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科技导报 |研究论文 2013 , 31 (19) : 62 -65
高能球磨法制备MgNb2O6粉体及其陶瓷性能
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付志粉1, 马建立1, 高娟1, 刘鹏2
作者信息
    1. 安徽理工大学理学院, 安徽 淮南 232001;2. 陕西师范大学物理学与信息技术学院, 西安 710062
Preparation of MgNb2O6 Powders by Using High-energy Ball-milling Method and Properties of MgNb2O6 Ceramics
  • FU Zhifen1, MA Jianli1, GAO Juan1, LIU Peng2
  • Affiliations
      1. School of science Anhui University of Science and Technology, Huainan 232001, Anhui Province, China;2. School of Physics and Information Technology, Shaanxi Normal University, Xi'an 710062, China
    出版时间: 2013-07-08 doi: 10.3981/j.issn.1000-7857.2013.19.010
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    采用高能球磨法在800℃保温2h预烧合成MgNb2O6粉体,研究了MgNb2O6陶瓷的相结构、显微结构和微波介电性能随烧结温度的变化关系。实验结果表明,高能球磨法有效促进MgNb2O6粉体的低温合成,降低MgNb2O6陶瓷的烧结温度。1220℃保温2h烧结MgNb2O6陶瓷,密度为4.80g/cm3,平均粒径为3.5μm,介电常数εr为19.7,品质因数(Q·f)为29444GHz的优良微波介电性能,MgNb2O6粉体有望成为新一代中温烧结高频微波介质基板材料。
    高能球磨法  /  MgNb2O6  /  微波介质陶瓷
    By using high-energy ball-milling method, MgNb2O6 powders were synthesized at 800℃ for 2h. Meanwhile, phase transition, sintering behavior, microstructures, and microwave dielectric properties of MgNb2O6 ceramics changing with sintering tempreature were investigated. It is found that the calcining temperature of MgNb2O6 powders and the sintering temperature of MgNb2O6 ceramic are able to be effectively reduced. The pottery of MgNb2O6 sintered at 1,220℃ for 2h possesses the average grain size of 3.5μm, ρ= 4.80g/cm3, and excellent microwave dielectric properties of r=19.7 and quality factor Q·f=29,444GHz. Therefore, MgNb2O6 pottery obtained by the high energy ball-milling method makes itself become an appropriate candidate for the new generation of middle-temperature sintered high frequency microwave dielectric material.
    high-energy ball-milling method  /  MgNb2O6  /  microwave dielectric pottery
    付志粉;马建立;高娟;刘鹏. 高能球磨法制备MgNb2O6粉体及其陶瓷性能. 科技导报, 2013 , 31 (19) : 62 -65 . DOI: 10.3981/j.issn.1000-7857.2013.19.010
    FU Zhifen;MA Jianli;GAO Juan;LIU Peng. Preparation of MgNb2O6 Powders by Using High-energy Ball-milling Method and Properties of MgNb2O6 Ceramics[J]. Science & Technology Review, 2013 , 31 (19) : 62 -65 . DOI: 10.3981/j.issn.1000-7857.2013.19.010

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    doi: 10.3981/j.issn.1000-7857.2013.19.010
    • 接收时间:2012-09-24
    • 首发时间:2013-07-08
    • 出版时间:2013-07-08
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    鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
    小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
    多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
    红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
    小菇属 Mycena 11 5.26
    光柄菇属 Pluteus 5 2.39
    红菇属 Russula 17 8.13
    栓菌属 Trametes 5 2.39
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