion of platinum powder were investigated. The results show that the nucleation and growth process of platinum atoms can be effectively separated by using PVP as the dispersion system and Na2PtCl6 and N2H4·H2O as the synchronous feeding method at 80 ℃. The high purity and high dispersion micron platinum powder with good dispersion and narrow particle size distribution (D90-D10=1.18 μm) is prepared. This method provides a reliable theoretical basis and technical path for the stable and mass production of high purity and high dispersion micron platinum powder.

, authors=Sheng TAN1, 2, Wanning ZHANG1, 2, Lei LIAO1, 2, Xiangrong XIANG1, 2, Shihao WAN1, 2, Yi YUAN1, 2, Yucheng XIAO1, 2, authorsList=Sheng TAN, Wanning ZHANG, Lei LIAO, Xiangrong XIANG, Shihao WAN, Yi YUAN, Yucheng XIAO, authorCompany=null, correspAuthors=null, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1305177743595950630, articleId=1305177742874530340, tenantId=1146029695717560320, journalId=1146120122248306696, language=CN, title=化学液相还原法制备高纯高分散铂粉技术研究, columnId=1152626641328501305, journalTitle=湿法冶金, columnName=试验研究, runingTitle=null, highlight=null, articleAbstract=

为精准控制高纯高分散铂粉制备过程中的铂原子还原、成核与生长过程,研究了采用化学液相还原法,以Na2PtCl6水溶液为前驱体、N2H4·H2O为还原剂、PVP为分散剂制备高纯高分散铂粉。考察了温度、反应体系及加料方式等因素对铂粉形貌、粒度分布及分散性的影响。结果表明:在80 ℃条件下,以PVP为分散体系,采用Na2PtCl6与N2H4·H2O同步加料的方式,能有效分离铂原子的形核与长大过程,制备出分散性良好、粒度分布窄(D90-D10=1.18 μm)的高纯高分散微米铂粉。该方法为高纯高分散微米铂粉的稳定、批量化生产提供了可靠的理论依据与技术路径。

, authors=谭生1, 2, 张婉宁1, 2, 廖磊1, 2, 向祥蓉1, 2, 万仕豪1, 2, 袁翌1, 2, 肖雨辰1, 2, authorsList=谭生, 张婉宁, 廖磊, 向祥蓉, 万仕豪, 袁翌, 肖雨辰, authorCompany=null, correspAuthors=null, authorNote=

谭生(1984—),男,博士,工程师,主要研究方向为贵金属粉体材料制备技术研究及应用推广。

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谭生(1984—),男,博士,工程师,主要研究方向为贵金属粉体材料制备技术研究及应用推广。

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谭生(1984—),男,博士,工程师,主要研究方向为贵金属粉体材料制备技术研究及应用推广。

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化学液相还原法制备高纯高分散铂粉技术研究
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谭生 1, 2 , 张婉宁 1, 2 , 廖磊 1, 2 , 向祥蓉 1, 2 , 万仕豪 1, 2 , 袁翌 1, 2 , 肖雨辰 1, 2
湿法冶金 | 试验研究 2026,45(4): 565-573
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湿法冶金 |试验研究 2026 , 45 (4) : 565 -573
化学液相还原法制备高纯高分散铂粉技术研究
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谭生(1984—),男,博士,工程师,主要研究方向为贵金属粉体材料制备技术研究及应用推广。

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谭生(1984—),男,博士,工程师,主要研究方向为贵金属粉体材料制备技术研究及应用推广。

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谭生1, 2, 张婉宁1, 2, 廖磊1, 2, 向祥蓉1, 2, 万仕豪1, 2, 袁翌1, 2, 肖雨辰1, 2
作者信息
  • 1.重庆材料研究院有限公司,重庆 400707
  • 2.国家仪表功能材料工程技术研究中心,重庆 400707
作者简介:

谭生(1984—),男,博士,工程师,主要研究方向为贵金属粉体材料制备技术研究及应用推广。

Preparation Technology of High purity and High Dispersion Platinum Powder by Chemical Liquid Phase Reduction Method
Sheng TAN1, 2, Wanning ZHANG1, 2, Lei LIAO1, 2, Xiangrong XIANG1, 2, Shihao WAN1, 2, Yi YUAN1, 2, Yucheng XIAO1, 2
Affiliations
  • 1.Chongqing Materials Research Institute Co., Ltd., Chongqing 400707, China
  • 2.National Engineering Research Center for Instrument Functional Materials, Chongqing 400707, China
出版时间: 2026-08-20 doi: 10.13355/j.cnki.sfyj.2026.04.013
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为精准控制高纯高分散铂粉制备过程中的铂原子还原、成核与生长过程,研究了采用化学液相还原法,以Na2PtCl6水溶液为前驱体、N2H4·H2O为还原剂、PVP为分散剂制备高纯高分散铂粉。考察了温度、反应体系及加料方式等因素对铂粉形貌、粒度分布及分散性的影响。结果表明:在80 ℃条件下,以PVP为分散体系,采用Na2PtCl6与N2H4·H2O同步加料的方式,能有效分离铂原子的形核与长大过程,制备出分散性良好、粒度分布窄(D90-D10=1.18 μm)的高纯高分散微米铂粉。该方法为高纯高分散微米铂粉的稳定、批量化生产提供了可靠的理论依据与技术路径。

铂粉  /  制备  /  化学液相法  /  还原  /  分散性  /  高纯

In order to accurately control the reduction, nucleation and growth process of platinum atoms in the preparation of high purity and high dispersion platinum powder, high purity and high dispersion platinum powder was prepared by chemical liquid phase reduction method with Na2PtCl6 aqueous solution as precursor, N2H4·H2O as reducing agent and PVP as dispersant. The effects of temperature, reaction system and feeding method on the morphology, particle size distribution and dispersion of platinum powder were investigated. The results show that the nucleation and growth process of platinum atoms can be effectively separated by using PVP as the dispersion system and Na2PtCl6 and N2H4·H2O as the synchronous feeding method at 80 ℃. The high purity and high dispersion micron platinum powder with good dispersion and narrow particle size distribution (D90-D10=1.18 μm) is prepared. This method provides a reliable theoretical basis and technical path for the stable and mass production of high purity and high dispersion micron platinum powder.

platinum powder  /  preparation  /  chemical liquid phase method  /  reduction  /  dispersion  /  high purity
谭生, 张婉宁, 廖磊, 向祥蓉, 万仕豪, 袁翌, 肖雨辰. 化学液相还原法制备高纯高分散铂粉技术研究. 湿法冶金, 2026 , 45 (4) : 565 -573 . DOI: 10.13355/j.cnki.sfyj.2026.04.013
Sheng TAN, Wanning ZHANG, Lei LIAO, Xiangrong XIANG, Shihao WAN, Yi YUAN, Yucheng XIAO. Preparation Technology of High purity and High Dispersion Platinum Powder by Chemical Liquid Phase Reduction Method[J]. Hydrometallurgy of China, 2026 , 45 (4) : 565 -573 . DOI: 10.13355/j.cnki.sfyj.2026.04.013
  • 重庆市技术创新与发展专项重点项目(CSTB2022TIAD-KPX0026)
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2026年第45卷第4期
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doi: 10.13355/j.cnki.sfyj.2026.04.013
  • 接收时间:2026-01-27
  • 首发时间:2026-09-11
  • 出版时间:2026-08-20
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  • 收稿日期:2026-01-27
  • 修回日期:2026-04-07
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重庆市技术创新与发展专项重点项目(CSTB2022TIAD-KPX0026)
作者信息
    1.重庆材料研究院有限公司,重庆 400707
    2.国家仪表功能材料工程技术研究中心,重庆 400707
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2种不同金属材料的力学参数

Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)

Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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