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In order to better monitor the filling morphology effect of goaf, a study on the characterization of grouting filling morphology effect with polarizability as the target was carried out based on resistivity parameters. Seven different kinds of cement were selected and prepared with five different contents of graphite powder. The variation of resistivity and polarizability of cement-based grouting filling materials was analyzed. The electrical characteristics and compressive strength of grouting filling materials under different cement types and ratios were studied, and the application test was carried out. The indoor test results indicate that with the increase of graphite powder conten, the compressive strength decreases, and the polarizability increases. When the ratio of cement to graphite is less than 10:1, the polarizability increases rapidly. In addition to sulphoaluminate cement, the content of graphite powder has little effect on the resistivity of cement-based grouting filling materials. Under the condition that the resistivity difference before and after grouting filling in goaf is not obvious, the visual characterization of filling morphology effect can be realized by polarizability (when the polarizability value of filling material is more than 3 times that of surrounding rock, the characterization effect is obvious). The research finding which is of great significance for broadening the field of grouting geophysical monitoring and improving the monitoring effect.
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为更好地监测采空区充填形态效果,在电阻率参数的基础上,以极化率为目标开展注浆充填形态效果表征研究。选取7种不同类型水泥并配备5种不同石墨粉掺量,分析水泥基注浆充填材料电阻率、极化率的变化规律,研究了不同水泥类型和配比下注浆充填材料的电学特征及抗压强度,并进行应用试验验证。室内测试结果表明:试件的抗压强度随石墨粉掺量的增加而降低;极化率随石墨粉掺量的增加而升高,当水泥与石墨的比例小于10:1后,极化率快速增长;除硫铝酸盐水泥外,石墨粉掺量对水泥基注浆充填材料电阻率的影响较小。在采空区注浆充填前后电阻率差异不明显的情况下,可以通过极化率实现充填形态效果的可视化表征(充填材料极化率值大于围岩3倍以上时,表征效果明显)。研究成果对于拓宽注浆物探监测领域、提升监测效果具有重要意义。
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, authorsList=宋洋, 王向鹏, 王堃鹏, 姚磊钧, 李论, 安新, 王珂)}, authors=[Author(id=1226462307740463971, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, orderNo=0, firstName=null, middleName=null, lastName=null, nameCn=null, orcid=null, stid=null, country=null, authorPic=null, dead=0, email=16337344@qq.com, emailSecond=null, emailThird=null, correspondingAuthor=0, authorType=1, ext={EN=AuthorExt(id=1226462307870487410, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, authorId=1226462307740463971, language=EN, stringName=Yang SONG, firstName=Yang, middleName=null, lastName=SONG, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
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1.China Anergy Group Third Engineering Bureau Co., Ltd., Chengdu, Sichuan 610036, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1226462308076008330, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, authorId=1226462307740463971, language=CN, stringName=宋洋, firstName=null, middleName=null, lastName=null, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
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1.中国安能集团第三工程局有限公司,四川 成都 610036, bio={"content":"
宋洋(1982一),男,吉林长春人,硕士,高级工程师,主要从事灾害应急处置研究。E-mail:16337344@qq.com
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宋洋(1982一),男,吉林长春人,硕士,高级工程师,主要从事灾害应急处置研究。E-mail:16337344@qq.com
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2.Key Laboratory of Earth Exploration and Information Techniques of Ministry of Education, Chengdu University of Technology, Chengdu, Sichuan 610059, China
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2.成都理工大学 地球勘探与信息技术教育部重点实验室,四川 成都 610059
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3.陕西千骏捷建筑工程有限公司,陕西 咸阳市 713699)])]), Author(id=1226462308659016647, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, orderNo=2, firstName=null, middleName=null, lastName=null, nameCn=null, orcid=null, stid=null, country=null, authorPic=null, dead=0, email=null, emailSecond=null, emailThird=null, correspondingAuthor=0, authorType=1, ext={EN=AuthorExt(id=1226462308801622997, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, authorId=1226462308659016647, language=EN, stringName=Kunpeng WANG, firstName=Kunpeng, middleName=null, lastName=WANG, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
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2.Key Laboratory of Earth Exploration and Information Techniques of Ministry of Education, Chengdu University of Technology, Chengdu, Sichuan 610059, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1226462308906480611, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, authorId=1226462308659016647, language=CN, stringName=王堃鹏, firstName=null, middleName=null, lastName=null, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
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2.成都理工大学 地球勘探与信息技术教育部重点实验室,四川 成都 610059, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null)}, companyList=[AuthorCompany(id=1226462307031626523, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, xref=2., ext=[AuthorCompanyExt(id=1226462307040015132, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, companyId=1226462307031626523, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=
2.Key Laboratory of Earth Exploration and Information Techniques of Ministry of Education, Chengdu University of Technology, Chengdu, Sichuan 610059, China), AuthorCompanyExt(id=1226462307048403741, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, companyId=1226462307031626523, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=
2.成都理工大学 地球勘探与信息技术教育部重点实验室,四川 成都 610059)])]), Author(id=1226462309015532526, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, orderNo=3, firstName=null, middleName=null, lastName=null, nameCn=null, orcid=null, stid=null, country=null, authorPic=null, dead=0, email=null, emailSecond=null, emailThird=null, correspondingAuthor=0, authorType=1, ext={EN=AuthorExt(id=1226462309124584443, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, authorId=1226462309015532526, language=EN, stringName=Leijun YAO, firstName=Leijun, middleName=null, lastName=YAO, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
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1.China Anergy Group Third Engineering Bureau Co., Ltd., Chengdu, Sichuan 610036, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1226462309216858120, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, authorId=1226462309015532526, language=CN, stringName=姚磊钧, firstName=null, middleName=null, lastName=null, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
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1.中国安能集团第三工程局有限公司,四川 成都 610036, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null)}, companyList=[AuthorCompany(id=1226462306901603080, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, xref=1., ext=[AuthorCompanyExt(id=1226462306909991689, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, companyId=1226462306901603080, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=
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4.CCTEG Xi'an Research Institute (Group) Co., Ltd., Xi'an, Shaanxi 710077, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1226462309569179699, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, authorId=1226462309334298649, language=CN, stringName=李论, firstName=null, middleName=null, lastName=null, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
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4.中煤科工西安研究院(集团)有限公司,陕西 西安 710077, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null)}, companyList=[AuthorCompany(id=1226462307283284797, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, xref=4., ext=[AuthorCompanyExt(id=1226462307287479102, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, companyId=1226462307283284797, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=
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1.China Anergy Group Third Engineering Bureau Co., Ltd., Chengdu, Sichuan 610036, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1226462310080884824, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, authorId=1226462309661454394, language=CN, stringName=安新, firstName=null, middleName=null, lastName=null, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
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1.中国安能集团第三工程局有限公司,四川 成都 610036, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null)}, companyList=[AuthorCompany(id=1226462306901603080, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, xref=1., ext=[AuthorCompanyExt(id=1226462306909991689, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, companyId=1226462306901603080, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=
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1.中国安能集团第三工程局有限公司,四川 成都 610036)])]), Author(id=1226462310185742434, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, orderNo=6, firstName=null, middleName=null, lastName=null, nameCn=null, orcid=null, stid=null, country=null, authorPic=null, dead=0, email=null, emailSecond=null, emailThird=null, correspondingAuthor=0, authorType=1, ext={EN=AuthorExt(id=1226462310298988656, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, authorId=1226462310185742434, language=EN, stringName=Ke WANG, firstName=Ke, middleName=null, lastName=WANG, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
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24:290-302., articleTitle=Force-electric characteristics of cement-based materials with silica fume and fly ash during uniaxial compression, refAbstract=null)], funds=[Fund(id=1226462313297916269, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, awardId=42004057, language=CN, fundingSource=国家自然科学基金项目(42004057), fundOrder=null, country=null), Fund(id=1226462313427939704, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, awardId=2023YFB3905004, language=CN, fundingSource=国家重点研发计划项目(2023YFB3905004), fundOrder=null, country=null)], companyList=[AuthorCompany(id=1226462306901603080, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, xref=1., ext=[AuthorCompanyExt(id=1226462306909991689, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, companyId=1226462306901603080, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=
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Polarizability of seven cement-based grouting materials with different ratios, figureFileSmall=iWCkHbQrYBfF4EwzlREALw==, figureFileBig=B4zbsw3QDe3ayyT9EoFopQ==, tableContent=null), ArticleFig(id=1226462311603417310, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, language=CN, label=图1, caption=
7种水泥基注浆材料不同配比下的极化率, figureFileSmall=iWCkHbQrYBfF4EwzlREALw==, figureFileBig=B4zbsw3QDe3ayyT9EoFopQ==, tableContent=null), ArticleFig(id=1226462311838298352, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, language=EN, label=Fig.2, caption=
Resistivity of seven cement-based grouting materials with different ratios, figureFileSmall=fJGWlzs452Q5QSiJ8vuAsA==, figureFileBig=o37gIZVxPxgmiMBzBaAVug==, tableContent=null), ArticleFig(id=1226462311938961658, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, language=CN, label=图2, caption=
7种水泥基注浆材料不同配比下的电阻率, figureFileSmall=fJGWlzs452Q5QSiJ8vuAsA==, figureFileBig=o37gIZVxPxgmiMBzBaAVug==, tableContent=null), ArticleFig(id=1226462312064790787, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, language=EN, label=Fig.3, caption=
Compressive strength of seven cement-based grouting materials with different ratios, figureFileSmall=WTaozNsiNMo6J20aePtSpw==, figureFileBig=TUHBiNoJYxiKG8Hw9aYMkg==, tableContent=null), ArticleFig(id=1226462312165454091, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, language=CN, label=图3, caption=
7种水泥基注浆材料不同配比下的抗压强度, figureFileSmall=WTaozNsiNMo6J20aePtSpw==, figureFileBig=TUHBiNoJYxiKG8Hw9aYMkg==, tableContent=null), ArticleFig(id=1226462312287088913, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, language=EN, label=Fig.4, caption=
Comparison of imaging results based on polarization before and after grouting filling, figureFileSmall=yvVueP5Ix+XQahgEd61llQ==, figureFileBig=LgcA7z7SZ59IYJHpjDBW/Q==, tableContent=null), ArticleFig(id=1226462312400335128, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, language=CN, label=图4, caption=
注浆充填前后基于极化率成像结果对比, figureFileSmall=yvVueP5Ix+XQahgEd61llQ==, figureFileBig=LgcA7z7SZ59IYJHpjDBW/Q==, tableContent=null), ArticleFig(id=1226462312526164258, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, language=EN, label=Fig.5, caption=
Comparison of imaging results based on apparent resistivity before and after grouting filling, figureFileSmall=aiTl9CF/rAUOvse/vuaoiA==, figureFileBig=COKMNK+7Gs7IjrsID/f1CA==, tableContent=null), ArticleFig(id=1226462312643604781, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, language=CN, label=图5, caption=
注浆充填前后基于视电阻率成像结果对比, figureFileSmall=aiTl9CF/rAUOvse/vuaoiA==, figureFileBig=COKMNK+7Gs7IjrsID/f1CA==, tableContent=null), ArticleFig(id=1226462312761045306, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, language=EN, label=Table 1, caption=
Physical properties indexes of 7 types of cement
, figureFileSmall=null, figureFileBig=null, tableContent=
| 水泥种类 | 主要成分(除硅酸盐之外) | 初凝时间/min | 终凝时间/min |
|---|
| 普通硅酸盐水泥 | 矿渣(4.0%)、石灰石(7%) | ≥45 | ≤600 |
| 铝酸盐水泥 | Al2O3(43.6%)、CaO(33.5%) | ≥60 | ≤600 |
| 硫铝酸盐水泥 | 硬石膏(16%)、石灰石(18%) | ≥60 | ≤600 |
| 复合硅酸盐水泥 | 火山灰(7.5%)、石灰石(17%) | ≥45 | ≤600 |
| 粉煤灰水泥 | 粉煤灰(38.0%)、柠檬酸渣(5.0%) | ≥60 | ≤600 |
| 火山灰水泥 | 火山灰(10.4%)、石灰石(27.2%) | ≥60 | ≤600 |
| 矿渣水泥 | MgO(3.27%)、SO3(2.32%) | ≥60 | ≤600 |
), ArticleFig(id=1226462312865902918, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, language=CN, label=表1, caption=
7种水泥的物性指标
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| 水泥种类 | 主要成分(除硅酸盐之外) | 初凝时间/min | 终凝时间/min |
|---|
| 普通硅酸盐水泥 | 矿渣(4.0%)、石灰石(7%) | ≥45 | ≤600 |
| 铝酸盐水泥 | Al2O3(43.6%)、CaO(33.5%) | ≥60 | ≤600 |
| 硫铝酸盐水泥 | 硬石膏(16%)、石灰石(18%) | ≥60 | ≤600 |
| 复合硅酸盐水泥 | 火山灰(7.5%)、石灰石(17%) | ≥45 | ≤600 |
| 粉煤灰水泥 | 粉煤灰(38.0%)、柠檬酸渣(5.0%) | ≥60 | ≤600 |
| 火山灰水泥 | 火山灰(10.4%)、石灰石(27.2%) | ≥60 | ≤600 |
| 矿渣水泥 | MgO(3.27%)、SO3(2.32%) | ≥60 | ≤600 |
), ArticleFig(id=1226462312983343438, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, language=EN, label=Table 2, caption=
Mixing ratio of different types of cement and graphite
, figureFileSmall=null, figureFileBig=null, tableContent=
| 水泥类型 | 配比(水泥:石墨:水) |
|---|
| 纯水泥 | 水泥:石墨为20∶1 | 水泥:石墨为10∶1 | 水泥:石墨为5∶1 | 水泥:石墨为3∶1 |
|---|
| 铝酸盐水泥(A) | 0.4∶/∶0.14 | 0.4∶0.02∶0.14 | 0.35∶0.035∶0.15 | 0.36∶0.072∶0.19 | 0.3∶0.1∶0.22 |
| 硫铝酸盐水泥(B) | 0.4∶/∶0.14 | 0.4∶0.02∶0.14 | 0.35∶0.035∶0.15 | 0.36∶0.072∶0.19 | 0.3∶0.1∶0.22 |
| 复合硅酸盐水泥(C) | 0.4∶/∶0.14 | 0.4∶0.02∶0.14 | 0.35∶0.035∶0.15 | 0.36∶0.072∶0.19 | 0.3∶0.1∶0.22 |
| 普通硅酸盐水泥(D) | 0.4∶/∶0.14 | 0.4∶0.02∶0.14 | 0.35∶0.035∶0.15 | 0.36∶0.072∶0.19 | 0.3∶0.1∶0.22 |
| 粉煤灰水泥(E) | 0.4∶/∶0.14 | 0.4∶0.02∶0.14 | 0.35∶0.035∶0.15 | 0.36∶0.072∶0.19 | 0.3∶0.1∶0.22 |
| 火山灰水泥(F) | 0.4∶/∶0.14 | 0.4∶0.02∶0.14 | 0.35∶0.035∶0.15 | 0.36∶0.072∶0.19 | 0.3∶0.1∶0.22 |
| 矿渣水泥(G) | 0.4∶/∶0.14 | 0.4∶0.02∶0.14 | 0.35∶0.035∶0.15 | 0.36∶0.072∶0.19 | 0.3∶0.1∶0.22 |
), ArticleFig(id=1226462313130144088, tenantId=1146029695717560320, journalId=1225396423026438145, articleId=1226462303479050689, language=CN, label=表2, caption=
不同种类水泥与石墨配比
, figureFileSmall=null, figureFileBig=null, tableContent=
| 水泥类型 | 配比(水泥:石墨:水) |
|---|
| 纯水泥 | 水泥:石墨为20∶1 | 水泥:石墨为10∶1 | 水泥:石墨为5∶1 | 水泥:石墨为3∶1 |
|---|
| 铝酸盐水泥(A) | 0.4∶/∶0.14 | 0.4∶0.02∶0.14 | 0.35∶0.035∶0.15 | 0.36∶0.072∶0.19 | 0.3∶0.1∶0.22 |
| 硫铝酸盐水泥(B) | 0.4∶/∶0.14 | 0.4∶0.02∶0.14 | 0.35∶0.035∶0.15 | 0.36∶0.072∶0.19 | 0.3∶0.1∶0.22 |
| 复合硅酸盐水泥(C) | 0.4∶/∶0.14 | 0.4∶0.02∶0.14 | 0.35∶0.035∶0.15 | 0.36∶0.072∶0.19 | 0.3∶0.1∶0.22 |
| 普通硅酸盐水泥(D) | 0.4∶/∶0.14 | 0.4∶0.02∶0.14 | 0.35∶0.035∶0.15 | 0.36∶0.072∶0.19 | 0.3∶0.1∶0.22 |
| 粉煤灰水泥(E) | 0.4∶/∶0.14 | 0.4∶0.02∶0.14 | 0.35∶0.035∶0.15 | 0.36∶0.072∶0.19 | 0.3∶0.1∶0.22 |
| 火山灰水泥(F) | 0.4∶/∶0.14 | 0.4∶0.02∶0.14 | 0.35∶0.035∶0.15 | 0.36∶0.072∶0.19 | 0.3∶0.1∶0.22 |
| 矿渣水泥(G) | 0.4∶/∶0.14 | 0.4∶0.02∶0.14 | 0.35∶0.035∶0.15 | 0.36∶0.072∶0.19 | 0.3∶0.1∶0.22 |
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