Article(id=1193230884070453861, tenantId=1146029695717560320, journalId=1149653034449285133, issueId=1193230615618220608, articleNumber=null, orderNo=null, doi=10.16790/j.cnki.1009-9239.im.2025.02.003, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=research-article, receivedDate=1711209600000, receivedDateStr=2024-03-24, revisedDate=1713888000000, revisedDateStr=2024-04-24, acceptedDate=null, acceptedDateStr=null, onlineDate=1762418011920, onlineDateStr=2025-11-06, pubDate=1739980800000, pubDateStr=2025-02-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1762418011920, onlineIssueDateStr=2025-11-06, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1762418011920, creator=13701087609, updateTime=1762418011920, updator=13701087609, issue=Issue{id=1193230615618220608, tenantId=1146029695717560320, journalId=1149653034449285133, year='2025', volume='58', issue='2', pageStart='1', pageEnd='138', issueExtLink='null', onlineDate='null', pubDate='null', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1762417947916, creator=13701087609, updateTime=1762418457365, updator=13701087609, preIssue=null, nextIssue=null, ext={EN=IssueExt(id=1193232752444145866, tenantId=1146029695717560320, journalId=1149653034449285133, issueId=1193230615618220608, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1193232752444145867, tenantId=1146029695717560320, journalId=1149653034449285133, issueId=1193230615618220608, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null}, startPage=16, endPage=24, ext={EN=ArticleExt(id=1193230884263391846, articleId=1193230884070453861, tenantId=1146029695717560320, journalId=1149653034449285133, language=EN, title=Effect of micro-water on insulation properties and decomposition characteristics of C₆F₁₂O/CO₂ gas mixture, columnId=1193230616230588994, journalTitle=Insulating Materials, columnName=Special Issue on Eco-friendly Insulating Gas, runingTitle=null, highlight=

C₆F₁₂O has good environmental protection characteristics and insulation properties, and has good application prospects in medium and low voltage gas-insulated equipment. In order to explore the influence of micro-water inside the gas-insulated equipment on the insulation performance and decomposition characteristics of C₆F₁₂O/CO₂ gas mixture, a gas power frequency breakdown test platform was set up, and the breakdown voltage of 4%C₆F₁₂O/96%CO₂ gas mixture under 0.14 MPa pressure within the range of 0-1 000 μL/L micro-water concentration was studied.The influence of different micro-water concentration on the power frequency breakdown characteristics of gas mixture was analyzed. The types and concentrations of the decomposition products of C₆F₁₂O/CO₂ gas mixture were analyzed quantitatively and qualitatively by gas chromatography-mass spectrometry (GC-MS) after breakdown, and the influence laws of micro-water concentration on the concentration of breakdown decomposition products and effective gas production rate were obtained. The results show that micro-water will reduce the power frequency breakdown voltage of C₆F₁₂O/CO₂ gas mixture. The main breakdown decomposition products of C₆F₁₂O/CO₂ gas mixture are CF₄, C₂F₆, C₃F₆, C₃F₈, C₃F₇H, CF₂O, C₄F₁₀, C₅F₁₂, and CF₃H, among them, the concentration and effective gas production rate of CF₄, C₂F₆, and C₃F₇H are positively correlated with the micro-water concentration, and the concentration of CF₄, C₂F₆, C₃F₆, C₃F₈, and C₃F₇H are positively correlated with the breakdown times. Considering the insulation performance and decomposition characteristics, it is recommended to strictly control the concentration of micro-water inside the C₆F₁₂O/CO₂ gas mixtures equipment during engineering application, and increase the test frequency of micro-water in the equipment.

, articleAbstract=

C₆F₁₂O has good environmental protection characteristics and insulation properties, and has good application prospects in medium and low voltage gas-insulated equipment. In order to explore the influence of micro-water inside the gas-insulated equipment on the insulation performance and decomposition characteristics of C₆F₁₂O/CO₂ gas mixture, a gas power frequency breakdown test platform was set up, and the breakdown voltage of 4%C₆F₁₂O/96%CO₂ gas mixture under 0.14 MPa pressure within the range of 0-1 000 μL/L micro-water concentration was studied.The influence of different micro-water concentration on the power frequency breakdown characteristics of gas mixture was analyzed. The types and concentrations of the decomposition products of C₆F₁₂O/CO₂ gas mixture were analyzed quantitatively and qualitatively by gas chromatography-mass spectrometry (GC-MS) after breakdown, and the influence laws of micro-water concentration on the concentration of breakdown decomposition products and effective gas production rate were obtained. The results show that micro-water will reduce the power frequency breakdown voltage of C₆F₁₂O/CO₂ gas mixture. The main breakdown decomposition products of C₆F₁₂O/CO₂ gas mixture are CF₄, C₂F₆, C₃F₆, C₃F₈, C₃F₇H, CF₂O, C₄F₁₀, C₅F₁₂, and CF₃H, among them, the concentration and effective gas production rate of CF₄, C₂F₆, and C₃F₇H are positively correlated with the micro-water concentration, and the concentration of CF₄, C₂F₆, C₃F₆, C₃F₈, and C₃F₇H are positively correlated with the breakdown times. Considering the insulation performance and decomposition characteristics, it is recommended to strictly control the concentration of micro-water inside the C₆F₁₂O/CO₂ gas mixtures equipment during engineering application, and increase the test frequency of micro-water in the equipment.

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C₆F₁₂O具有良好的环保特性和绝缘性能，在中低压气体绝缘设备中具有良好的应用前景。为探究气体绝缘设备内部的微水对C₆F₁₂O/CO₂混合气体绝缘性能和分解特性的影响，本文搭建气体工频击穿试验平台，测试0～1 000 μL/L微水浓度范围内0.14 MPa气压下4%C₆F₁₂O/96%CO₂混合气体的击穿电压，分析不同微水浓度对混合气体工频击穿特性的影响。使用气相色谱质谱联用仪（GC-MS）定性定量分析C₆F₁₂O/CO₂混合气体工频击穿后分解产物的种类和浓度，获得微水浓度对击穿分解产物浓度和有效产气速率的影响规律。结果表明：微水会降低C₆F₁₂O/CO₂混合气体的工频击穿电压。C₆F₁₂O/CO₂混合气体的主要击穿分解产物为CF₄、C₂F₆、C₃F₆、C₃F₈、C₃F₇H、CF₂O、C₄F₁₀、C₅F₁₂和CF₃H，其中CF₄、C₂F₆和C₃F₇H的浓度及有效产气速率与微水浓度呈正相关，CF₄、C₂F₆、C₃F₆、C₃F₈、C₃F₇H的浓度与击穿次数呈正相关。综合考虑绝缘性能和分解特性，建议在工程应用中严格控制C₆F₁₂O/CO₂混合气体设备内部微水的浓度，同时提高设备微水的检测频率。

, articleAbstract=

C₆F₁₂O具有良好的环保特性和绝缘性能，在中低压气体绝缘设备中具有良好的应用前景。为探究气体绝缘设备内部的微水对C₆F₁₂O/CO₂混合气体绝缘性能和分解特性的影响，本文搭建气体工频击穿试验平台，测试0～1 000 μL/L微水浓度范围内0.14 MPa气压下4%C₆F₁₂O/96%CO₂混合气体的击穿电压，分析不同微水浓度对混合气体工频击穿特性的影响。使用气相色谱质谱联用仪（GC-MS）定性定量分析C₆F₁₂O/CO₂混合气体工频击穿后分解产物的种类和浓度，获得微水浓度对击穿分解产物浓度和有效产气速率的影响规律。结果表明：微水会降低C₆F₁₂O/CO₂混合气体的工频击穿电压。C₆F₁₂O/CO₂混合气体的主要击穿分解产物为CF₄、C₂F₆、C₃F₆、C₃F₈、C₃F₇H、CF₂O、C₄F₁₀、C₅F₁₂和CF₃H，其中CF₄、C₂F₆和C₃F₇H的浓度及有效产气速率与微水浓度呈正相关，CF₄、C₂F₆、C₃F₆、C₃F₈、C₃F₇H的浓度与击穿次数呈正相关。综合考虑绝缘性能和分解特性，建议在工程应用中严格控制C₆F₁₂O/CO₂混合气体设备内部微水的浓度，同时提高设备微水的检测频率。

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田双双（1989-），女（汉族），湖北武汉人，副教授，博士，研究方向为气体绝缘设备在线检测与故障诊断、SF6替代气体。

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田双双（1989-），女（汉族），湖北武汉人，副教授，博士，研究方向为气体绝缘设备在线检测与故障诊断、SF6替代气体。

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标准名称	微水浓度/(μL/L)
	灭弧气室	非灭弧气室
GB/T 8905—2012	交接验收值≤150 运行允许值≤300	交接验收值≤250 运行允许值≤500
DL/T 603—2017	交接验收值≤150 运行允许值≤500	交接验收值≤250 运行允许值≤800
Q/CSG 1206007—2017	交接验收值≤150 运行允许值≤300	交接验收值≤250 运行允许值≤1000

), ArticleFig(id=1193616361151754682, tenantId=1146029695717560320, journalId=1149653034449285133, articleId=1193230884070453861, language=CN, label=表1, caption=

SF₆气体绝缘设备的微水浓度标准

, figureFileSmall=null, figureFileBig=null, tableContent=

标准名称	微水浓度/(μL/L)
	灭弧气室	非灭弧气室
GB/T 8905—2012	交接验收值≤150 运行允许值≤300	交接验收值≤250 运行允许值≤500
DL/T 603—2017	交接验收值≤150 运行允许值≤500	交接验收值≤250 运行允许值≤800
Q/CSG 1206007—2017	交接验收值≤150 运行允许值≤300	交接验收值≤250 运行允许值≤1000

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