Article(id=1297161235842233129, tenantId=1146029695717560320, journalId=1296125381406982186, issueId=1297161216049308076, articleNumber=null, orderNo=null, doi=10.13550/j.jxhg.20250216, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1743177600000, receivedDateStr=2025-03-29, revisedDate=null, revisedDateStr=null, acceptedDate=1747756800000, acceptedDateStr=2025-05-21, onlineDate=1787196938714, onlineDateStr=2026-08-20, pubDate=1778774400000, pubDateStr=2026-05-15, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1787196938714, onlineIssueDateStr=2026-08-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1787196938714, creator=13701087609, updateTime=1787196938714, updator=13701087609, issue=Issue{id=1297161216049308076, tenantId=1146029695717560320, journalId=1296125381406982186, year='2026', volume='43', issue='5', pageStart='929', pageEnd='1184', issueExtLink='null', onlineDate='null', pubDate='1778774400000', pubDateStr='2026-05-15', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=1, specialIssue=null, createTime=1787196933996, creator='13701087609', updateTime=1787202244949, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1297183491922354645, tenantId=1146029695717560320, journalId=1296125381406982186, issueId=1297161216049308076, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1297183491922354646, tenantId=1146029695717560320, journalId=1296125381406982186, issueId=1297161216049308076, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1057, endPage=1066, ext={EN=ArticleExt(id=1297161236030976810, articleId=1297161235842233129, tenantId=1146029695717560320, journalId=1296125381406982186, language=EN, title=Preparation and viscosity-reducing, emulsifying and foaming properties of polyquaternary cationic surfactants, columnId=null, journalTitle=Fine Chemicals, columnName=null, runingTitle=null, highlight=null, articleAbstract=

Polyquaternary ammonium salt cationic surfactants Tz-6C_nQC (n=12, 14, 16) containing a rigid triazine spacer group were prepared via a two-step method using N,N-dimethylalkylamine with different alkyl chain lengths (C₁₂, C₁₄, C₁₆), melamine and epichlorohydrin as raw materials. The Tz-6C_nQC were characterized by FTIR and ¹HNMR for chemical structure, and analyzed through tests on surface tension, conductivity, Krafft point, and rheological properties for its surface activity, with its viscosity reduction, emulsification, and foaming performance evaluated. The results showed that the critical micelle concentration (CMC) of Tz-6C₁₂QC was 0.17 mmol/L, significantly lower than that of dodecyltrimethylammonium bromide (14.0 mmol/L) with the same hydrophobic alkyl chain length, and CMC showed a regular decreasing trend with the increase of alkyl chains. The foaming performance of Tz-6C_nQC increased with the growth of alkyl chains, and the foaming volume was better than that of sodium dodecylbenzenesulfonate and sodium dodecylbenzenesulfonate, with the foaming volume reaching up to 150 mL. Tz-6C_nQC had good viscosity reduction effect on polyacrylamide (PHIII, relative molecular mass 8×10⁶~1×10⁷) solution, and the viscosity reduction efficiency was positively correlated with the length of alkyl chain, among which, Tz-6C₁₆QC exhibited the best performance under high temperature (45 ℃) and high concentration (1.00 mmol/L) conditions, and the viscosity of Tz-6C₁₆QC/PHIII water-soluble solution reduced to 2.42 Pa·s. The emulsification performance showed concentration dependence. At low concentration (≤1.00 mmol/L), the emulsification performance increased significantly with the increase of alkyl chain, and at high concentration (3.00~30.00 mmol/L), it decreased with the increase of alkyl chain, in which the separation time of Tz-6C₁₂QC solution at 30.00 mmol/L was 1527 min.

, authors=Yudong LIU¹, Chi MA^{1, *}, Risheng LONG², Mingrui SHAO¹, Qi WANG¹, Fan LI^{3, *}, authorsList=Yudong LIU, Chi MA, Risheng LONG, Mingrui SHAO, Qi WANG, Fan LI, authorCompany=null, correspAuthors=Chi MA, Fan LI, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1297161236446212908, articleId=1297161235842233129, tenantId=1146029695717560320, journalId=1296125381406982186, language=CN, title=多聚季铵盐阳离子表面活性剂的制备及降黏、乳化发泡性能, columnId=1297161236131640107, journalTitle=精细化工, columnName=表面活性剂, runingTitle=null, highlight=null, articleAbstract=

以三聚氰胺、环氧氯丙烷和不同烷基链（C₁₂、C₁₄、C₁₆）长度的N，N-二甲基烷基胺为原料，经两步法制备了含刚性三嗪间隔基的多聚季铵盐阳离子表面活性剂Tz-6C_nQC（n=12、14、16）。采用FTIR、¹HNMR对Tz-6C_nQC的化学结构进行了表征，通过对Tz-6C_nQC的表面张力、电导率、Krafft点及流变性能测试分析了其表面活性，并考察了其降黏、乳化和发泡性能。结果表明，Tz-6C₁₂QC的临界胶束浓度（CMC）为0.17 mmol/L，显著低于疏水烷基链长度相同的十二烷基三甲基溴化铵（14.00 mmol/L），并且随着烷基链的增长，CMC呈规律性降低趋势；其发泡性能随烷基链的增长而增强，且发泡量优于十二烷基硫酸钠及十二烷基苯磺酸钠，Tz-6C₁₆QC溶液的发泡量可达150 mL；Tz-6C_nQC对聚丙烯酰胺（PHIII，相对分子质量为8×10⁶~1×10⁷）体系具有良好的降黏效果，降黏效率与烷基链长度呈正相关，其中，Tz-6C₁₆QC在高温（45 ℃）、高浓度（1.00 mmol/L）下表现出最优性能，Tz-6C₁₆QC/PHIII水溶液剪切黏度降至2.42 Pa·s；Tz-6C_nQC的乳化性能呈现浓度依赖性，低浓度（≤1.00 mmol/L）时乳化性能随烷基链增长而显著增强，高浓度（3.00~30.00 mmol/L）时，随烷基链增长而降低，其中浓度为30.00 mmol/L的Tz-6C₁₂QC溶液分离时间为1527 min。

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刘雨东（2000—），男，硕士生，E-mail: 1416434077@qq.com。

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刘雨东（2000—），男，硕士生，E-mail: 1416434077@qq.com。

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