Article(id=1297161238325252248, tenantId=1146029695717560320, journalId=1296125381406982186, issueId=1297161216049308076, articleNumber=null, orderNo=null, doi=10.13550/j.jxhg.20250279, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1745164800000, receivedDateStr=2025-04-21, revisedDate=null, revisedDateStr=null, acceptedDate=1748275200000, acceptedDateStr=2025-05-27, onlineDate=1787196939306, onlineDateStr=2026-08-20, pubDate=1778774400000, pubDateStr=2026-05-15, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1787196939306, onlineIssueDateStr=2026-08-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1787196939306, creator=13701087609, updateTime=1787196939306, updator=13701087609, issue=Issue{id=1297161216049308076, tenantId=1146029695717560320, journalId=1296125381406982186, year='2026', volume='43', issue='5', pageStart='929', pageEnd='1184', issueExtLink='null', onlineDate='null', pubDate='1778774400000', pubDateStr='2026-05-15', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=1, specialIssue=null, createTime=1787196933996, creator='13701087609', updateTime=1787202244949, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1297183491922354645, tenantId=1146029695717560320, journalId=1296125381406982186, issueId=1297161216049308076, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1297183491922354646, tenantId=1146029695717560320, journalId=1296125381406982186, issueId=1297161216049308076, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1121, endPage=1135, ext={EN=ArticleExt(id=1297161238534967449, articleId=1297161238325252248, tenantId=1146029695717560320, journalId=1296125381406982186, language=EN, title=Preparation and properties of diosmetin-loaded nanoemulsions coated with lotus seed protein peptides/tea saponin, columnId=null, journalTitle=Fine Chemicals, columnName=null, runingTitle=null, highlight=null, articleAbstract=

A lotus seed protein peptide (LSP)/tea saponin (TS) coated diosmetin (Dios) nanoemulsion (Dios-NE) based on a natural emulsifier system formulated with LSP and TS was prepared by dispersing and encapsulating the lipophilic active ingredient Dios in rapeseed oil, and characterized by FTIR, SEM, nanoparticle size analyzer and polarizing microscopy. The effects of m(LSP)∶m(TS), volume ratio of dispersed phase to deionized water (oil-to-water ratio) and homogenization pressure on the particle size of Dios-NE were investigated through response surface experiment. The in vitro antioxidant activity of Dios-NE was evaluated using 1,1-diphenyl-2-picrylhydrazyl (DPPH) radical and 2,2'-azino-bis (3-ethylbenzothiazoline-6-sulfonic acid)diammonium salt (ABTS) cation radical scavenging assays, while the gradient sustained-release performance and bioaccessibility of Dios-NE were assessed through simulated digestion experiments. The results indicated that, under the optimal preparation conditions of mass ratio of m(LSP)∶m(TS)=3∶20, oil-to-water ratio 5∶95, homogenization pressure 172.375 MPa, Dios-NE showed a particle size of (138.8±0.2) nm, with Dios stably embedded within the emulsion core by hydrophobic interactions and hydrogen bonding. Dios-NE maintained stable particle size and Zeta potential across a wide range of conditions, including pH (2~11), NaCl concentration (0~50 mmol/L), and temperature (30~90 ℃). The controlled-release properties of Dios-NE and the synergistic antioxidant effects of LSP/TS significantly enhanced the scavenging abilities for DPPH radical and ABTS+ radical, reaching 99% at a mass concentration of 24 mg/L. Dios-NE could delay the degradation of Dios in gastric fluid (retention rate 87%) and achieve targeted release in intestinal fluid through micellization, with a bioaccessibility of 57%.

, authors=Han LUO1, Wei FAN1, Shiyin GUO1, Zhonghai TANG1, Na ZHANG2, *, authorsList=Han LUO, Wei FAN, Shiyin GUO, Zhonghai TANG, Na ZHANG, authorCompany=null, correspAuthors=Na ZHANG, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1297161238925037723, articleId=1297161238325252248, tenantId=1146029695717560320, journalId=1296125381406982186, language=CN, title=莲子蛋白肽/茶皂素包覆香叶木素纳米乳液的制备及性能, columnId=1297161238627242138, journalTitle=精细化工, columnName=食品与营养化学品, runingTitle=null, highlight=null, articleAbstract=

以莲子蛋白肽(LSP)和茶皂素(TS)为原料,经菜籽油分散和包覆亲脂性活性成分香叶木素(Dios),制备了一种LSP/TS包覆香叶木素纳米乳液(Dios-NE)。采用FTIR、SEM、纳米粒度分析仪和偏光显微镜对Dios-NE进行了表征。通过响应面实验考察了m(LSP)∶m(TS)、分散相与去离子水体积比(简称油水比)及均质压力对Dios-NE粒径的影响,基于1,1-二苯基-2-三硝基苯肼(DPPH)自由基和2,2′-联氮双(3-乙基苯并噻唑啉-6-磺酸)二铵盐(ABTS)阳离子(ABTS+)自由基清除实验,探究了Dios-NE的体外抗氧化活性;通过模拟消化实验,评价了Dios-NE的梯度缓释性能和生物可及性。结果表明,Dios-NE的最佳制备条件为m(LSP)∶m(TS)=3∶20、油水比5∶95、均质压力172.375 MPa,在该条件下制备的Dios-NE乳液粒径为(138.8±0.2) nm,Dios通过疏水作用与氢键稳定地嵌入乳液核心,其在pH(2~11)、NaCl浓度(0~50 mmol/L)和温度(30~90 ℃)等较宽泛条件下仍能维持粒径与Zeta电位的稳定。Dios-NE的控释特性和LSP/TS的协同抗氧化作用显著提升了其DPPH自由基和ABTS+自由基清除能力,质量浓度为24 mg/L的Dios-NE对ABTS+自由基的清除率为99%;Dios-NE可以延缓Dios在胃液中降解(保留率为87%),并在肠液中通过胶束化实现靶向释放,生物可及率为57%。

, authors=罗涵1, 范伟1, 郭时印1, 唐忠海1, 张娜2, *, authorsList=罗涵, 范伟, 郭时印, 唐忠海, 张娜, authorCompany=null, correspAuthors=张娜, authorNote=

罗涵(2001—),男,硕士生,E-mail:

, correspAuthorsNote=
张娜(1981—),女,副教授,博士,E-mail:
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莲子蛋白肽/茶皂素包覆香叶木素纳米乳液的制备及性能
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罗涵 1 , 范伟 1 , 郭时印 1 , 唐忠海 1 , 张娜 2, *
精细化工 | 食品与营养化学品 2026,43(5): 1121-1135
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精细化工 |食品与营养化学品 2026 , 43 (5) : 1121 -1135
莲子蛋白肽/茶皂素包覆香叶木素纳米乳液的制备及性能
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罗涵1 , 范伟1, 郭时印1, 唐忠海1, 张娜2, *
作者信息
  • 1.湖南农业大学 食品科学技术学院 湖南省菜籽油营养健康与深度开发工程技术研究中心,湖南 长沙 410128
  • 2.塔里木大学 食品科学与工程学院 南疆特色农产品深加工兵团重点实验室,新疆 阿拉尔 843300
通讯作者:
张娜(1981—),女,副教授,博士,E-mail:
作者简介:

罗涵(2001—),男,硕士生,E-mail:

Preparation and properties of diosmetin-loaded nanoemulsions coated with lotus seed protein peptides/tea saponin
Han LUO1 , Wei FAN1, Shiyin GUO1, Zhonghai TANG1, Na ZHANG2, *
Affiliations
  • 1.Hunan Engineering Technology Research Center for Rapeseed Oil Nutrition Health and Deep Development, School of Food Science and Technology, Hunan Agricultural University, Changsha 410128, Hunan, China
  • 2.Key Laboratory of Southern Xinjiang Special Agricultural Products Deep Processing Corps, College of Food Science and Engineering, Tarim University, Alar 843300, Xinjiang, China
出版时间: 2026-05-15 doi: 10.13550/j.jxhg.20250279
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以莲子蛋白肽(LSP)和茶皂素(TS)为原料,经菜籽油分散和包覆亲脂性活性成分香叶木素(Dios),制备了一种LSP/TS包覆香叶木素纳米乳液(Dios-NE)。采用FTIR、SEM、纳米粒度分析仪和偏光显微镜对Dios-NE进行了表征。通过响应面实验考察了m(LSP)∶m(TS)、分散相与去离子水体积比(简称油水比)及均质压力对Dios-NE粒径的影响,基于1,1-二苯基-2-三硝基苯肼(DPPH)自由基和2,2′-联氮双(3-乙基苯并噻唑啉-6-磺酸)二铵盐(ABTS)阳离子(ABTS+)自由基清除实验,探究了Dios-NE的体外抗氧化活性;通过模拟消化实验,评价了Dios-NE的梯度缓释性能和生物可及性。结果表明,Dios-NE的最佳制备条件为m(LSP)∶m(TS)=3∶20、油水比5∶95、均质压力172.375 MPa,在该条件下制备的Dios-NE乳液粒径为(138.8±0.2) nm,Dios通过疏水作用与氢键稳定地嵌入乳液核心,其在pH(2~11)、NaCl浓度(0~50 mmol/L)和温度(30~90 ℃)等较宽泛条件下仍能维持粒径与Zeta电位的稳定。Dios-NE的控释特性和LSP/TS的协同抗氧化作用显著提升了其DPPH自由基和ABTS+自由基清除能力,质量浓度为24 mg/L的Dios-NE对ABTS+自由基的清除率为99%;Dios-NE可以延缓Dios在胃液中降解(保留率为87%),并在肠液中通过胶束化实现靶向释放,生物可及率为57%。

莲子蛋白肽  /  茶皂素  /  菜籽油  /  香叶木素  /  复合乳化剂  /  模拟消化  /  食品化学品

A lotus seed protein peptide (LSP)/tea saponin (TS) coated diosmetin (Dios) nanoemulsion (Dios-NE) based on a natural emulsifier system formulated with LSP and TS was prepared by dispersing and encapsulating the lipophilic active ingredient Dios in rapeseed oil, and characterized by FTIR, SEM, nanoparticle size analyzer and polarizing microscopy. The effects of m(LSP)∶m(TS), volume ratio of dispersed phase to deionized water (oil-to-water ratio) and homogenization pressure on the particle size of Dios-NE were investigated through response surface experiment. The in vitro antioxidant activity of Dios-NE was evaluated using 1,1-diphenyl-2-picrylhydrazyl (DPPH) radical and 2,2'-azino-bis (3-ethylbenzothiazoline-6-sulfonic acid)diammonium salt (ABTS) cation radical scavenging assays, while the gradient sustained-release performance and bioaccessibility of Dios-NE were assessed through simulated digestion experiments. The results indicated that, under the optimal preparation conditions of mass ratio of m(LSP)∶m(TS)=3∶20, oil-to-water ratio 5∶95, homogenization pressure 172.375 MPa, Dios-NE showed a particle size of (138.8±0.2) nm, with Dios stably embedded within the emulsion core by hydrophobic interactions and hydrogen bonding. Dios-NE maintained stable particle size and Zeta potential across a wide range of conditions, including pH (2~11), NaCl concentration (0~50 mmol/L), and temperature (30~90 ℃). The controlled-release properties of Dios-NE and the synergistic antioxidant effects of LSP/TS significantly enhanced the scavenging abilities for DPPH radical and ABTS+ radical, reaching 99% at a mass concentration of 24 mg/L. Dios-NE could delay the degradation of Dios in gastric fluid (retention rate 87%) and achieve targeted release in intestinal fluid through micellization, with a bioaccessibility of 57%.

lotus peptide  /  tea saponin  /  rapeseed oil  /  diosmetin  /  composite emulsifiers  /  simulated digestion  /  food chemicals
罗涵, 范伟, 郭时印, 唐忠海, 张娜. 莲子蛋白肽/茶皂素包覆香叶木素纳米乳液的制备及性能. 精细化工, 2026 , 43 (5) : 1121 -1135 . DOI: 10.13550/j.jxhg.20250279
Han LUO, Wei FAN, Shiyin GUO, Zhonghai TANG, Na ZHANG. Preparation and properties of diosmetin-loaded nanoemulsions coated with lotus seed protein peptides/tea saponin[J]. Fine Chemicals, 2026 , 43 (5) : 1121 -1135 . DOI: 10.13550/j.jxhg.20250279
  • 国家自然科学基金项目(32360579)
  • 新疆建设兵团自然科学支持计划资助项目(2024DA045)
  • 郴州国家可持续发展议程创新示范区建设专项(2022SFQ49)
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2026年第43卷第5期
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doi: 10.13550/j.jxhg.20250279
  • 接收时间:2025-04-21
  • 首发时间:2026-08-20
  • 出版时间:2026-05-15
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  • 收稿日期:2025-04-21
  • 录用日期:2025-05-27
基金
国家自然科学基金项目(32360579)
新疆建设兵团自然科学支持计划资助项目(2024DA045)
郴州国家可持续发展议程创新示范区建设专项(2022SFQ49)
作者信息
    1.湖南农业大学 食品科学技术学院 湖南省菜籽油营养健康与深度开发工程技术研究中心,湖南 长沙 410128
    2.塔里木大学 食品科学与工程学院 南疆特色农产品深加工兵团重点实验室,新疆 阿拉尔 843300

通讯作者:

张娜(1981—),女,副教授,博士,E-mail:
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2种不同金属材料的力学参数

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Percentage of
total species (%)

Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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