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Based on the preparation of graphene oxide-ferroferric oxide composite (GO-Fe₃O₄) by chemical co-precipitation, hydrophobic modification of GO-Fe₃O₄ was carried out via physical adsorption using D2EHPA to obtain the D2EHPA@GO-Fe₃O₄ composite material (GOFP). Subsequently, a W/O-type GO-Fe₃O₄-based Pickering emulsion was successfully constructed using sulfonated kerosene as the oil phase, 1 mol/L hydrochloric acid as the internal aqueous phase, P507 (extractant) as the mobile carrier and GOFP as the solid emulsifier, which was used to extract heavy rare earth ion Ho³⁺. The effects of extraction time, mobile carrier dosage, emulsion-to-aqueous phase ratio, feed solution pH, and initial Ho³⁺ concentration on the extraction rate of Ho³⁺ were systematically investigated. The results indicate that under optimal conditions of extraction time of 3 min, feed solution pH ≥ 4.6, initial Ho³⁺ concentration of 0.002 mol/L, P507 (extractant) dosage of 0.5 mL, and emulsion-to-aqueous phase ratio of 0.3, the extraction rate of Ho³⁺ reaches 88%. The GO-Fe₃O₄-based Pickering emulsion liquid membrane method demonstrates promising application potential.

, authors=Xujiao JIANG, Yong LI, authorsList=Xujiao JIANG, Yong LI, authorCompany=null, correspAuthors=Yong LI, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1311350701561831565, articleId=1311350700915908747, tenantId=1146029695717560320, journalId=1146120122248306696, language=CN, title=用GO-Fe₃O₄系Pickering乳状液膜法萃取Ho³⁺试验研究, columnId=1152626641328501305, journalTitle=湿法冶金, columnName=试验研究, runingTitle=null, highlight=null, articleAbstract=

在以化学共沉淀法制备氧化石墨烯-四氧化三铁复合材料（GO-Fe₃O₄）基础上，采用物理吸附法，利用D2EHPA对GO-Fe₃O₄进行疏水改性，制备D2EHPA@GO-Fe₃O₄复合材料（GOFP），再以磺化煤油为油相、1 mol/L盐酸为内水相、P507（萃取剂）为流动载体、GOFP为固体乳化剂，成功构筑了W/O型GO-Fe₃O₄系Pickering乳状液，并用于萃取重稀土离子Ho³⁺。系统考察了萃取时间、流动载体添加量、乳水比、料液pH及Ho³⁺初始浓度对Ho³⁺萃取率的影响。结果表明：在萃取时间3min、料液pH≥4.6、Ho³⁺初始浓度0.002 mol/L、流动载体P507（萃取剂）添加量0.5 mL、乳水比为0.3最佳条件下，Ho³⁺萃取率达88%。GO-Fe₃O₄系Pickering乳状液膜法具有一定应用前景。

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蒋旭娇（2001—），女，硕士研究生，主要研究方向为稀土萃取分离。

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蒋旭娇（2001—），女，硕士研究生，主要研究方向为稀土萃取分离。

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