Article(id=1305177720460173838, tenantId=1146029695717560320, journalId=1146120122248306696, issueId=1305177706027578094, articleNumber=null, orderNo=null, doi=10.13355/j.cnki.sfyj.2026.04.007, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1776960000000, receivedDateStr=2026-04-24, revisedDate=1779033600000, revisedDateStr=2026-05-18, acceptedDate=null, acceptedDateStr=null, onlineDate=1789108217587, onlineDateStr=2026-09-11, pubDate=1787155200000, pubDateStr=2026-08-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1789108217587, onlineIssueDateStr=2026-09-11, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1789108217587, creator=13701087609, updateTime=1789108217587, updator=13701087609, issue=Issue{id=1305177706027578094, tenantId=1146029695717560320, journalId=1146120122248306696, year='2026', volume='45', issue='4', pageStart='455', pageEnd='612', issueExtLink='null', onlineDate='null', pubDate='1787155200000', pubDateStr='2026-08-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=1, specialIssue=null, createTime=1789108214146, creator='13701087609', updateTime=1789108456673, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1305178723335037263, tenantId=1146029695717560320, journalId=1146120122248306696, issueId=1305177706027578094, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1305178723335037264, tenantId=1146029695717560320, journalId=1146120122248306696, issueId=1305177706027578094, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=510, endPage=520, ext={EN=ArticleExt(id=1305177720678277647, articleId=1305177720460173838, tenantId=1146029695717560320, journalId=1146120122248306696, language=EN, title=Antimony Diaphragm Electrorefining Technology and Impurity Removal Based on Tartrate Salt System, columnId=1152626641181700664, journalTitle=Hydrometallurgy of China, columnName=Experiment Research, runingTitle=null, highlight=null, articleAbstract=

An antimony diaphragm electrorefining technology suitable for tartrate system was developed using refined antimony as raw material. The effects of different diaphragm types and electrolysis process parameters including current density, electrolysis temperature, electrolyte circulation speed and electrode spacing on cathode current efficiency, cell voltage, direct current consumption, cathode antimony purity and typical impurity removal rate are systematically investigated. The optimum process conditions are determined as follows:tartrate ion mass concentration is 250 g/L, antimony ion mass concentration is 45 g/L, current density is 150 A/m², electrolysis temperature is 35 ℃, electrolyte circulation speed is 300 mL/min, electrode spacing is 70 mm. The research results show that according to the single point impurity content requirements of 5N grade high purity antimony in the national standard' high purity antimony' (GB/T 10117—2021), the impurities that are easy to exceed the standard in the antimony tartrate electrolysis system are mainly arsenic, bismuth, lead and copper. Only regulating the electrolysis process conditions can not achieve the deep removal of the above impurities. Further electrolyte purification measures are needed to ensure the batch stability of high purity antimony products, while the remaining 16 main control impurities can meet the requirements of the national standard Sb-05 by electrolytic refining. Under the optimal electrolysis conditions, the electrolyte is deeply purified with antimony-based adsorbent (polyhydroxyantimonic acid with the main phase of H₁₄Sb₁₄O₂₁(OH)₄₂) to obtain cathode antimony with a purity of 99.995% and a dense and bright surface. The average cell voltage is 0.808 V, the current efficiency is 96.27%, and the direct current consumption is 485.85 kWh/t.

, authors=Xingrui TAO^{1, 2, 3}, Yu WANG^{1, 2, 3}, Guangping WANG^{1, 2, 3}, Yan LIN^{1, 2, 3}, authorsList=Xingrui TAO, Yu WANG, Guangping WANG, Yan LIN, authorCompany=null, correspAuthors=Yan LIN, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1305177720963490320, articleId=1305177720460173838, tenantId=1146029695717560320, journalId=1146120122248306696, language=CN, title=基于酒石酸盐体系的锑隔膜电解精炼技术及杂质脱除研究, columnId=1152626641328501305, journalTitle=湿法冶金, columnName=试验研究, runingTitle=null, highlight=null, articleAbstract=

以精锑为原料，研发了适用于酒石酸盐体系的锑隔膜电解精炼技术，系统考察了不同隔膜类型和电解工艺参数,包括电流密度、电解温度、电解液循环速度和极间距对阴极电流效率、槽电压、直流电耗、阴极锑纯度及典型杂质脱除率的影响规律。试验确定最佳工艺条件为：酒石酸根离子质量浓度250 g/L，锑离子浓度45 g/L，电流密度150 A/m²，电解温度35 ℃,电解液循环速度300 mL/min,极间距70 mm。研究结果表明:参照国标《高纯锑》（GB/T 10117—2021）中5N级别高纯锑的单点杂质含量要求，酒石酸锑电解体系易超标的杂质主要是砷、铋、铅和铜，仅调控电解工艺条件无法实现上述杂质的深度脱除，需配合进一步的电解液净化措施才能保证高纯锑产品的批次稳定性，而其余16种主控杂质通过电解精炼即能满足国标Sb-05要求;在最优电解条件下，配合锑基吸附剂（主相为H₁₄Sb₁₄O₂₁(OH)₄₂的多羟基锑酸）对电解液进行深度净化，可获得纯度为99.995%且表面致密光亮的阴极锑，平均槽电压为0.708 V，电流效率达96.27%，吨锑直流电耗为485.75 kWh/t。

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陶星睿（1999—），男，硕士研究生，主要研究方向为金属电解精炼。

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陶星睿（1999—），男，硕士研究生，主要研究方向为金属电解精炼。

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