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Rude fatty acids from the seeds of barley were extracted by Soxhler extractor and the acid-hydrolysis method. After being methyl-esterified with the presence of KOH/MeOH, the components of fatty acids were analyzed by GC/MS. The results show that the extracting amounts of rude fatty acids using these two methods are 1.87g/100g and 1.98g/100g, respectively. 12 and 14 kinds of fatty acids were obtained from the two methods. The main components are linoleic acid (52.20%, 53.27%), palmitic acid (22.75%, 22.15%), oleic acid (16.35%, 14.63%), and linolenic acid (4.65%, 5.48%). Most of the fatty acids are polyunsaturated fatty ones, which constitute more than 75% of the total mass. 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科技导报
| 研究论文 2010, 28(15): 75-78
大麦籽粒油脂肪酸成分分析
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郑敏燕1,魏永生1,宁建刚2,耿 薇1,张君才1
作者信息
1. 咸阳师范学院化学与化工学院,陕西咸阳 7120002. 青海师范大学民族师范学院化学系,西宁 810008
通讯作者:
郑敏燕
Analysis of Fatty Components from the Seed of Barley
Affiliations
出版时间: 2010-07-13
文章导航
测定、分析大麦籽粒油脂的质量分数及其脂肪酸组成。分别采用索氏抽提法和酸水解法提取大麦籽粒中的粗脂肪油,再经过氢氧化钾/甲醇碱催化甲酯化法进行衍生化处理后,通过气相色谱/质谱联用技术分析脂肪酸的组成。结果显示,两种方法大麦籽粒粗脂肪的提取量分别为1.87g/100g和1.98g/100g,分别鉴定出12种和14种脂肪酸成分,主要成分为亚油酸(52.20%,53.27%)、棕榈酸(22.75%,22.15%)、油酸(16.35%,14.63%)和亚麻酸(4.65%,5.48%),油脂中不饱和脂肪酸的质量分数都超过75%。研究结果可为大麦类食品的相关研究提供基础数据。
大麦
/
脂肪酸
/
气相色谱/质谱法
/
甲酯化
The amount of fatty and the compositions of fatty acids in the seeds of barley were determined and analyzed. Rude fatty acids from the seeds of barley were extracted by Soxhler extractor and the acid-hydrolysis method. After being methyl-esterified with the presence of KOH/MeOH, the components of fatty acids were analyzed by GC/MS. The results show that the extracting amounts of rude fatty acids using these two methods are 1.87g/100g and 1.98g/100g, respectively. 12 and 14 kinds of fatty acids were obtained from the two methods. The main components are linoleic acid (52.20%, 53.27%), palmitic acid (22.75%, 22.15%), oleic acid (16.35%, 14.63%), and linolenic acid (4.65%, 5.48%). Most of the fatty acids are polyunsaturated fatty ones, which constitute more than 75% of the total mass. The results could offer some basic data to the food research related with barley.
barley
/
fatty acids
/
GC/MS
/
methyl-esterifying
郑敏燕;魏永生;宁建刚;耿 薇;张君才.
大麦籽粒油脂肪酸成分分析.
科技导报,
2010
, 28
(15)
: 75
-78
.
.
Analysis of Fatty Components from the Seed of Barley[J].
Science & Technology Review ,
2010
, 28
(15)
: 75
-78
.
2010年第28卷第15期
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接收时间:2009-12-01
首发时间:2010-07-13
出版时间:2010-07-13
收稿日期:2009-12-01
修回日期:2010-01-17
https://castjournals.cast.org.cn/joweb/kjdb/CN/1242120419755491849
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2种不同金属材料的力学参数
科 Family 属数 Number of genus 种数 Number of species 占总种数比例 Percentage of total species (%) 属 Genus 种数 Number of species 占总种数比例 Percentage of total species (%) 鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78 小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39 多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39 红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87 小菇属 Mycena 11 5.26 光柄菇属 Pluteus 5 2.39 红菇属 Russula 17 8.13 栓菌属 Trametes 5 2.39
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