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The Plackett-Burman design was adopted to select the most important nutrients and Box-Benhnken Design was used to identify the optimum concentrations of the key nutrients. The optimum conditions were determined: the chitosan concentration of 1.5g/L, the emulsification of 45min, the rotational speed of 600r/min, the reaction time of 60min, the poly (malic acid) concentration of 1.0g/L, the ratio of poly (malic acid) to chitosan of 1:2, the pH value of 6.0, the dropping speed of 7.5mL/h, and the core material amount of 1mL. 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β-聚苹果酸/壳聚糖在香精微胶囊制备中的应用
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科技导报 | 研究论文 2013,31(4): 54-59
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科技导报 | 研究论文 2013, 31(4): 54-59
β-聚苹果酸/壳聚糖在香精微胶囊制备中的应用
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马霞, 吴艳丽, 俞鸿千
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    上海应用技术学院香精香料与工程技术学院,上海 201418
Application of β-Poly-Malic Acid/Chitosan in the Preparation of Essence Microcapsule
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出版时间: 2013-02-08 doi: 10.3981/j.issn.1000-7857.2013.04.008
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通过复凝聚法将β-聚苹果酸(PMA)与壳聚糖(CS)作为壁材,制得粒径为200~600nm,分散系数<0.30的具有长久缓释效果的香精微胶囊.通过Plackett-Burman(PB)实验和Box-Benhnken Design(BBD)优化确定了制备缓释型香精微胶囊的最佳工艺条件,得出制备香精微胶囊的最优条件为:壳聚糖浓度1.5g/L,乳化时间45min、转速600r/min、反应时间60min,聚苹果酸浓度为1.0g/L,聚苹果酸(mL)﹕壳聚糖(mL)=1:2,pH值为6.0,滴加速度为7.5mL/h,芯材添加量为1mL/15mL壁材.借助扫描电镜观察与壁材形成的微球形微胶囊,粒径为480.1nm,包埋率为28.57%,缓释效果持续长久.
β-聚苹果酸  /  微胶囊  /  Plackett-Burman实验  /  Box-Benhnken Design  /  缓释
The paper studies the preparation of the fragrance microcapsule, of diameter in the range of 200-600nm and with the coefficient of dispersion less than 0.30, enjoying a long sustained-release effects, based on β-poly-malic acid (PMA) and chitosan (CS) as the wall materials. The Plackett-Burman design was adopted to select the most important nutrients and Box-Benhnken Design was used to identify the optimum concentrations of the key nutrients. The optimum conditions were determined: the chitosan concentration of 1.5g/L, the emulsification of 45min, the rotational speed of 600r/min, the reaction time of 60min, the poly (malic acid) concentration of 1.0g/L, the ratio of poly (malic acid) to chitosan of 1:2, the pH value of 6.0, the dropping speed of 7.5mL/h, and the core material amount of 1mL. In the SEM observation of the micro-spherical microcapsules, the particle size is 481.0nm, and the embedding ratio is 28.57% with a continuous long-term releasing effect.
β-poly-malic acid  /  microcapsule  /  Plackett-Burman experiment  /  Box-Benhnken Design  /  release
马霞;吴艳丽;俞鸿千. β-聚苹果酸/壳聚糖在香精微胶囊制备中的应用. 科技导报, 2013 , 31 (4) : 54 -59 . DOI: 10.3981/j.issn.1000-7857.2013.04.008
MA Xia;WU Yanli;YU Hongqian. Application of β-Poly-Malic Acid/Chitosan in the Preparation of Essence Microcapsule[J]. Science & Technology Review, 2013 , 31 (4) : 54 -59 . DOI: 10.3981/j.issn.1000-7857.2013.04.008
2013年第31卷第4期
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doi: 10.3981/j.issn.1000-7857.2013.04.008
  • 接收时间:2012-10-09
  • 首发时间:2013-02-08
  • 出版时间:2013-02-08
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  • 收稿日期:2012-10-09
  • 修回日期:2012-11-29
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2种不同金属材料的力学参数

Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)

Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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