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粉煤灰酸浸提铝试验条件的优化
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赵苏, 刘大为, 赵悦, 吕剑, 田中心
科技导报 | 研究论文 2014,32(23): 39-44
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科技导报 | 研究论文 2014, 32(23): 39-44
粉煤灰酸浸提铝试验条件的优化
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赵苏, 刘大为, 赵悦, 吕剑, 田中心
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Research on Optimized Experimental Conditions of Acid Leaching to Extract Alumina from Fly Ash
ZHAO Su, LIU Dawei, ZHAO Yue, LÜ Jian, TIAN Zhongxin
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出版时间: 2014-08-18 doi: 10.3981/j.issn.1000-7857.2014.23.005
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为优化酸浸法从粉煤灰中提取氧化铝的试验条件,提高酸溶过程浸出率,降低氟化物掺量,采用正交试验,对影响浸出率的各种因素进行研究。通过优化试验条件,提高铝的浸出率,大大降低环境污染。当溶出温度达沸腾硫酸浓度为12 mol/L固液比为1:3溶出时间为120 min、KF 和粉煤灰的质量比为4:100 时,铝的浸出率可达91.2%。在没有降低浸出率的前提下,有毒氟化物的掺量约减少一半。
酸浸法  /  粉煤灰  /  氧化铝  /  正交试验
Acid leaching is used to extract alumina from fly ash with generally concentrated sulfuric acid as solvent and fluoride as co-solvent. This method has some problems such as low leaching rate, fluoride environmental pollution, etc. The factors influencing the leaching rate with orthogonal test method are studied in this paper. By optimizing the experimental conditions, not only is the leaching rate of aluminum improved but also the environmental pollution is reduced. The results show that when the temperature reaches the boiling temperature of the dissolution, the concentration of sulfuric acid is 12 mol/L, the solid-to-liquid ratio is 1:3, the elution time is 120 min, and m(KF):m(fly ash)=0.04, the leaching rate of aluminum can be up to 91.2%, and the toxic fluoride dosage is reduced by half in the same leaching rate.
acid leaching method  /  fly ash  /  alumina  /  orthogonal test
赵苏, 刘大为, 赵悦, 吕剑, 田中心. 粉煤灰酸浸提铝试验条件的优化. 科技导报, 2014 , 32 (23) : 39 -44 . DOI: 10.3981/j.issn.1000-7857.2014.23.005
ZHAO Su, LIU Dawei, ZHAO Yue, LÜ Jian, TIAN Zhongxin. Research on Optimized Experimental Conditions of Acid Leaching to Extract Alumina from Fly Ash[J]. Science & Technology Review, 2014 , 32 (23) : 39 -44 . DOI: 10.3981/j.issn.1000-7857.2014.23.005
2014年第32卷第23期
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doi: 10.3981/j.issn.1000-7857.2014.23.005
  • 接收时间:2014-01-22
  • 首发时间:2014-08-26
  • 出版时间:2014-08-18
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  • 收稿日期:2014-01-22
  • 修回日期:2014-06-27
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2种不同金属材料的力学参数

Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)

Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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