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Acidification reagents are consisted of the volume fraction of 15% sulfuric acid, hydrochloric acid and oxalic acid saturated solution. Add acidification reagents to the wheel grinding machine for rolling. After a certain period of time, add Ca(OH)2 and adjust the material to 5 or 6 pH values, meanwhile add reductant sodium dithionite (Na2 S2 O4 ). After 5 minutes, stop working and discharging, drying the material at 110℃, preparing of high efficient active floridin after crushing. The research results indicate that the main factors influencing the activity and decolorization ratio of floridin include mixed acid concentration, solid-to-acid ratio, rolling time, moisture content and reducing agent dosage. 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科技导报
|研究论文
2012
, 30
(13) :
57
-61
轮碾法制备高效活性白土试验
全屏
舒明勇1,2 , 刘光辉2
作者信息
1. 攀枝花学院生物与化学工程学院,四川攀枝花 617000;2. 攀枝花学院攀枝花市冶金辅助矿产资源综合利用重点实验室,四川攀枝花 617000
Experiments on the Preparation of High-efficient Active Floridin by Wheel Rolling
SHU Mingyong1,2 , LIU Guanghui2
Affiliations
1. School of Biological and Chemical Engineering, Panzhihua University, Panzhihua 617000, Sichuan Province, China;2. Comprehensive Utilization Key Laboratory of Metallurgical Assistance of Mineral Resources of Panzhihua City, Panzhihua University, Panzhihua 617000, Sichuan Province, China
出版时间: 2012-05-08
doi: 10.3981/j.issn.1000-7857.2012.13.009
文章导航
以钙基膨润土为原料,采用体积分数为15%的硫酸、盐酸与草酸饱和溶液组成的混酸为酸化试剂,通过轮碾法制备高效活性白土。结果表明,混酸浓度、固酸比、碾压时间、含水率和还原剂用量是影响活性白土活性度、脱色率和相对白度的主要因素。当混酸体积分数为15%、固酸比为4:1、含水率为22%、碾压时间为40min、还原剂用量为膨润土物料质量的0.8%时,可制备出活性度为204,脱色率为96%,相对白度为82的高性能活性白土。
活性白土
/
轮碾法
/
活化效果
/
活性度
/
脱色率
Taking Ca-bentonite of Zhanyi County, Qujing City, Yunnan Province as the raw material, after drying, the moisture content is less than 5%, and broken into particles of 3—5mm. Acidification reagents are consisted of the volume fraction of 15% sulfuric acid, hydrochloric acid and oxalic acid saturated solution. Add acidification reagents to the wheel grinding machine for rolling. After a certain period of time, add Ca(OH)2 and adjust the material to 5 or 6 pH values, meanwhile add reductant sodium dithionite (Na2 S2 O4 ). After 5 minutes, stop working and discharging, drying the material at 110℃, preparing of high efficient active floridin after crushing. The research results indicate that the main factors influencing the activity and decolorization ratio of floridin include mixed acid concentration, solid-to-acid ratio, rolling time, moisture content and reducing agent dosage. When the mixed acid volume fraction is 15%, solid-to-acid ratio is 4:1, moisture content is 22%, rolling time is 40min and reducing agent dosage is 0.8%, it is possible to prepare the high-efficient active floridin with active degree being 204, decolorization ratio being 96%, the relative brightness being 82.
active floridin
/
wheel rolling method
/
active effect
/
activity degree
/
decolorization ratio
舒明勇;刘光辉.
轮碾法制备高效活性白土试验.
科技导报,
2012
, 30
(13)
: 57
-61
.
DOI: 10.3981/j.issn.1000-7857.2012.13.009
SHU Mingyong;LIU Guanghui.
Experiments on the Preparation of High-efficient Active Floridin by Wheel Rolling[J].
Science & Technology Review ,
2012
, 30
(13)
: 57
-61
.
DOI: 10.3981/j.issn.1000-7857.2012.13.009
2012年第30卷第13期
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文章信息
doi: 10.3981/j.issn.1000-7857.2012.13.009
接收时间:2012-01-27
首发时间:2012-05-08
出版时间:2012-05-08
收稿日期:2012-01-27
修回日期:2012-04-16
https://castjournals.cast.org.cn/joweb/kjdb/CN/10.3981/j.issn.1000-7857.2012.13.009
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2种不同金属材料的力学参数
科 Family 属数 Number of genus 种数 Number of species 占总种数比例 Percentage of total species (%) 属 Genus 种数 Number of species 占总种数比例 Percentage of total species (%) 鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78 小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39 多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39 红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87 小菇属 Mycena 11 5.26 光柄菇属 Pluteus 5 2.39 红菇属 Russula 17 8.13 栓菌属 Trametes 5 2.39
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