Article(id=1297161230750348029, tenantId=1146029695717560320, journalId=1296125381406982186, issueId=1297161216049308076, articleNumber=null, orderNo=null, doi=10.13550/j.jxhg.20250173, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1741881600000, receivedDateStr=2025-03-14, revisedDate=null, revisedDateStr=null, acceptedDate=1744819200000, acceptedDateStr=2025-04-17, onlineDate=1787196937500, onlineDateStr=2026-08-20, pubDate=1778774400000, pubDateStr=2026-05-15, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1787196937500, onlineIssueDateStr=2026-08-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1787196937500, creator=13701087609, updateTime=1787196937500, updator=13701087609, issue=Issue{id=1297161216049308076, tenantId=1146029695717560320, journalId=1296125381406982186, year='2026', volume='43', issue='5', pageStart='929', pageEnd='1184', issueExtLink='null', onlineDate='null', pubDate='1778774400000', pubDateStr='2026-05-15', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=1, specialIssue=null, createTime=1787196933996, creator='13701087609', updateTime=1787202244949, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1297183491922354645, tenantId=1146029695717560320, journalId=1296125381406982186, issueId=1297161216049308076, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1297183491922354646, tenantId=1146029695717560320, journalId=1296125381406982186, issueId=1297161216049308076, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1030, endPage=1036, ext={EN=ArticleExt(id=1297161230981034750, articleId=1297161230750348029, tenantId=1146029695717560320, journalId=1296125381406982186, language=EN, title=Preparation and flame retardancy of phosphorus-amine ion liquid type epoxy resin flame retardant, columnId=null, journalTitle=Fine Chemicals, columnName=null, runingTitle=null, highlight=null, articleAbstract=

A phosphorus-amine ionic liquid, 1-(3-amino-3-oxopropyl)-3-propyl-imidazolium phosphate (IL) was prepared by quaternization reaction and ion exchange method using acrylamide, imidazole, 1-bromopropane, and sodium hypophosphite as raw materials, characterized via FTIR, ¹HNMR and HRMS, and then used as curing agent to obtain epoxy resin (EP) composites. The effect of IL mass fraction on the properties of EP composites was analyzed through SEM characterization, tensile strength, impact strength tests, limiting oxygen index, horizontal/vertical burning, thermal analysis and conical calorimetry experiments. The results showed that the addition of IL improved the mechanical properties of EP composites. When the mass fraction of IL was 6.4%, the impact strength of the prepared EP composites (EP-2) increased by 46.16% compared with that of pure EP (EP-0). Meanwhile, the addition of IL broadened the decomposition temperature range of EP composites, increased the residual carbon content, and significantly reduced the maximum heat release rate (PHRR) and total heat release (THR). When the mass fraction of IL was 8.4%, the PHRR of the prepared EP composites (EP-3) was 664.95 kW/m², a decrease of 27.86% compared with that of EP-0 (921.72 kW/m²), while THR decreased from 119.27 kJ/m² of EP-0 to 86.39 kJ/m², a decrease of 27.57%. The ultimate oxygen index reached 30.6%, and the horizontal/vertical combustion level reached V-0 level.

, authors=Shaowen WO¹, Yisong LIU², Bing LIANG^{1, *}, Jiapeng LONG^{1, *}, authorsList=Shaowen WO, Yisong LIU, Bing LIANG, Jiapeng LONG, authorCompany=null, correspAuthors=Bing LIANG, Jiapeng LONG, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1297161231291413247, articleId=1297161230750348029, tenantId=1146029695717560320, journalId=1296125381406982186, language=CN, title=磷-胺离子液体型环氧树脂阻燃剂的制备及阻燃性能, columnId=1297161221933913088, journalTitle=精细化工, columnName=功能材料, runingTitle=null, highlight=null, articleAbstract=

以丙烯酰胺、咪唑、1-溴丙烷和次亚磷酸钠为原料，采用季铵化反应和离子交换法制备了磷-胺离子液体1-(3-氨基-3-氧丙基)-3-丙基-咪唑次磷酸盐（IL）。采用FTIR、¹HNMR和HRMS确认了其结构。将其作为固化剂用于固化环氧树脂（EP），得到了EP复合材料。通过SEM表征和拉伸强度、冲击强度测试及极限氧指数、水平/垂直燃烧、热分析、锥形量热实验，探究了IL质量分数对EP复合材料性能的影响。结果表明，IL的添加提高了EP复合材料的力学性能，当IL质量分数为6.4%时，制备的EP复合材料（EP-2）的冲击强度比纯EP（EP-0）提高了46.16%。IL的加入拓宽了EP复合材料的分解温度区间，提高了残炭量，大幅降低了最大热释放速率（PHRR）和总释放热（THR），当其质量分数为8.4%时，制备的EP复合材料（EP-3）的PHRR为664.95 kW/m²，比EP-0（921.72 kW/m²）下降了27.86%，而THR从EP-0的119.27 kJ/m²降至86.39 kJ/m²，下降了27.57%，极限氧指数达到了30.6%，水平/垂直燃烧等级达到V-0级。

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沃少文（1998—），男，硕士生，E-mail: 1643539523@qq.com。

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沃少文（1998—），男，硕士生，E-mail: 1643539523@qq.com。

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