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The 0.55Pb(Ni1/3Nb2/3)O3-0.45Pb(Zr0.3Ti0.7)O3(0.55PNN-0.45PZT) piezoelectric ceramics by doping with Fe2O3 were prepared using the microwave sintering process at 1,200℃ for 2h. The effect of Fe2O3 doping on microstructure, dielectric and piezoelectric properties were investigated by using X-Ray Diffraction (XRD), Scanning Electron Microscope (SEM), impedance analyser, and ferroelectric tester in detail. The XRD results indicate that all samples possess typical pervoskite phase. In addition, both the piezoelectric and dielectric constants increases firstly and then decreases with increasing x. The optimum electrical properties of d33=520pC/N, kp=0.51, εr=4768, and tanδ=0.026 are obtained for the 0.55PNN-0.45PZT ceramics by doping with 0.8% Fe2O3., authors=DU Jianzhou, QIU Jinhao, ZHU Kongjun, JI Hongli, authorsList=DU Jianzhou;QIU Jinhao;ZHU Kongjun;JI Hongli, authorCompany=State Key Laboratory of Mechanics and Control of Mechanical Structures, Nanjing University of Aeronautics and Astronautics, Nanjing 210016, China, correspAuthors=null, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=eNkIsk7dmEFVe9tAOfOTlQ==, pdfFileSize=1679026, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1242129944730468780, articleId=1242129941286945182, tenantId=1146029695717560320, journalId=1146031591421210625, language=CN, title=微波烧结法制备Fe2O3掺杂0.55PNN-0.45PZT压电陶瓷及性能, columnId=1242116902361830275, journalTitle=科技导报, columnName=专题论文, runingTitle=null, highlight=null, articleAbstract=微波烧结是一种新型、高效的陶瓷烧结工艺,具有升温速度快、节能省时、改善微观结构以及降低烧结温度等特点.本文采用微波烧结工艺制备了Fe2O3掺杂的0.55Pb(Ni1/3Nb2/3)O3-0.45Pb(Zr0.3Ti0.7)O3(简写为0.55PNN-0.45PZT)压电陶瓷,烧结温度为1200℃、保温时间为2h.利用X射线衍射(X-ray Diffraction,XRD)、扫描电子显微镜(Scanning Electron Microscope, SEM)、阻抗分析仪及铁电分析仪等测试表征方法,研究了Fe2O3掺杂对陶瓷的结构、介电以及压电性能的影响.结果表明,所有陶瓷样品均为钙钛矿结构,随着Fe2O3掺杂量的增加,压电和介电性能呈先增加后减小趋势.当Fe2O3掺杂量为0.8%(质量分数)时,陶瓷达到最优电学性能:压电常数(d33)、平面机电耦合系数(kp)、相对介电常数(εr)和介电损耗(tanδ)分别为d33=520pC/N,kp=0.51,εr=4768,tanδ=0.026., authors=杜建周, 裘进浩, 朱孔军, 季宏丽, authorsList=杜建周;裘进浩;朱孔军;季宏丽, authorCompany=南京航空航天大学机械结构力学及控制国家重点实验室,南京 210016, correspAuthors=null, authorNote=null, correspAuthorsNote=裘进浩,教授,研究方向为智能材料与结构,电子信箱:qiu@nuaa.edu.cn, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, 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微波烧结法制备Fe2O3掺杂0.55PNN-0.45PZT压电陶瓷及性能
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微波烧结法制备Fe2O3掺杂0.55PNN-0.45PZT压电陶瓷及性能
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杜建周, 裘进浩, 朱孔军, 季宏丽
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    南京航空航天大学机械结构力学及控制国家重点实验室,南京 210016

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裘进浩,教授,研究方向为智能材料与结构,电子信箱:qiu@nuaa.edu.cn
Preparation of 0.55PNN-0.45PZT Piezoelectric Ceramics by and Doped with Fe2O3 Using Microwave Sintering and Its Properties
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出版时间: 2013-02-28 doi: 10.3981/j.issn.1000-7857.2013.h1.004
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微波烧结是一种新型、高效的陶瓷烧结工艺,具有升温速度快、节能省时、改善微观结构以及降低烧结温度等特点.本文采用微波烧结工艺制备了Fe2O3掺杂的0.55Pb(Ni1/3Nb2/3)O3-0.45Pb(Zr0.3Ti0.7)O3(简写为0.55PNN-0.45PZT)压电陶瓷,烧结温度为1200℃、保温时间为2h.利用X射线衍射(X-ray Diffraction,XRD)、扫描电子显微镜(Scanning Electron Microscope, SEM)、阻抗分析仪及铁电分析仪等测试表征方法,研究了Fe2O3掺杂对陶瓷的结构、介电以及压电性能的影响.结果表明,所有陶瓷样品均为钙钛矿结构,随着Fe2O3掺杂量的增加,压电和介电性能呈先增加后减小趋势.当Fe2O3掺杂量为0.8%(质量分数)时,陶瓷达到最优电学性能:压电常数(d33)、平面机电耦合系数(kp)、相对介电常数(εr)和介电损耗(tanδ)分别为d33=520pC/N,kp=0.51,εr=4768,tanδ=0.026.
微波烧结  /  三氧化二铁掺杂  /  铌镍酸铅-锆钛酸铅陶瓷  /  压电性能
Microwave sintering is a novel and high efficiency sintering technology for ceramics, which exhibits many significant advantages, such as high rapid heating rate, energy saving and shorter sintering time, microstructures improvement, and lower sintering temperature. The 0.55Pb(Ni1/3Nb2/3)O3-0.45Pb(Zr0.3Ti0.7)O3(0.55PNN-0.45PZT) piezoelectric ceramics by doping with Fe2O3 were prepared using the microwave sintering process at 1,200℃ for 2h. The effect of Fe2O3 doping on microstructure, dielectric and piezoelectric properties were investigated by using X-Ray Diffraction (XRD), Scanning Electron Microscope (SEM), impedance analyser, and ferroelectric tester in detail. The XRD results indicate that all samples possess typical pervoskite phase. In addition, both the piezoelectric and dielectric constants increases firstly and then decreases with increasing x. The optimum electrical properties of d33=520pC/N, kp=0.51, εr=4768, and tanδ=0.026 are obtained for the 0.55PNN-0.45PZT ceramics by doping with 0.8% Fe2O3.
microwave sintering  /  Fe2O3 doping  /  PNN-PZT ceramics  /  piezoelectric property
杜建周;裘进浩;朱孔军;季宏丽. 微波烧结法制备Fe2O3掺杂0.55PNN-0.45PZT压电陶瓷及性能. 科技导报, 2013 , 31 (5-6) : 29 -32 . DOI: 10.3981/j.issn.1000-7857.2013.h1.004
DU Jianzhou;QIU Jinhao;ZHU Kongjun;JI Hongli. Preparation of 0.55PNN-0.45PZT Piezoelectric Ceramics by and Doped with Fe2O3 Using Microwave Sintering and Its Properties[J]. Science & Technology Review, 2013 , 31 (5-6) : 29 -32 . DOI: 10.3981/j.issn.1000-7857.2013.h1.004
2013年第31卷第5-6期
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doi: 10.3981/j.issn.1000-7857.2013.h1.004
  • 接收时间:2012-12-20
  • 首发时间:2013-02-28
  • 出版时间:2013-02-28
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  • 收稿日期:2012-12-20
  • 修回日期:2013-01-16
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裘进浩,教授,研究方向为智能材料与结构,电子信箱:qiu@nuaa.edu.cn
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2种不同金属材料的力学参数

Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)

Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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