Article(id=1242133627379720562, tenantId=1146029695717560320, journalId=1146031591421210625, issueId=1242133617015595332, articleNumber=null, orderNo=8, doi=10.3981/j.issn.1000-7857.2015.13.006, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1422288000000, receivedDateStr=2015-01-27, revisedDate=1431273600000, revisedDateStr=2015-05-11, acceptedDate=null, acceptedDateStr=null, onlineDate=1437799357183, onlineDateStr=2015-07-25, pubDate=1436716800000, pubDateStr=2015-07-13, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1437799357183, onlineIssueDateStr=2015-07-25, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1774077334491, creator=sys-migrate, updateTime=1774077334491, updator=sys-migrate, issue=Issue{id=1242133617015595332, tenantId=1146029695717560320, journalId=1146031591421210625, year='2015', volume='33', issue='13', pageStart='1', pageEnd='112', issueExtLink='null', onlineDate='null', pubDate='1436716800000', pubDateStr='2015-07-13', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=3, issueType=-1, specialIssue=null, createTime=1774077332020, creator='sys-migrate', updateTime=1774077332020, updator='sys-migrate', preIssue=null, nextIssue=null, articleTotal=null, ext=null, issueFiles=null, downloadFileDto=null}, startPage=39, endPage=45, ext={EN=ArticleExt(id=1242133629963415987, articleId=1242133627379720562, tenantId=1146029695717560320, journalId=1146031591421210625, language=EN, title=Study on demulsification and dehydration of emulsion of returned acidizing fluids and crude oil, columnId=1242116080374710456, journalTitle=Science & Technology Review, columnName=Articles, runingTitle=null, highlight=null, articleAbstract=The emulsion that is mixed with returned acidizing fluids and crude oil has strong stability, which may have a great influence on the crude oil dehydration and the safe operation of crude setting tank. The effects of temperature, demulsifier dosage, pH value, viscosity reducer dosage on the viscosity of emulsion and demulsification performance are studied, and the microscopic changes of emulsion at different times are observed. It is indicated by experiments that the viscosity of emulsion mixed with returned acidizing fluids and crude oil declines significantly firstly and then decreases gradually with the increasing temperature; when the temperature is lower than 40℃, the emulsion has stronger stability, however, between the temperature of 50-60℃, the dehydration rate does not increase significantly with the increasing temperature. So it is concluded that the best demulsification temperature is 50℃. It is also found that emulsion viscosity could be decreased by adding demulsifier, but not significantly; the more the dosage of demulsifier is, the better the demulsification performance is, and the dehydration rate is not remarkably increased when the demulsifier dosage is more than 150 mg/L. So it is concluded that the best demulsifier dosage is 150 mg/L. Moreover, it is beneficial for demulsification performance to adjust the returned acidizing fluids pH value to 6.0-7.0. With the increasing pH value, the oil water interface grows suddenly angular and the structure of crude oil after dewatering is more tight. Finally, the dehydrating speed is improved obviously by using viscosity reducer. These conclusions can be used as references to the demulsification and dehydration of emulsion that is flowed back early after the implementation of acidification., authors=WAN Liping1, KONG Bin1, ZHU Li1, MENG Yingfeng1, ZHOU Bonian1, ZHAI Lituan2, authorsList=WAN Liping, KONG Bin, ZHU Li, MENG Yingfeng, ZHOU Bonian, ZHAI Lituan, authorCompany=1. State Key Laboratory of Oil and Gas Reservoir Geology and Exploitation, Southwest Petroleum University, Chengdu 610500, China;
2. Tarim Oilfield Company, PetroChina, Kuerle 841000, China, correspAuthors=null, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=V0kQ4VXfh6sg1R0YKfKOoA==, pdfFileSize=2297003, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1242133628885475713, articleId=1242133627379720562, tenantId=1146029695717560320, journalId=1146031591421210625, language=CN, title=酸化返排液/原油乳状液的破乳脱水研究, columnId=1146540929516700224, journalTitle=科技导报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=酸化返排液与原油混合可形成稳定性强的乳状液,影响原油的脱水及原油沉降罐的安全运行.通过室内实验考察温度、破乳剂加量、pH 值及降黏剂加量对乳状液黏度和破乳效果的影响,并采用显微镜观察不同阶段乳状液微观形态变化.实验表明:酸化返排液与原油混合成的乳状液其黏度随温度升高先急剧下降,后平缓下降,在温度低于40℃时乳状液稳定性较强,温度50~60℃时,随着温度升高,乳状液脱水率上升幅度不大,综合选取破乳温度为50℃;添加破乳剂有利于降低乳状液黏度,但效果不明显,破乳剂加量越大,乳状液破乳效果越好,当破乳剂加量达到150 mg/L 后,随破乳剂用量加大,乳状液脱水率上升幅度不大,综合选取破乳剂加量为150 mg/L;调节酸化返排液pH 值至6.0~7.0 有利于乳状液破乳,pH 值越高,油水界面变得棱角分明,脱出水的原油结构更加紧密;加入降黏剂后,乳状液脱水速度明显加快.研究结论对指导油田酸化改造后,井口初期返出的乳状液实施破乳具有借鉴作用., authors=万里平1, 孔斌1, 朱利1, 孟英峰1, 周柏年1, 翟立团2, authorsList=万里平, 孔斌, 朱利, 孟英峰, 周柏年, 翟立团, authorCompany=1. 西南石油大学油气藏地质及开发工程国家重点实验室, 成都610500;
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酸化返排液/原油乳状液的破乳脱水研究
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科技导报 | 研究论文 2015, 33(13): 39-45
酸化返排液/原油乳状液的破乳脱水研究
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万里平1, 孔斌1, 朱利1, 孟英峰1, 周柏年1, 翟立团2
作者信息
    1. 西南石油大学油气藏地质及开发工程国家重点实验室, 成都610500;
    2. 中国石油塔里木油田分公司, 库尔勒841000
Study on demulsification and dehydration of emulsion of returned acidizing fluids and crude oil
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出版时间: 2015-07-13 doi: 10.3981/j.issn.1000-7857.2015.13.006
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酸化返排液与原油混合可形成稳定性强的乳状液,影响原油的脱水及原油沉降罐的安全运行.通过室内实验考察温度、破乳剂加量、pH 值及降黏剂加量对乳状液黏度和破乳效果的影响,并采用显微镜观察不同阶段乳状液微观形态变化.实验表明:酸化返排液与原油混合成的乳状液其黏度随温度升高先急剧下降,后平缓下降,在温度低于40℃时乳状液稳定性较强,温度50~60℃时,随着温度升高,乳状液脱水率上升幅度不大,综合选取破乳温度为50℃;添加破乳剂有利于降低乳状液黏度,但效果不明显,破乳剂加量越大,乳状液破乳效果越好,当破乳剂加量达到150 mg/L 后,随破乳剂用量加大,乳状液脱水率上升幅度不大,综合选取破乳剂加量为150 mg/L;调节酸化返排液pH 值至6.0~7.0 有利于乳状液破乳,pH 值越高,油水界面变得棱角分明,脱出水的原油结构更加紧密;加入降黏剂后,乳状液脱水速度明显加快.研究结论对指导油田酸化改造后,井口初期返出的乳状液实施破乳具有借鉴作用.
酸化返排液  /  乳状液  /  破乳  /  脱水率
The emulsion that is mixed with returned acidizing fluids and crude oil has strong stability, which may have a great influence on the crude oil dehydration and the safe operation of crude setting tank. The effects of temperature, demulsifier dosage, pH value, viscosity reducer dosage on the viscosity of emulsion and demulsification performance are studied, and the microscopic changes of emulsion at different times are observed. It is indicated by experiments that the viscosity of emulsion mixed with returned acidizing fluids and crude oil declines significantly firstly and then decreases gradually with the increasing temperature; when the temperature is lower than 40℃, the emulsion has stronger stability, however, between the temperature of 50-60℃, the dehydration rate does not increase significantly with the increasing temperature. So it is concluded that the best demulsification temperature is 50℃. It is also found that emulsion viscosity could be decreased by adding demulsifier, but not significantly; the more the dosage of demulsifier is, the better the demulsification performance is, and the dehydration rate is not remarkably increased when the demulsifier dosage is more than 150 mg/L. So it is concluded that the best demulsifier dosage is 150 mg/L. Moreover, it is beneficial for demulsification performance to adjust the returned acidizing fluids pH value to 6.0-7.0. With the increasing pH value, the oil water interface grows suddenly angular and the structure of crude oil after dewatering is more tight. Finally, the dehydrating speed is improved obviously by using viscosity reducer. These conclusions can be used as references to the demulsification and dehydration of emulsion that is flowed back early after the implementation of acidification.
returned acidizing fluids  /  emulsion  /  demulsification  /  dehydration rate
万里平, 孔斌, 朱利, 孟英峰, 周柏年, 翟立团. 酸化返排液/原油乳状液的破乳脱水研究. 科技导报, 2015 , 33 (13) : 39 -45 . DOI: 10.3981/j.issn.1000-7857.2015.13.006
WAN Liping, KONG Bin, ZHU Li, MENG Yingfeng, ZHOU Bonian, ZHAI Lituan. Study on demulsification and dehydration of emulsion of returned acidizing fluids and crude oil[J]. Science & Technology Review, 2015 , 33 (13) : 39 -45 . DOI: 10.3981/j.issn.1000-7857.2015.13.006
2015年第33卷第13期
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doi: 10.3981/j.issn.1000-7857.2015.13.006
  • 接收时间:2015-01-27
  • 首发时间:2015-07-25
  • 出版时间:2015-07-13
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  • 收稿日期:2015-01-27
  • 修回日期:2015-05-11
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2种不同金属材料的力学参数

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Number of
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Percentage of total
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鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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