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天麻超微饮片的HPLC指纹图谱研究
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蔡光先1,2,李顺祥1,2
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    1. 湖南中医学院 长沙2. 湖南省中医药研究院 长沙
通讯作者:
蔡光先
Studies on HPLC Fingerprint of Ultramicro Rhizoma Gastrodiae
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    出版时间: 2006-02-10
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    研究天麻超微饮片的HPLC指纹图谱,考察其有效成分及含量,为天麻超微饮片的质控提供可靠方法。色谱柱为大连依利特公司HypersilBDSC18(4.6mm×200mm,5μm)柱。流动相为0.05%磷酸水溶液洗脱,柱温为25℃,流速为1.0ml·min-1,检测波长为220nm。建立了天麻超微饮片的HPLC指纹图谱,标定了7个共有峰。结论为利用HPLC指纹图谱可以较全面的控制天麻超微饮片的内在质量。
    中药学  /  天麻超微饮片  /  指纹图谱  /  高效液相色谱法
    To determine the HPLC fingerprint of the ultramicro rhizoma Gastrodiae and to test its potent constituents and content. Chromatographic column: Hypersil BDS C18(4.6 mm×200 mm,5μm). Mobile phase: 0.05% phosphoric acid in water. Column temperature: 25℃. Flow rate: 1.0 ml·min-1. Wavelength: 220nm. The fingerprint of ultramicro rhizoma Gastrodiae was established and 7common peaks are in the fingerprint. Conclusion is that methods and data can be used to control the quality of the ultramicro rhizoma Gastrodiae.
    蔡光先;李顺祥;. 天麻超微饮片的HPLC指纹图谱研究. 科技导报, 2006 , 24 (0602) : 33 -35 .
    . Studies on HPLC Fingerprint of Ultramicro Rhizoma Gastrodiae[J]. Science & Technology Review, 2006 , 24 (0602) : 33 -35 .

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    • 接收时间:2009-03-20
    • 首发时间:2006-02-10
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    鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
    小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
    多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
    红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
    小菇属 Mycena 11 5.26
    光柄菇属 Pluteus 5 2.39
    红菇属 Russula 17 8.13
    栓菌属 Trametes 5 2.39
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