Article(id=1242131432559157403, tenantId=1146029695717560320, journalId=1146031591421210625, issueId=1242131407250731366, articleNumber=null, orderNo=9, doi=10.3981/j.issn.1000-7857.2014.009, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1375027200000, receivedDateStr=2013-07-29, revisedDate=1383148800000, revisedDateStr=2013-10-31, acceptedDate=null, acceptedDateStr=null, onlineDate=1390352092953, onlineDateStr=2014-01-22, pubDate=1389110400000, pubDateStr=2014-01-08, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1390352092953, onlineIssueDateStr=2014-01-22, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1774076811205, creator=sys-migrate, updateTime=1774076811205, updator=sys-migrate, issue=Issue{id=1242131407250731366, tenantId=1146029695717560320, journalId=1146031591421210625, year='2014', volume='32', issue='1', pageStart='1', pageEnd='96', issueExtLink='null', onlineDate='null', pubDate='null', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=3, issueType=-1, specialIssue=null, createTime=1774076805165, creator=sys-migrate, updateTime=1774076805165, updator=sys-migrate, preIssue=null, nextIssue=null, ext=null, issueFiles=null}, startPage=65, endPage=69, ext={EN=ArticleExt(id=1242131436115927222, articleId=1242131432559157403, tenantId=1146029695717560320, journalId=1146031591421210625, language=EN, title=Effects of Various Solvent Systems and the Ratios on Thin-Layer Chromatographic Enantio-separation of Propranolol Hydrochloride, columnId=1242116080374710456, journalTitle=Science & Technology Review, columnName=Articles, runingTitle=null, highlight=null, articleAbstract=This paper evaluates the hydroxypropyl-β-cyclodextrin or methyl-β-cyclodextrin-based chiral stationary phase, with oxidized multi-walled carbon nanotubes as additional adsorbing materials, for the chiral separation of propranolol hydrochloride enantiomers. The compositions of the developing solvent (acetonitrile/various alcohols), with/without acetic acid, are optimized. The optimal solvent system of acetonitrile/iso-butanol 9/1 (V/V) containing 2% acetic acid (in volume) for hydroxypropyl-β-cyclodextrin/ oxidized multi-walled carbon nanotubes impregnated thin-layer chromatography, and the optimal solvent system of acetonitrile/n-butanol 1/1 (V/V) containing 2% acetic acid (in volume) for methyl-β-cyclodextrin/oxidized multi-walled carbon nanotubes impregnated thinlayer chromatography are obtained., correspAuthors=null, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=C6qfTDVkEWcLv4eKguJ6Aw==, pdfFileSize=1333117, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, authorCompany=1. Research and Development Center, China Tobacco Hunan Industrial Corporation, Changsha 410014, China;
2. Key Laboratory of Resources Chemistry of Nonferrous Metals, College of Chemistry and Chemical Engineering, Central South University, Changsha 410083, China, fund=null, authors=YAO Yuanxiang¹, LIU Jinyun¹, TAN Xinliang¹, PENG Zhiguang^1,2, JIN Hangdan², authorsList=YAO Yuanxiang, LIU Jinyun, TAN Xinliang, PENG Zhiguang, JIN Hangdan), CN=ArticleExt(id=1242131435188986022, articleId=1242131432559157403, tenantId=1146029695717560320, journalId=1146031591421210625, language=CN, title=不同溶剂及配比对碳纳米管辅助薄层色谱拆分盐酸普萘洛尔的影响, columnId=1146540929516700224, journalTitle=科技导报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=以羟丙基-β-环糊精、甲基-β-环糊精为手性固定相，氧化多壁碳纳米管为拆分辅助吸附添加剂，采用薄层色谱法拆分了盐酸普萘洛尔对映体。优化得到了最佳展开剂条件，并对展开剂中是否添加冰醋酸进行了比较。当以羟丙基-β-环糊精/氧化多壁碳纳米管为固定相制备薄层色谱板，用于拆分盐酸普萘洛尔时，最佳的展开剂条件为：乙腈/异丁醇（体积比为9:1）混合溶剂中添加体积分数为2%的冰醋酸。当以甲基-β-环糊精/氧化多壁碳纳米管为固定相制备薄层色谱板，用于拆分盐酸普萘洛尔时，最佳的展开剂条件为：乙腈/正丁醇（体积比为1：1）混合溶剂中添加体积分数为2%的冰醋酸。, correspAuthors=null, authorNote=姚元香，工程师，研究方向为新材料制备及应用、分离分析新技术等，电子信箱：yuanxyao@sina.com, correspAuthorsNote=彭志光，讲师，研究方向 为纳米材料制备及应用，电子信箱：zhgpeng@csu.edu.cn, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=hqVXEt22fFBsFYQOQJPvsw==, pdfFileSize=1333117, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, authorCompany=1. 湖南中烟工业有限责任公司技术研发中心, 长沙 410014;
2. 中南大学化学化工学院, 有色资源化学教育部重点实验室, 长沙 410083, fund=国家自然科学基金项目（21201181）；有色金属资源化学教育部重点实验室开放基金项目（2012-KF-04）；湖南省科技计划项目 （2012RS4007）, authors=姚元香¹, 刘金云¹, 谭新良¹, 彭志光^1,2, 金杭丹², authorsList=姚元香, 刘金云, 谭新良, 彭志光, 金杭丹)}, authors=null, keywords=[Keyword(id=1242131434777944223, tenantId=1146029695717560320, journalId=1146031591421210625, articleId=1242131432559157403, language=CN, orderNo=1, keyword=多壁碳纳米管), Keyword(id=1242131434857636000, tenantId=1146029695717560320, journalId=1146031591421210625, articleId=1242131432559157403, language=CN, orderNo=1, keyword=β-环糊精衍生物), Keyword(id=1242131434937327777, tenantId=1146029695717560320, journalId=1146031591421210625, articleId=1242131432559157403, language=CN, orderNo=1, keyword=手性分离), Keyword(id=1242131435029602468, tenantId=1146029695717560320, journalId=1146031591421210625, articleId=1242131432559157403, language=CN, orderNo=1, keyword=薄层色谱), Keyword(id=1242131435742634158, tenantId=1146029695717560320, journalId=1146031591421210625, 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