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科技导报 |研究论文 2010 , 28 (13) : 92 -96
微波辅助提取废次烟叶水溶性糖工艺
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杜林洳1,徐翠莲2,樊素芳2,万郑凯2,王喜云2
作者信息
    1. 河南农业大学烟草学院,郑州 4500022. 河南农业大学理学院,郑州 450002
通讯作者:
徐翠莲
Extraction of Water-soluble Saccharides from Abandoned Tobaccos with Microwave-assisted Technique
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      Corresponding Author:
      Xu Cui lian
    出版时间: 2010-07-13
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    为了有效地提取废次烟叶中水溶性糖,进一步对水溶性糖生物活性进行基础和应用开发研究,为废次烟叶水溶性糖的开发利用提供依据,采用连续微波辐射方法进行微波萃取工艺的优化,在单因素试验的基础上,通过正交试验和极差分析考查了提取温度、微波功率、提取时间和料水比对水溶性糖提取率的影响。通过极差分析显示影响因素从大到小依次为:料液比>功率>时间>温度,正交实验的最佳提取条件是:料液比1:30、提取功率400W、提取时间20min、提取温度60℃,提取率为28.54%。与经典法和直接水提法相比,微波辅助提取法可将水溶性糖的提取率分别提高6.39%和6.92%,并具有高效、节能、产率稳定、省时等特点。
    废次烟叶  /  水溶性糖  /  微波提取  /  正交试验  /  参数优化
    In order to extract water-soluble saccharides from discarded tobaccos effectively, and to study their biological activity, the microwave technology is used in extraction of water-soluble polysaccharides from discarded tobaccos and the optimal process of extraction was obtained by the method of continuous microwave radiation. On the basis of one-factor tests, the effects of extraction temperature, microwave power, extraction time and liquid-to-solid ratio on the microwave extraction of water-soluble saccharides were analyzed by the orthogonal experiment and the range analysis. The results of range analysis show that the factors affecting extraction rate are in the following order in their importance: ratio of solid to liquid>microwave power>extraction time>temperature. The optimized conditions are:
    1:30 of the ratio of solid to liquid, 400W of the microwave power, 20 min of the extraction time and 60℃ of the temperature. The extraction rate of 28.54% can be obtained under the above conditions, an increase of 6.39% and 6.92%, respectively, as compared with the classical method and the direct water extraction This method enjoys advantages such as high efficiency, energy-saving, yield stability and time-saving.
    discarded tobaccos  /  water-soluble saccharides  /  microwave extraction  /  orthogonal test  /  optimization
    杜林洳;徐翠莲;樊素芳;万郑凯;王喜云. 微波辅助提取废次烟叶水溶性糖工艺. 科技导报, 2010 , 28 (13) : 92 -96 .
    . Extraction of Water-soluble Saccharides from Abandoned Tobaccos with Microwave-assisted Technique[J]. Science & Technology Review, 2010 , 28 (13) : 92 -96 .

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    • 首发时间:2010-07-13
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    2种不同金属材料的力学参数

    Family
    属数
    Number of
    genus
    种数
    Number of
    species
    占总种数比例
    Percentage of
    total species (%)

    Genus
    种数
    Number of
    species
    占总种数比例
    Percentage of total
    species (%)
    鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
    小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
    多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
    红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
    小菇属 Mycena 11 5.26
    光柄菇属 Pluteus 5 2.39
    红菇属 Russula 17 8.13
    栓菌属 Trametes 5 2.39
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